CN102417867A - Soaping agent composition for dyeing fabric and production method thereof - Google Patents
Soaping agent composition for dyeing fabric and production method thereof Download PDFInfo
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- CN102417867A CN102417867A CN2010105047881A CN201010504788A CN102417867A CN 102417867 A CN102417867 A CN 102417867A CN 2010105047881 A CN2010105047881 A CN 2010105047881A CN 201010504788 A CN201010504788 A CN 201010504788A CN 102417867 A CN102417867 A CN 102417867A
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- soaping
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Abstract
The invention provides a soaping agent composition for dyeing fabric and a production method thereof, and relates to the technical field of textile dyeing, and especially relates to soaping agent composition for dyeing fabric and a production method thereof. A formula of the composition comprises, by weight, 10-25% of fatty alcohol polyoxyethylene ether, 5-15% of fatty alcohol sulfate, 2-6% of alpha-alkenyl sulfonate, 4-8% of chelating auxiliary agent, 3-6% of resist printing salt S and 55-65% of water. Composition of the ingredients has good soaping and anti-contamination effects on reactive dyes of cotton, blending fabric and polyester cotton fabric, etc; a good soaping fastness can be realized without acid neutralization and high temperature soaping; besides, a process is simple, saves time and reduces consumption of water, electricity and steam, so as to lower cost and increase working efficiency.
Description
Technical field
The present invention relates to the textile dyeing technical field, relate in particular to a kind of textile dyeing with soaping agent compsn and working method thereof.
Background technology
As everyone knows, hydrolysis can take place last when dying set in reactive dyestuffs, and hydrolised dye is adsorbed on the colour fastness that can have a strong impact on dyeing product on the fiber, thereby must soap after the reactive dyeing.The main purpose of soaping is exactly in order to remove the hydrolised dye that attaches on fiber, not set dyestuff and other impurity.Usually use the basic soap lotion, cloth cover pH value be 10-11 in bathing when soaping, and is alkalescence, and reactive dyestuffs are prone to scission of link takes place when high temperature is soaped, so after the reactive dyestuffs alkali fixation, must wash through three times, and could get into the bath of soaping after making cloth cover pH value near neutrality carries out soap boiling.Nonetheless, the finished product that can not guarantee to dye is being accepted to soap under nearly neutrallty condition; Acid scouring agent is also arranged on the market, but washing effect and poor stability, and contain higher toxicity in the prescription, environment is caused very major injury, so the prior art existing problems have much room for improvement.
Summary of the invention
The objective of the invention is to provides a kind of good stability to the problems referred to above, and the textile dyeing of environmental protection is with soaping agent compsn and working method thereof.
Technical scheme of the present invention is following: the soaping agent compsn is used in textile dyeing; Form by weight percentage by following prescription: AEO: 10-25%, aliphatic alcohol sulfate: 5-15%, α-sodium olefin sulfonate: 2-6%, chelating auxiliary agent: 4-8%, reservehao S: 3-6%, water: 55-65%, wherein: the chelating auxiliary agent be YD 30, nitrilotriacetic acid or Citrate trianion wherein any.
Preferably, said soaping agent compsn is made up of following prescription by weight percentage: AEO: aliphatic alcohol sulfate 24%: α-sodium olefin sulfonate 5%: chelating auxiliary agent 3%: reservehao S 5%: 5% and water: 58%.
Said soaping agent composition manufacturing method comprises the steps:
Steps A, in the reaction kettle that whisking appliance is housed, add chelating auxiliary agent and water, the powerful stirring half a hour forms solution; Step B, AEO, aliphatic alcohol sulfate and α-sodium olefin sulfonate are joined in the said solution; Under constantly stirring, be heated to 55～60 ℃, make it to dissolve the back and add reserve salt, stirred 45 minutes; And insulation reaction 1～2 hour, be cooled to 30 ℃ of dischargings.
The effect one of soaping agent is to have stronger washing power, the 2nd, have dissemination, and it has following performance: a, solubilising: increase the auxiliary agent that remains on the fabric and reach the not solvability of combination dye; B, chelating: play sequestering action with high volence metal ion, the softening washing water; C, dispersion: the solid dirt is had anti-freezing effect of gathering and dissemination; D, washing: the auxiliary agent and the unconjugated dyestuff that will remain on the fabric wash; C, emulsification and anti-contamination effect: auxiliary agent, the dyestuff of washing are emulsified in the solution equably, form micella, prevent to stain again on the fabric, form micella at fabric face on the other hand, prevent that auxiliary agent, dyestuff that washing is got off from staiing on the fabric again; F, an alkaline shock absorption: replace using in the general washing alkaline matters such as soda ash.
The soaping agent compsn is used in textile dyeing provided by the present invention, adopts the plurality of raw materials formulated in combination to form, and wherein: AEO (secondary AEO-9) has emulsification, decomposition, washing, anti-contamination effect; Aliphatic alcohol sulfate has emulsification, infiltration, decontamination, solubilising function; α-sodium olefin sulfonate has solvability, infiltration and Water purification preferably; Chelating selection of auxiliary YD 30, nitrilotriacetic acid or Citrate trianion wherein any, have good chelating, dispersion and pooling feature; Reservehao S, another name: the 3-nitrobenzene sodium sulfonate has solubilising, anti-stains, improves the doing of fabric, fastness to wet rubbing and soaping fastness.The compsn of these components all has good soaping and anti-contamination effect to reactive dyestuffs of cotton textiles, BLENDED FABRIC, polyester-cotton fabric etc.; Need not to carry out the acid neutralization; Do not need high temperature to soap, can reach good soaping fastness, and technology simple, save time and reduce water, electricity, the steam consumption and use; Reduce cost, increase work efficiency.
Embodiment
Embodiment 1
1, textile dyeing is with the prescription (weight percent) of soaping agent compsn: AEO: aliphatic alcohol sulfate 14%: α-sodium olefin sulfonate 12%: YD 30 4%: reservehao S 5%: water 3%: 62%;
2, in the reaction kettle that whisking appliance is housed, add 5 kilograms of YD 30s and 62 kg of water, the powerful stirring half a hour forms solution; 14 kilograms of AEOs, 12 kilograms of aliphatic alcohol sulfates and α-sodium olefin sulfonate are joined in the solution for 4 kilograms; Under constantly stirring, be heated to 58 ℃, make it to dissolve the back and add 3 kilograms of reserve salts, stirred 45 minutes; And insulation reaction 1.5 hours, be cooled to 30 ℃ of dischargings and be finished product.Adopt following method to be applied on the fabric: to take by weighing 0.4 kilogram of soaping agent composition dissolves in 93.6 kg of water, add 6 kilograms of cottons and knit active emerald green DYED FABRICS, be warming up to 95 degree and soaped 12 minutes, cooling, cold wash oven dry.
Embodiment 2:
1, by following formulated soaping agent compsn: AEO: aliphatic alcohol sulfate 24%: α-sodium olefin sulfonate 5%: Citrate trianion 3%: reservehao S 5%: 5% and water: 58%.
2, in the reaction kettle that whisking appliance is housed, add 5 kilograms of Citrate trianions and 58 kg of water, the powerful stirring half a hour forms solution; 24 kilograms of AEOs, 5 kilograms of aliphatic alcohol sulfates and α-sodium olefin sulfonate are joined in the solution for 3 kilograms; Under constantly stirring, be heated to 55 ℃, make it to dissolve the back and add 5 kilograms of reserve salts, stirred 45 minutes; And insulation reaction 1 hour, be cooled to 30 ℃ of dischargings and be finished product.Adopt following method to be applied on the fabric: to take by weighing 0.3 kilogram of soaping agent composition dissolves in 93.7 kg of water, add 6 kilograms of cottons and knit reactive violet red colouring fabric, be warming up to 96 degree and soaped 8 minutes, cooling, cold wash oven dry.
Embodiment 3:
1, textile dyeing is with the prescription (weight percent) of soaping agent compsn: AEO: aliphatic alcohol sulfate 19%: α-sodium olefin sulfonate 7%: nitrilotriacetic acid 3%: reservehao S 6%: water 4%: 55%;
2, in the reaction kettle that whisking appliance is housed, add 6 kilograms of nitrilotriacetic acids and 55 kg of water, the powerful stirring half a hour forms solution; 19 kilograms of AEOs, 7 kilograms of aliphatic alcohol sulfates and α-sodium olefin sulfonate are joined in the solution for 3 kilograms; Under constantly stirring, be heated to 55 ℃, make it to dissolve the back and add 4 kilograms of reserve salts, stirred 45 minutes; And insulation reaction 1.5 hours, be cooled to 30 ℃ of dischargings and be finished product.Adopt following method to be applied on the fabric: to take by weighing 0.35 kilogram of soaping agent composition dissolves in 93.65 kg of water, add 6 kilograms of cottons and knit active purple DYED FABRICS, be warming up to 95 degree and soaped 8 minutes, cooling, cold wash oven dry.
What should explain is; Above embodiment is only unrestricted in order to technical scheme of the present invention to be described; Although with reference to preferred embodiment the present invention is specified, those of ordinary skill in the art should be appreciated that and can make amendment or be equal to replacement technical scheme of the present invention; And not breaking away from the spirit and the scope of technical scheme of the present invention, it all should be encompassed in the middle of the claim scope of the present invention.
Claims (4)
1. the soaping agent compsn is used in textile dyeing, it is characterized in that: be made up of by weight percentage following prescription:
AEO 10-25%
Aliphatic alcohol sulfate 5-15%
α-sodium olefin sulfonate 2-6%
Chelating auxiliary agent 4-8%
Reservehao S 3-6%
Water 55-65%.
2. the soaping agent compsn is used in textile dyeing according to claim 1, it is characterized in that: said chelating auxiliary agent be YD 30, nitrilotriacetic acid or Citrate trianion wherein any.
3. the soaping agent compsn is used in textile dyeing according to claim 1, it is characterized in that: said compsn is made up of following prescription by weight percentage:
AEO: aliphatic alcohol sulfate 24%: α-sodium olefin sulfonate 5%: chelating auxiliary agent 3%: reservehao S 5%: 5% and water: 58%.
4. produce textile dyeing as claimed in claim 1 and use the soaping agent method for compositions, it is characterized in that: comprise the steps:
Steps A, in the reaction kettle that whisking appliance is housed, add chelating auxiliary agent and water, the powerful stirring half a hour forms solution;
Step B, AEO, aliphatic alcohol sulfate and α-sodium olefin sulfonate are joined in the said solution; Under constantly stirring, be heated to 5560 ℃, make it to dissolve the back and add reserve salt, stirred 45 minutes; And insulation reaction 1～2 hour, be cooled to 30 ℃ of dischargings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105047881A CN102417867A (en) | 2010-09-28 | 2010-09-28 | Soaping agent composition for dyeing fabric and production method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010105047881A CN102417867A (en) | 2010-09-28 | 2010-09-28 | Soaping agent composition for dyeing fabric and production method thereof |
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| Publication Number | Publication Date |
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| CN102417867A true CN102417867A (en) | 2012-04-18 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2010105047881A Pending CN102417867A (en) | 2010-09-28 | 2010-09-28 | Soaping agent composition for dyeing fabric and production method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102899195A (en) * | 2012-10-22 | 2013-01-30 | 青岛蔚蓝生物集团有限公司 | Soaping compound enzyme and application method thereof |
| CN102911805A (en) * | 2012-10-25 | 2013-02-06 | 南京大地冷冻食品有限公司 | Method for preparing novel efficient soaping agent for activated dyes |
| CN104562802A (en) * | 2015-01-08 | 2015-04-29 | 广东溢达纺织有限公司 | Method for soaping object dyed with reactive dye to remove flooding |
| CN106118915A (en) * | 2016-07-11 | 2016-11-16 | 山东如意科技集团有限公司 | A kind of soaping agent for highly dense flower pattern cotton textiles figured cloth and technique of soaping thereof |
| CN110699974A (en) * | 2019-09-24 | 2020-01-17 | 杭州卓达染整有限公司 | Acetate fiber and lyocell fiber interwoven fabric and dyeing process thereof |
| CN111748418A (en) * | 2020-07-23 | 2020-10-09 | 石狮市瑞鹰纺织科技有限公司 | Low-temperature cleaning agent and application thereof in washing process after dyeing of polyester knitted fabric |
| CN111793993A (en) * | 2020-07-07 | 2020-10-20 | 山东黄河三角洲纺织科技研究院有限公司 | Anti-printing process of viscose/lyocell/cotton blended fabric |
-
2010
- 2010-09-28 CN CN2010105047881A patent/CN102417867A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102899195A (en) * | 2012-10-22 | 2013-01-30 | 青岛蔚蓝生物集团有限公司 | Soaping compound enzyme and application method thereof |
| CN102899195B (en) * | 2012-10-22 | 2013-08-28 | 青岛蔚蓝生物集团有限公司 | Soaping compound enzyme and application method thereof |
| CN102911805A (en) * | 2012-10-25 | 2013-02-06 | 南京大地冷冻食品有限公司 | Method for preparing novel efficient soaping agent for activated dyes |
| CN104562802A (en) * | 2015-01-08 | 2015-04-29 | 广东溢达纺织有限公司 | Method for soaping object dyed with reactive dye to remove flooding |
| CN106118915A (en) * | 2016-07-11 | 2016-11-16 | 山东如意科技集团有限公司 | A kind of soaping agent for highly dense flower pattern cotton textiles figured cloth and technique of soaping thereof |
| CN106118915B (en) * | 2016-07-11 | 2019-01-22 | 山东如意科技集团有限公司 | A kind of soaping agent and its technique of soaping for highly dense flower pattern pure cotton figured cloth |
| CN110699974A (en) * | 2019-09-24 | 2020-01-17 | 杭州卓达染整有限公司 | Acetate fiber and lyocell fiber interwoven fabric and dyeing process thereof |
| CN111793993A (en) * | 2020-07-07 | 2020-10-20 | 山东黄河三角洲纺织科技研究院有限公司 | Anti-printing process of viscose/lyocell/cotton blended fabric |
| CN111748418A (en) * | 2020-07-23 | 2020-10-09 | 石狮市瑞鹰纺织科技有限公司 | Low-temperature cleaning agent and application thereof in washing process after dyeing of polyester knitted fabric |
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Application publication date: 20120418 |