CN102423065A - Fluffy powder composite sweetening agent and preparation method thereof - Google Patents
Fluffy powder composite sweetening agent and preparation method thereof Download PDFInfo
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- CN102423065A CN102423065A CN2011104296152A CN201110429615A CN102423065A CN 102423065 A CN102423065 A CN 102423065A CN 2011104296152 A CN2011104296152 A CN 2011104296152A CN 201110429615 A CN201110429615 A CN 201110429615A CN 102423065 A CN102423065 A CN 102423065A
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Abstract
The present invention relates to a fluffy powder composite sweetening agent and a preparation method thereof. Components of the sweetening agent comprise: 4-18% of rebaudioside A, 5-25% of sucralose, 5-10% of xylitol, 25-65% of oligoisomaltose and 15-35% of erythritol. The preparation process comprises that: the rebaudioside A and the sucralose are respectively added to heating containers; deionized water are respectively added to the containers, and treatments of mixing, heating dissolving are performed; active carbon are respectively added to the resulting solutions, a filtration treatment is performed while hot, and the filtrates are respectively collected in a storage tank; the crushed erythritol, the crushed xylitol and the crushed oligoisomaltose are mixed, the positive pressure is applied, and the resulting mixture enters a spraying fluidized bed from the bottom of the spraying fluidized bed, and acceleratively flows from bottom to top; the negative pressure is applied on the upper part of the spraying fluidized bed, and the spraying fluidized bed vibrates from top to bottom, such that the material in the spraying fluidized bed boils upwards and downwards; the refined rebaudioside A solution is firstly continuously sprayed and dispersed on fine sugar alcohol bodies by a multi-point spray gun; then the sucralose solution is introduced by pumping; the treatment of continuous spray drying is performed to obtain the sugar-free low calory sweetening agent.
Description
Technical field
The present invention relates to a kind of edible sweetener, relate in particular to a kind of fluffy powdery composite sweetener and preparation method thereof.
Background technology
Along with people's is because of the increase with chronic metabolic disease such as too much inferior health that brings of sugar and cardiovascular and cerebrovasculars, people's demand safety, healthy Sugarless type sweetener; In production procedure, reach the advanced preparation technology who puts into finished product one step completion from raw material; Make between the sweet substance sweet sense learn from other's strong points to offset one's weaknesses, have complementary advantages on the formula for a product, can play during product uses cover, the effect of synergy and lifting mouthfeel.People crave for and are satisfying under the low prerequisite of sugariness height, heat, easy to useization, with cane-sugar taste safety and Health Sugarless type sweetener roughly the same.
Summary of the invention
The objective of the invention is to overcome the deficiency that prior art exists, a kind of fluffy powdery composite sugar-free type sweetener and preparation method thereof is provided, adopt the scientific technology of easy operation control, the molten speed property of product, mouthfeel, sugariness all are higher than the prior art optimum value.
The object of the invention is realized through following technical scheme:
Fluffy powdery composite sweetener, characteristics are to comprise following percentage by weight composition: Lai Baodi glycosides A 4 ~ 18%, Sucralose 5 ~ 25%, xylitol 5 ~ 10%, oligoisomaltose 25 ~ 65%, antierythrite 15 ~ 35%; Its preparation method comprises following processing step:
1. Lai Baodi glycosides A, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 45～100 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned Lai Baodi glycosides A solution and the sucralose solution, be incubated 10～20 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite and oligoisomaltose being pulverized; The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned Lai Baodi glycosides A solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned sucralose solution that refines again, spray-drying obtains a kind of fluffy powdery composite sweetener continuously.
Further, above-mentioned fluffy powdery composite sweetener, Lai Baodi glycosides A 4.3% wherein, Sucralose 5.83%, xylitol 8%, oligoisomaltose 51.87%, antierythrite 30%.
The preparation method of the fluffy powdery composite sweetener of the present invention comprises following processing step:
1. Lai Baodi glycosides A, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 45～100 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned Lai Baodi glycosides A solution and the sucralose solution, be incubated 10～20 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite and oligoisomaltose being pulverized; The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned Lai Baodi glycosides A solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned sucralose solution that refines again, spray-drying obtains a kind of fluffy powdery composite sweetener continuously.
Again further, the preparation method of above-mentioned fluffy powdery composite sweetener: Lai Baodi glycosides A, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 45～100 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 10 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and oligoisomaltose reach 100～160 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and control fluidisation EAT is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned Lai Baodi glycosides A solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned sucralose solution that refines again, spray drying granulation obtains a kind of fluffy powdery composite sweetener continuously.
Again further; The preparation method of above-mentioned fluffy powdery composite sweetener; The EAT scope of said fluidized bed with spraying is 50～120 ℃, and the bed temperature that first rank Lai Baodi glycosides A spraying disperses is 50～90 ℃, and the EAT of second stage Sucralose mist projection granulating is 60～120 ℃.
Again further, the preparation method of above-mentioned fluffy powdery composite sweetener, in the second stage of said Spray Mixing fluid bed, Lai Baodi glycosides A spraying is dispersed in fluidisation and smashes on the fine sugar alcohol crystal body; In the phase III, the Sucralose spray drying granulation is on the noncrystal of mixing sugar alcohol.
Substantive distinguishing features and obvious improvement that technical scheme of the present invention is outstanding are mainly reflected in:
Adopt the negative pressure fluid bed fluidization technique of scientific formula, uses advanced to combine the multi-point atomizing method, time sharing segment control appliance EAT efficiently solves even dispersion, coats problems such as granulation, drying.With antierythrite, xylitol, oligoisomaltose, Sucralose and Lai Baodi glycosides A is primary raw material; Modify uniformly and coat through preparation method to sugariness; Make product sweetness reach 50～200 times of common sucrose, products obtained therefrom does not have smell, even white, and is soluble in water.This a kind of fluffy powdery composite sweetener is easy to use, and its preparation process science is simple and easy to operate, is fit to very much large-scale production.
The specific embodiment
The fluffy powdery composite sweetener of the present invention, its composition is: Lai Baodi glycosides A 4 ~ 18%, Sucralose 5 ~ 25%, xylitol 5 ~ 10%, oligoisomaltose 25 ~ 65%, antierythrite 15 ~ 35%.Ideal formulations is: Lai Baodi glycosides A 4.3%, Sucralose 5.83%, xylitol 8%, oligoisomaltose 51.87%, antierythrite 30%.
The preparation technology of fluffy powdery composite sweetener: at first, Lai Baodi glycosides A, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 45～100 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 10 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and oligoisomaltose reach 100～160 orders through pulverizing; Be sent in the spray-fluidized bed apparatus (heating temperature control and technological with the boiling that in fluid bed, circulates of sugar alcohol material again through the positive negative pressure boiling of equipment; Mix that fluidisation is anhydrated and fluffy processing; Passing through following steps again: mixed material → malleation material quickens to flow from bottom to top → and negative pressure vibrates → makes material boiling up and down in fluid bed → by the fluid bed side multiple spot spray gun liquid material ejection fog-like liquid of naming a person for a particular job from top to bottom; Be sprayed onto on the trickle solid mixture material of boiling); The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned Lai Baodi glycosides A solution that refines continuously earlier and is distributed on the trickle amalgam, and the EAT that control Lai Baodi glycosides A spraying disperses is 50～90 ℃, and Lai Baodi glycosides A even spraying is dispersed on the mixing sugar alcohol crystalline solid of powder; The rising bed temperature; At mixing sugar alcohol after fluidisation loses surface crystallization water; Pump into the above-mentioned sucralose solution that refines again; Continuous spray drying granulation, the EAT of Sucralose mist projection granulating controlled well is 60～120 ℃, the Sucralose spray drying granulation is on the noncrystalline fluffy body of sugar alcohol; Obtain even sugariness and modify good fluffy powder product.
Embodiment 1:
4.3 kilograms of Lai Baodi glycosides A and deionized water are dissolved in a stainless steel reacting by heating pot for 15 kilograms; 5.83 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20 kilograms, and material is heated to 80 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon respectively; Be incubated 10 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 8 kilograms of xylitols, 30 kilograms of antierythrites, 51.87 kilograms of oligoisomaltoses; Pulverizing reaches 120 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned Lai Baodi glycosides A solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidisation EAT is 50～90 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed EAT to 60～120 ℃ again, the fluidisation of xylitol, antierythrite and oligoisomaltose mix lose surface crystallization water after; Pump into the above-mentioned sucralose solution that refines; Continuous spray drying granulation is controlled EAT and mist flow well, obtains even sugariness and modifies good fluffy powder product.
Embodiment 2:
8.6 kilograms of Lai Baodi glycosides A and deionized water are dissolved in a stainless steel reacting by heating pot for 15 kilograms; 11.66 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 20.0 kilograms, and material is heated to 85 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon respectively; Be incubated 10 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 5 kilograms of xylitols, 28 kilograms of antierythrites, 46.74 kilograms of oligoisomaltoses; Pulverizing reaches 120 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned Lai Baodi glycosides A solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidisation EAT is 50～90 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed EAT to 60～120 ℃ again, the fluidisation of xylitol, antierythrite and oligoisomaltose mix lose surface crystallization water after; Pump into the above-mentioned sucralose solution that refines; Continuous spray drying granulation is controlled EAT and mist flow well, obtains even sugariness and modifies good fluffy powder product.
Embodiment 3:
12.9 kilograms of Lai Baodi glycosides A and deionized water are dissolved in a stainless steel reacting by heating pot for 20 kilograms; 17.49 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 30.0 kilograms, and material is heated to 85 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon respectively; Be incubated 10 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 5 kilograms of xylitols, 18 kilograms of antierythrites, 46.61 kilograms of oligoisomaltoses; Pulverizing reaches 120 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned Lai Baodi glycosides A solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidisation EAT is 50～90 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed EAT to 60～120 ℃ again, the fluidisation of xylitol, antierythrite and oligoisomaltose mix lose surface crystallization water after; Pump into the above-mentioned sucralose solution that refines; Continuous spray drying granulation is controlled EAT and mist flow well, obtains even sugariness and modifies good fluffy powder product.
Embodiment 4:
17.2 kilograms of Lai Baodi glycosides A and deionized water are dissolved in a stainless steel reacting by heating pot for 30 kilograms; 23.32 kilograms of Sucraloses and deionized water are also dissolved in another stainless steel reacting by heating pot for 30.0 kilograms, and material is heated to 85 ℃ by chuck in the pot, starts stirring; Add 0.5 kilogram of active carbon respectively; Be incubated 10 minutes, filter while hot, for use in the storage tank that collects in the chuck insulation respectively of filtrating; 5 kilograms of xylitols, 21 kilograms of antierythrites, 33.48 kilograms of oligoisomaltoses; Pulverizing reaches 120 orders through pulverizer, is sent in the spray-fluidized bed apparatus, and the mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned Lai Baodi glycosides A solution that refines continuously spraying be distributed on the fine sugar alcohol body, controlling the fluidisation EAT is 50～70 ℃; The multiple spot even spraying is disperseed; After operation is accomplished, improve bed EAT to 60～120 ℃ again, the fluidisation of xylitol, antierythrite and oligoisomaltose mix lose surface crystallization water after; Pump into the above-mentioned sucralose solution that refines; Continuous spray drying granulation is controlled EAT and mist flow well, obtains even sugariness and modifies good fluffy powder product.
Through detecting, adopt the fluffy powdery composite sweetener of technical scheme acquisition of the present invention, its main performance index is seen table 1.
Table 1
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Particle size | 40～100 orders | 40～100 orders | 40～100 orders | 40～100 orders |
| Sugariness (sucrose contrast) | 50 times | 100 times | 150 times | 200 times |
| Outward appearance | The white powder | The white powder | The white powder | The white powder |
The stability test of sweetener is to check sweetener to guarantee the ability that undergoes no deterioration within a certain period of time, and the sweetener product of the embodiment of the invention was stored 3 years at normal temperatures, phenomenons such as rotten and sugariness reduction occur, and the stability ten minutes is superior.
The sugariness degree of modification of a kind of fluffy powdery composite sweetener of the present invention will be according to Lai Baodi glycosides A and the adjustment of Sucralose in consumption, 50～200 times of selecting the common sucrose sugariness usually for use; The use needs that relatively are fit to food enterprise; Form according to prescription, under same sugariness situation, people compare with sucrose and can ignore the absorption of heat; This sweetener can not cause blood sugar to raise, and satisfies three high crowds, pursues healthy needs of people.
Show obviously that to sum up the present invention adopts scientific formula, uses advanced science and technology technology and method, products obtained therefrom does not have smell, evenly white, soluble in water, and it is very convenient that this a kind of fluffy powdery composite sweetener is used.Granularity, dissolution velocity, mouthfeel, sugariness all are much better than the prior art value, and the scientific preparation process simple flow is prone to row, are fit to very much large-scale production, are worth wide popularization and application in the field of business.
What need understand is: the above only is a preferred implementation of the present invention; For those skilled in the art; Under the prerequisite that does not break away from the principle of the invention, can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (5)
1. fluffy powdery composite sweetener is characterized in that comprising following percentage by weight composition: Lai Baodi glycosides A 4 ~ 18%, Sucralose 5 ~ 25%, xylitol 5 ~ 10%, oligoisomaltose 25 ~ 65%, antierythrite 15 ~ 35%; Its preparation method comprises following processing step:
1. Lai Baodi glycosides A, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 45～100 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned Lai Baodi glycosides A solution and the sucralose solution, be incubated 10～20 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite and oligoisomaltose being pulverized; The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned Lai Baodi glycosides A solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned sucralose solution that refines again, spray-drying obtains a kind of fluffy powdery composite sweetener continuously.
2. fluffy powdery composite sweetener according to claim 1 is characterized in that its component has following percentage by weight: Lai Baodi glycosides A 4.3 %, Sucralose 5.83 %, xylitol 8%, oligoisomaltose 51.87%, antierythrite 30%.
3. the preparation method of the described fluffy powdery composite sweetener of claim 1 is characterized in that comprising following processing step:
1. Lai Baodi glycosides A, Sucralose are joined respectively in the heating container, add deionized water respectively and mix;
2. be warming up to 45～100 ℃ of dissolvings respectively, and stir;
3. add active carbon respectively in above-mentioned Lai Baodi glycosides A solution and the sucralose solution, be incubated 10～20 minutes, filter while hot, for use in the storage tank that is pooled to heat tracing respectively of filtrating;
4. put in the spray-fluidized bed apparatus after xylitol, antierythrite and oligoisomaltose being pulverized; The mixed material of xylitol, antierythrite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying impose negative pressure vibrate from top to bottom make material in fluid bed up and down the boiling; The multiple spot spray gun of fluid bed sidepiece is sprayed the above-mentioned Lai Baodi glycosides A solution that refines continuously earlier and is distributed on the fine sugar alcohol body; Pump into the above-mentioned sucralose solution that refines again, spray-drying obtains a kind of fluffy powdery composite sweetener continuously.
4. the preparation method of fluffy powdery composite sweetener according to claim 3 is characterized in that: Lai Baodi glycosides A, Sucralose are joined respectively in the container, add deionized water respectively and mix; Be warming up to 45～100 ℃ of dissolvings respectively, and stir; Add active carbon respectively, be incubated 10 minutes, filter while hot, filtrating is pooled to respectively in the storage tank that has heat tracing; Xylitol, antierythrite and oligoisomaltose reach 100～160 orders through pulverizing; Be sent in the spray-fluidized bed apparatus; The mixed material of xylitol, D-sorbite and oligoisomaltose also quickens to flow from the bottom entering fluidized bed with spraying of fluidized bed with spraying with malleation from bottom to top; The top of fluidized bed with spraying imposes negative pressure and vibrates from top to bottom and make material boiling up and down in fluid bed, and the control EAT is at 50～120 ℃, and the multiple spot spray gun of fluid bed sidepiece earlier will the above-mentioned Lai Baodi glycosides A solution that refines be sprayed continuously and is distributed on the fine sugar alcohol body; After the mixing of sugar alcohol fluidisation loses surperficial moisture content; Pump into the above-mentioned sucralose solution that refines again, spray drying granulation obtains a kind of fluffy powdery composite sweetener continuously.
5. the preparation method of fluffy powdery composite sweetener according to claim 4; It is characterized in that: the EAT scope of said fluidized bed with spraying is 50～120 ℃; Wherein the temperature of phase I dissolving making beating is 45～100 ℃; The EAT that second stage Lai Baodi glycosides A spraying disperses is 50～90 ℃, and the spray-dired EAT of second stage is 60～120 ℃.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101897426A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Granular composite sugar-free sweetener and preparation method thereof |
| CN102202523A (en) * | 2008-08-26 | 2011-09-28 | 梅里桑特公司 | Sweetener compositions comprising rebaudioside a, erythritol, a disaccharide carbohydrate or fructose and a taste-improving amount of cellulose, and methods for their manufacture |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102202523A (en) * | 2008-08-26 | 2011-09-28 | 梅里桑特公司 | Sweetener compositions comprising rebaudioside a, erythritol, a disaccharide carbohydrate or fructose and a taste-improving amount of cellulose, and methods for their manufacture |
| CN101897426A (en) * | 2009-12-04 | 2010-12-01 | 苏州工业园区尚融科技有限公司 | Granular composite sugar-free sweetener and preparation method thereof |
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Application publication date: 20120425 |