CN102429203A - Fluffy powdery compound sugar-free sweetening agent and preparation method thereof - Google Patents
Fluffy powdery compound sugar-free sweetening agent and preparation method thereof Download PDFInfo
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- CN102429203A CN102429203A CN201110407988XA CN201110407988A CN102429203A CN 102429203 A CN102429203 A CN 102429203A CN 201110407988X A CN201110407988X A CN 201110407988XA CN 201110407988 A CN201110407988 A CN 201110407988A CN 102429203 A CN102429203 A CN 102429203A
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Abstract
The invention relates to a fluffy powdery compound sugar-free sweetening agent and a preparation method thereof. The fluffy powdery compound sugar-free sweetening agent comprises the following components in percentage by weight: 30-79 percent of isomaltose oligosaccharide, 10-30 percent of erythrol, 10-30 percent of sucralose and 1-10 percent of neotame. The preparation method comprises the following steps of: adding sucralose into a heating container respectively, and adding deionized water for mixing; heating and stirring; adding active carbon into the sucralose solution, filtering while the solution is hot, and converging the filtrate into a storing tank for heating and preserving heat for later use; and crashing the isomaltose oligosaccharide, erythrol and neotame, putting into atomizing fluidized bed equipment, feeding the mixture into an atomizing fluidized bed under the positive pressure from the bottom of the atomizing fluidized bed, preparing the mixture flow from bottom to top at increasing speed, applying negative pressure to the upper part of the atomizing fluidized bed, vibrating from top to bottom to boil the material in the fluidized bed up and down, continually atomizing and dispersing the refined sucralose solution onto fine sugar alcohol by using a multipoint spraying gun on the side part of the fluidized bed, and performing continuous atomized drying to obtain the fluffy powdery compound sugar-free sweetening agent.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy powdery composite sugar-free sweetener and preparation method thereof.
Background technology
Along with people's is because of the increase with chronic metabolic disease such as too much inferior health that brings of sugar and cardiovascular and cerebrovasculars, the Sugarless type sweetener of people's demand safety, health; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; Make between the sweet substance sweet sense learn from other's strong points to offset one's weaknesses, have complementary advantages on the formula for a product; Can play during product uses cover, the effect of synergy and lifting mouthfeel; People crave for and are satisfying under the low prerequisite of sugariness height, heat, easy to useization, with cane-sugar taste safety and Health Sugarless type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy powdery composite sugar-free sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
Fluffy powdery composite sugar-free sweetener, characteristics are to comprise following percentage by weight composition: oligoisomaltose 30～79%, antierythrite 10～30%, Sucralose 10～30%, knob sweet 1～10%.
Further, above-mentioned fluffy powdery composite sugar-free sweetener, wherein, oligoisomaltose 60%, antierythrite 21.63%, Sucralose 16.7%, knob sweet 1.67%.
The preparation method of the fluffy powdery composite sugar-free sweetener of the present invention comprises following processing step:
1. Sucralose is joined in the heating container, add deionized water and mix;
2. be warming up to 50～100 ℃ of dissolvings, and stir;
3. add active carbon in the above-mentioned sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. with putting in the spray-fluidized bed apparatus after the sweet pulverizing of oligoisomaltose, antierythrite and knob; This mixed material also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously and is distributed on the fine sugar alcohol body; Spray-drying obtains fluffy powdery composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy powdery composite sugar-free sweetener: Sucralose is joined in the container, add deionized water and mix; Be warming up to 50～100 ℃ of dissolvings, and stir; Add active carbon, be incubated 30 minutes, filter while hot, filtrating is pooled in the storage tank that has heat tracing; Oligoisomaltose, antierythrite and knob are sweet to reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; This three's mixed material also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; Spray drying granulation obtains fluffy powdery composite sugar-free sweetener continuously.
Again further, the preparation method of above-mentioned fluffy powdery composite sugar-free sweetener, the bed temperature scope of said fluidized bed with spraying is 50～120 ℃, wherein the EAT of Sucralose spraying dispersion is 50～100 ℃.
Again further, the preparation method of above-mentioned fluffy powdery composite sugar-free sweetener, in the phase I of said Spray Mixing fluid bed, the Sucralose spraying is dispersed in fluidisation and smashes on the trickle crystalline mixture body;
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance bed temperature efficiently solves even dispersion, coats problems such as granulation, drying.With antierythrite, Sucralose, knob is sweet is primary raw material; Modify uniformly and coat through preparation method to sugariness, make product sweetness reach 50～200 times of common sucrose, products obtained therefrom does not have smell, even white; Soluble in water; This fluffy powdery composite sugar-free sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
The specific embodiment
The fluffy powdery composite sugar-free sweetener of the present invention, its composition is: oligoisomaltose 30～79%, antierythrite 10～30%, Sucralose 10～30%, knob sweet 1～10%.Ideal formulations is: oligoisomaltose 60%, antierythrite 21.63%, Sucralose 16.7%, knob sweet 1.67%.
The preparation technology of fluffy powdery composite sugar-free sweetener: at first, Sucralose is joined in the container, add deionized water and mix; Be warming up to 50～100 ℃ of dissolvings, and stir; Add active carbon, be incubated 30 minutes, filter while hot, filtrating is pooled in the storage tank that has heat tracing; Oligoisomaltose, antierythrite and knob are sweet to reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus (heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material again through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Passing through following steps again: mixed material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid mixture material of boiling); The mixed material that oligoisomaltose, antierythrite and knob are sweet also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece will the above-mentioned sucralose solution that refines continuously spraying be distributed on the trickle amalgam, the bed temperature of control Sucralose spraying dispersion is 50～100 ℃; Spray drying granulation obtains even sugariness and modifies good fluffy powder product continuously.
Embodiment 1:
14.2 kilograms of Sucraloses and deionized water are dissolved in stainless steel reacting by heating pot for 15 kilograms, and material is heated to 60 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation of filtrating; 69 kilograms of oligoisomaltoses; The sweet 1.42 kilograms of process pulverizers of 15.38 kilograms of antierythrites and knob are pulverized and are reached 150 orders; Mix also being sent in the spray-fluidized bed apparatus, this mixed material gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously and is distributed on the fine amalgam; Control fluidized-bed layer temperature is 50～120 ℃, and the multiple spot even spraying is disperseed, continuously spray drying granulation; Control EAT and mist flow well, obtain even sugariness and modify good fluffy powder product.
Embodiment 2:
18.4 kilograms of Sucraloses and deionized water are dissolved in stainless steel reacting by heating pot for 20 kilograms, and material is heated to 65 ℃ by chuck in the pot, starts stirring; Add 1.0 kilograms of active carbons; Be incubated 25 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation of filtrating; 59 kilograms of oligoisomaltoses; The sweet 1.84 kilograms of process pulverizers of 20.76 kilograms of antierythrites and knob are pulverized and are reached 160 orders; Mix also being sent in the spray-fluidized bed apparatus, this mixed material gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously and is distributed on the fine amalgam; Control fluidized-bed layer temperature is 50～120 ℃, and the multiple spot even spraying is disperseed, continuously spray drying granulation; Control EAT and mist flow well, obtain even sugariness and modify good fluffy powder product.
Embodiment 3:
12.5 kilograms of Sucraloses and deionized water are dissolved in stainless steel reacting by heating pot for 25 kilograms, and material is heated to 62 ℃ by chuck in the pot, starts stirring; Add 1.5 kilograms of active carbons; Be incubated 27 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation of filtrating; 65 kilograms of oligoisomaltoses; The sweet 1.25 kilograms of process pulverizers of 21.25 kilograms of antierythrites and knob are pulverized and are reached 160 orders; Mix also being sent in the spray-fluidized bed apparatus, this mixed material gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously and is distributed on the fine amalgam; Control fluidized-bed layer temperature is 50～120 ℃, and the multiple spot even spraying is disperseed, continuously spray drying granulation; Control EAT and mist flow well, obtain even sugariness and modify good fluffy powder product.
Embodiment 4:
16.7 kilograms of Sucraloses and deionized water are dissolved in stainless steel reacting by heating pot for 25 kilograms, and material is heated to 63 ℃ by chuck in the pot, starts stirring; Add 1.8 kilograms of active carbons; Be incubated 30 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation of filtrating; 60 kilograms of oligoisomaltoses; The sweet 1.67 kilograms of process pulverizers of 21.63 kilograms of antierythrites and knob are pulverized and are reached 170 orders; Mix also being sent in the spray-fluidized bed apparatus, this mixed material gets into the fluidized bed with spraying and quickens from bottom to top from the bottom of fluidized bed with spraying with malleation and flows, and the top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously and is distributed on the fine amalgam; Control fluidized-bed layer temperature is 50～120 ℃, and the multiple spot even spraying is disperseed, continuously spray drying granulation; Control EAT and mist flow well, obtain even sugariness and modify good fluffy powder product.
Through detecting, adopt the fluffy powdery composite sugar-free sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 60～100 orders | 60～100 orders | 60～100 orders | 60～100 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | White particle | White particle | White particle | White particle |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of the fluffy powdery composite sugar-free sweetener of the present invention, will according to knob sweet with the adjustment of Sucralose in consumption, be made into 50～200 times of common sucrose sugariness usually; The use needs that relatively are fit to food enterprise; Form according to prescription, under same sugariness situation, people compare with sucrose and can ignore the absorption of heat; This sweetener can not cause blood sugar to raise, and satisfies three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, evenly white, soluble in water, and it is very convenient that this fluffy powdery composite sugar-free sweetener is used.Granularity, dissolution velocity, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. fluffy powdery composite sugar-free sweetener is characterized in that comprising following percentage by weight composition: oligoisomaltose 30～79%, antierythrite 10～30%, Sucralose 10～30%, knob sweet 1～10%.
2. fluffy powdery composite sugar-free sweetener according to claim 1 is characterized in that its component has following percentage by weight: oligoisomaltose 60%, antierythrite 21.63%, Sucralose 16.7%, knob sweet 1.67%.
3. the preparation method of the described fluffy powdery composite sugar-free sweetener of claim 1 is characterized in that comprising following processing step:
1. Sucralose is joined in the heating container, add deionized water and mix;
2. be warming up to 50～100 ℃ of dissolvings, and stir;
3. add active carbon in the above-mentioned sucralose solution, be incubated 25～30 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. with putting in the spray-fluidized bed apparatus after the sweet pulverizing of oligoisomaltose, antierythrite and knob; This mixed material also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned sucralose solution that refines continuously and is distributed on the fine sugar alcohol body; Spray-drying obtains fluffy powdery composite sugar-free sweetener continuously.
4. the preparation method of fluffy powdery composite sugar-free sweetener according to claim 3 is characterized in that: Sucralose is joined in the container, add deionized water and mix; Be warming up to 50～100 ℃ of dissolvings, and stir; Add active carbon, be incubated 30 minutes, filter while hot, filtrating is pooled in the storage tank that has heat tracing; Oligoisomaltose, antierythrite and knob are sweet to reach 120～180 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; This three's mixed material also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidized-bed layer temperature is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece will the above-mentioned sucralose solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; Spray drying granulation obtains fluffy powdery composite sugar-free sweetener continuously.
5. the preparation method of fluffy powdery composite sugar-free sweetener according to claim 4 is characterized in that: the bed temperature scope of said fluidized bed with spraying is 50～120 ℃, and wherein the EAT of Sucralose spraying dispersion is 50～100 ℃.
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| CN201110407988XA CN102429203A (en) | 2011-12-09 | 2011-12-09 | Fluffy powdery compound sugar-free sweetening agent and preparation method thereof |
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| CN201110407988XA CN102429203A (en) | 2011-12-09 | 2011-12-09 | Fluffy powdery compound sugar-free sweetening agent and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110506922A (en) * | 2019-09-24 | 2019-11-29 | 湖南艾达伦科技有限公司 | A kind of Siraitia grosvenorii compound sweetener and preparation method thereof for stabilizing blood glucose |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1969674A (en) * | 2006-11-30 | 2007-05-30 | 吴江中怡实业有限公司 | Food additive |
| CN101897422A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Fluffy granular compound low-sugar low-calorie sweetening agent and preparation method thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1969674A (en) * | 2006-11-30 | 2007-05-30 | 吴江中怡实业有限公司 | Food additive |
| CN101897422A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Fluffy granular compound low-sugar low-calorie sweetening agent and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110506922A (en) * | 2019-09-24 | 2019-11-29 | 湖南艾达伦科技有限公司 | A kind of Siraitia grosvenorii compound sweetener and preparation method thereof for stabilizing blood glucose |
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Application publication date: 20120502 |