CN103215829A - Cotton knitted fabric active dye refining and dyeing one-bath method - Google Patents
Cotton knitted fabric active dye refining and dyeing one-bath method Download PDFInfo
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- CN103215829A CN103215829A CN 201210582895 CN201210582895A CN103215829A CN 103215829 A CN103215829 A CN 103215829A CN 201210582895 CN201210582895 CN 201210582895 CN 201210582895 A CN201210582895 A CN 201210582895A CN 103215829 A CN103215829 A CN 103215829A
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Abstract
The invention relates to a cotton knitted fabric active dye refining and dyeing one-bath method. According to the method, a tea saponin compounding agent is adopted as a pretreatment surfactant in the refining and dyeing one-bath method; with the method, contradiction between refining and dyeing is effectively solved, a good color fixation rate is obtained, refining and dyeing one-bath is achieved, and light, medium and dark fabrics can be dyed; the method has characteristics of process shortening, water and energy source consumption reduction, reduction of BOD and COD emission in wastewater, and the like, such that the method is an effective approach for achieving high efficiency, energy saving, and environmental protection cotton fabric production; the method further has characteristics of simple operation and easy production; the process comprises the following two sets of processes: (1) adding tea saponin, a penetrant, a stabilizer, a refining agent, an active dye, a salt and a color fixation substitute alkali, carrying out dyeing and refining, soaping, carrying out water washing, carrying out color fixation, and drying, and (2) adding BuGong tea saponin composite tea saponin, a penetrant, a refining agent and a hydrogen peroxide stabilizer to carry out refining rinsing, removing oxygen, adding an active dye, a salt and a color fixation substitute alkali to dye, soaping, carrying out water washing, carrying out color fixation, and drying.
Description
Technical field the present invention relates to a kind of method of cotton fabrics REACTIVE DYES scouring and dyeing.
Background technology
Cotton meets the subsequent production requirement for indexs such as water imbibition, whiteness, needs pre-treatment, and process comprises destarch, concise, bleaching three process, exists: complicated operation, and operation is loaded down with trivial details; Utilization rate of equipment and installations is low, needs a large amount of caustic soda, hydrogen peroxide and various chemical assistant; A series of problems such as there is very big problem of environmental pollution in discharge of wastewater, and it is huge to consume energy.Present this technology is still generally being used in dyeing and finishing industry.
Along with development of new techniques, Tea Saponin is used on COTTON FABRIC and is accepted by more and more enterprises.Tea Saponin has another name called the tea saponin, is by a class candy glucoside compound that extracts in the tea tree seed, is a kind of natural surfactant of excellent performance.Not highly basic, it or not strong oxidizer, do not contain APEO any harmful chemical elements such as (alkylphenol polyoxyethylene), needn't add caustic soda, hydrogen peroxide again during use, can satisfy every specification requirement of printing and dyeing pre-treatment, effect is very obvious, and can handle cotton, the nearly all lining of blended fibre knitwears.And to fiber not burn into do not damage, can not produce fulling milling.The researcher [Liu Ruining, Liu Yang, Cui Shuling. " the composite tea saponin pre-treatment of COTTON FABRIC " [J]. printing and dyeing, 2011, (5): 9-12] to the composite discovery of Tea Saponin: can effectively better improve the fabric pretreatment level, mainly show whiteness, capillary effect, aspects such as brute force.Composite Tea Saponin can effectively integrate Tea Saponin characteristic and traditional alkali oxygen pre-treatment characteristic.
The reactive dyeing fastness is good, and dyeing is convenient, lovely luster, and numerous advantages such as chromatogram is complete are the topmost dyestuffs of cotton fabrics and yarn dyeing.The use of Tea Saponin makes that the condition of cotton fabrics and yarn pre-treatment is gentle relatively, how to realize dyeing with the pre-treatment single bath process, significantly reduces discharging, saves cost, enhances productivity, become one useful
Technological project.
Summary of the invention
The purpose of this invention is to provide the method that a kind of cotton fabrics pre-treatment is bathed with reactive dyeing one.With the existing composite basis that is applied as of Tea Saponin, optimize experimental program, select the suitable activity dyestuff, the pre-treatment that realizes cotton fabrics and dyeing is with bathing, obtain shallow, in, dark all kinds of textiless.
The purpose of this invention is to provide the method that a kind of cotton fabrics pre-treatment is bathed with reactive dyeing one.With the existing composite basis that is applied as of Tea Saponin, optimize experimental program, select the suitable activity dyestuff, the pre-treatment that realizes cotton fabrics and dyeing is with bathing, obtain shallow, in, dark all kinds of textiless.
The present invention is that the Tea Saponin compounded technology is by in composite pre-treatment of Tea Saponin and composite tea saponin pre-treatment two cover technical schemes, dyes with bathing thereby implement in full short stream refining, reaches energy-saving and emission-reduction, the purpose that increases production and improves productivity.
Technical solution of the present invention: be divided into composite and (foretelling public tea soap) composite tea saponin two covers of Tea Saponin.
The mat woven of fine bamboo strips one cover technical scheme,
(1) main flow process:
Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation substitutes alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(2) scouring and dyeing basic recipe:
Dye dosage (heavy) 0～10% to fabric,
Glauber salt or salt 30～100 g/L,
Fixation substitutes alkali 2.0～4.0 g/L,
Scouring agent YS198 5～7 g/l,
Tea Saponin 40～60 g/L,
REACTIVE DYES stabilizing agent 2～4 g/L,
Bleeding agent 4～6 g/L,
Bath raio 1:15.
(3) dyeing course
Room temperature adds enough water, and the fabric running is made it fully wetting.Add composite Tea Saponin, dyestuff, glauber salt or salt, dye protection agent to practicing dye bath respectively, bleeding agent divides the fabric 10-15 that turns round kind, adds fixation alkali then in batches.Begin heating afterwards, rise to 60 ℃ from room temperature with the speed of 1.5 ℃/min, dye 30 minutes, again with heat up 95 ℃ of white silks 30 minutes of the speed of 2 ℃/min.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Described scouring and dyeing is with composite Tea Saponin pre-treatment and reactive dyeing single bath process.
Described suitable activity dyestuff is various REACTIVE DYES types.
Described scouring and dyeing bath raio 1:5 to 1:50.
Beneficial effect
(1) the present invention effectively solves the contradiction of " practice with dye ", realizes scouring and dyeing, initiative composite dose of Tea Saponin is used for the scouring and dyeing method as the pre-treatment surfactant, do not fall or reduce degree of fixation less, and can dye shallow, in, dark fabric;
(2) the present invention can reduce caustic soda and hydrogen peroxide use amount, has characteristics such as BOD and COD discharging in shortened process, minimizing water and energy resource consumption, the reduction waste water, is to realize effective way efficient, the energy-saving and environmental protection cotton pretreatment.
(3) the present invention is simple to operate, is convenient to produce.
Embodiment 1
Thick moldeed depth look dyeing
(1) main flow process:
Composite Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(2) scouring and dyeing basic recipe:
K type dye consumption (heavy) 8 % to fabric,
Glauber salt 100 g/L,
Fixation substitutes alkali 4.0 g/L,
REACTIVE DYES stabilizing agent 4 g/L,
Scouring agent YS198 6 g/l,
Tea Saponin 70 g/L,
Bleeding agent 6 g/L,
Bath raio 1:15.
(3) dyeing course
Room temperature adds enough water, and the fabric running is made it fully wetting.Add composite Tea Saponin, dyestuff, glauber salt or salt, dye protection agent to practicing dye bath respectively, bleeding agent divides the fabric 10-15 that turns round kind, adds fixation alkali then in batches.Begin heating afterwards, rise to 80 ℃ from room temperature with the speed of 1.5 ℃/min, dye 30 minutes, again with heat up 95 ℃ of white silks 30 minutes of the speed of 2 ℃/min.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Embodiment 2
Look dyeing in slim
(1) main flow process:
Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(2) scouring and dyeing basic recipe:
M type dye consumption (heavy) 4 % to fabric,
Glauber salt 50 g/L,
Fixation substitutes alkali 3 g/L,
Stabilizing agent 4 g/L,
Scouring agent YS198 3 g/l,
Tea Saponin 40 g/L,
Bleeding agent 3 g/L,
Bath raio 1:20.
(3) dyeing course
Room temperature adds enough water, and the fabric running is made it fully wetting.Add Tea Saponin, dyestuff, glauber salt or salt, dye protection agent to practicing dye bath respectively, bleeding agent divides the fabric 10-15 that turns round kind, adds fixation alkali then in batches.Begin heating afterwards, rise to 60 or 80 ℃ from room temperature with the speed of 1.5 ℃/min, dye 30 minutes, again with heat up 95 ℃ of white silks 30 minutes of the speed of 2 ℃/min.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Embodiment 3
Slim light-colored dyeing
(1) main flow process:
Composite Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(2) scouring and dyeing basic recipe:
KN type dye consumption (heavy) 1 % to fabric,
Salt 30 g/L,
Fixation substitutes alkali 2.5 g/L,
Stabilizing agent 3 g/L,
Scouring agent YS198 3 g/l,
Tea Saponin 40 g/L,
Bleeding agent 3 g/L,
Bath raio 1:15.
(3) dyeing course
Room temperature adds enough water, and the fabric running is made it fully wetting.Add composite Tea Saponin, dyestuff, glauber salt or salt, dye protection agent to practicing dye bath respectively, bleeding agent divides the fabric 10-15 that turns round kind, adds fixation alkali then in batches.Begin heating afterwards, rise to 60 or 80 ℃ from room temperature with the speed of 1.5 ℃/min, dye 30 minutes, again with heat up 95 ℃ of white silks 30 minutes of the speed of 2 ℃/min.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
The mat woven of fine bamboo strips two cover technical schemes,
(1) main flow process:
(foretelling public Tea Saponin) composite tea saponin+bleeding agent+scouring agent+hydrogen peroxide stabilizer scourings and bleaching → and deoxidizing, polishing enzyme → REACTIVE DYES+salt+fixation substitutes alkali and dyes → soap → wash → fixation → oven dry.
(2) scouring and dyeing basic recipe:
Composite Tea Saponin 40～60 g/L,
Bleeding agent 4～6 g/L,
Hydrogen peroxide stabilizer 2～4 g/L,
The scouring agent consumption is 4～7g/L,
Deoxidizing, polishing enzyme 2～4 g/L,
Dye dosage (heavy) 0～10% to fabric,
Glauber salt or salt 30～100 g/L,
Fixation substitutes alkali 2.0～4.0 g/L,
Bath raio 1:10～15.
(3) dyeing course
Room temperature, add enough water, fabric and yarn running are made it fully wetting, add respectively and foretell public soap composite tea saponin 40L, penetrating agent JFC 5g/L, scouring agent/hydrogen peroxide stabilizer heats up 95 ℃～100 ℃ and scourings and bleaching, and bath raio 1:12 practiced 30～50 minutes, add 55～60 ℃ of water for cooling; bath raio 1:15, pH value is transferred neutral, adds and adds dyestuff, glauber salt or salt again after the deoxidizing, polishing enzyme is walked 10 minutes; add fixation alkali after walking 15 minutes; 55～60 ℃ of insulations were dyeed 30 minutes, and the speed with 2 ℃/min heats up 80 or 90 ℃ again, is incubated 20～-30 minutes.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Described scouring and dyeing is with composite Tea Saponin pre-treatment and reactive dyeing single bath process.
Described suitable activity dyestuff is various REACTIVE DYES types.
Described scouring and dyeing bath raio 1:5 to 1:50.
Beneficial effect
(4) the present invention effectively solves the contradiction of " practice with dye ", realize scouring and dyeing, initiative composite dose of Tea Saponin is used for the scouring and dyeing method as the pre-treatment surfactant, by the deoxidizing, polishing enzyme, deoxidizing, polishing and dyeing is synchronous, do not fall or reduce degree of fixation less, and can dye shallow, in, dark fabric, the light color of special bright color or bleaching.
(5) the present invention can reduce caustic soda and hydrogen peroxide use amount, has characteristics such as BOD and COD discharging in shortened process, minimizing water and energy resource consumption, the reduction waste water, is to realize effective way efficient, the energy-saving and environmental protection cotton pretreatment.
(6) the present invention is simple to operate, is convenient to produce.
Embodiment 1
Thick moldeed depth look dyeing
(3) main flow process:
Composite Tea Saponin+bleeding agent+stabilizing agent+hydrogen peroxide stabilizer+scouring agent+REACTIVE DYES+salt+fixation alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(4) scouring and dyeing basic recipe:
K type dye consumption (heavy) 8 % to fabric,
Composite Tea Saponin 50 g/L,
Bleeding agent 5 g/L,
Hydrogen peroxide stabilizer 4 g/L,
The scouring agent consumption is 6g/L,
Deoxidizing, polishing enzyme 2 g/L,
Dye dosage (heavy) 0～10% to fabric,
Salt or glauber salt 40～100 g/L,
Fixation substitutes alkali 4.0 g/L,
Bath raio 1:12～15.
(3) dyeing course
Room temperature, add enough water, fabric and yarn running are made it fully wetting, add respectively and foretell public soap composite tea saponin 40L, penetrating agent JFC 5g/L, scouring agent/hydrogen peroxide stabilizer heats up 95 ℃～100 ℃ and scourings and bleaching, and bath raio 1:12 practiced 30～50 minutes, add 55～60 ℃ of water for cooling; bath raio 1:15, pH value is transferred neutral, adds and adds dyestuff, glauber salt or salt again after the deoxidizing, polishing enzyme is walked 10 minutes; add fixation alkali after walking 15 minutes; 55～60 ℃ of insulations were dyeed 30 minutes, and the speed with 2 ℃/min heats up 80 or 90 ℃ again, is incubated 20～-30 minutes.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Embodiment 2
Look dyeing in slim
(3) main flow process:
Composite Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(4) scouring and dyeing basic recipe:
M type dye consumption (heavy) 4 % to fabric,
Composite Tea Saponin 50 g/L,
Bleeding agent 5 g/L,
Hydrogen peroxide stabilizer 4 g/L,
The scouring agent consumption is 6g/L,
Deoxidizing, polishing enzyme 2 g/L,
Salt or glauber salt 50 g/L,
Fixation substitutes alkali 3.0 g/L,
Bath raio 1:12～15.
(3) dyeing course
Room temperature, add enough water, fabric and yarn running are made it fully wetting, add respectively and foretell public soap composite tea saponin 40L, penetrating agent JFC 5g/L, scouring agent/hydrogen peroxide stabilizer heats up 95 ℃～100 ℃ and scourings and bleaching, and bath raio 1:12 practiced 30～50 minutes, add 55～60 ℃ of water for cooling; bath raio 1:15, pH value is transferred neutral, adds and adds dyestuff, glauber salt or salt again after the deoxidizing, polishing enzyme is walked 10 minutes; add fixation alkali after walking 15 minutes; 55～60 ℃ of insulations were dyeed 30 minutes, and the speed with 2 ℃/min heats up 80 or 90 ℃ again, is incubated 20～-30 minutes.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Embodiment 3
Slim light-colored dyeing
(3) main flow process:
Composite Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
(4) scouring and dyeing basic recipe:
KN type dye consumption (heavy) 1 % to fabric,
Composite Tea Saponin 40 g/L,
Bleeding agent 5 g/L,
Hydrogen peroxide stabilizer 4 g/L,
The scouring agent consumption is 6g/L,
Deoxidizing, polishing enzyme 2 g/L,
Salt 30 g/L,
Fixation substitutes alkali 2.0 g/L,
Bath raio 1:12～15.
(3) dyeing course
Room temperature, add enough water, fabric and yarn running are made it fully wetting, add respectively and foretell public soap composite tea saponin 40L, penetrating agent JFC 5g/L, scouring agent/hydrogen peroxide stabilizer heats up 95 ℃～100 ℃ and scourings and bleaching, and bath raio 1:12 practiced 30～50 minutes, add 55～60 ℃ of water for cooling; bath raio 1:15, pH value is transferred neutral, adds and adds dyestuff, glauber salt or salt again after the deoxidizing, polishing enzyme is walked 10 minutes; add fixation alkali after walking 15 minutes; 55～60 ℃ of insulations were dyeed 30 minutes, and the speed with 2 ℃/min heats up 80 or 90 ℃ again, is incubated 20～-30 minutes.
(4) soap boiling prescription and process conditions are as follows:
Detergent: 1 g/L,
Soda ash: 0.5 g/L,
Bath raio 1:20,
Temperature: 90 ℃,
Time: 15 min.
Claims (11)
1. the purpose of this invention is to provide the method that a kind of cotton fabrics pre-treatment is bathed with reactive dyeing one, with the existing composite basis that is applied as of Tea Saponin, with two cover complex process, optimize experimental program, select the suitable activity dyestuff, the pre-treatment of realization cotton fabrics and yarn is bathed together with dyeing, obtains shallow, in, dark all kinds of textiless.
2. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its technological process one: Tea Saponin+bleeding agent+stabilizing agent+scouring agent+REACTIVE DYES+salt+fixation substitutes alkali → dyeing and pre-treatment → soap → wash → fixation → oven dry.
3. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its technological process two: foretell public Tea Saponin composite tea saponin+bleeding agent+scouring agent+hydrogen peroxide stabilizer to scouring and bleaching → deoxygenation → REACTIVE DYES+salt+fixation substitutes alkali and dyes → soap → wash → fixation → oven dry.
4. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its white silk are dyed the mat woven of fine bamboo strips one cover prescription: dye dosage (heavy to fabric or yarn)/glauber salt or salt/fixation substitute alkali/scouring agent YS198/ composite tea saponin/REACTIVE DYES stabilizing agent/bleeding agent.
5. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its white silk are dyed the mat woven of fine bamboo strips two cover prescriptions: foretell public soap composite tea saponin 40L, penetrating agent JFC 5g/L, scouring agent YS1986g/L, hydrogen peroxide stabilizer C-J101 4g/L; With remove oxygenase/dye dosage (heavy)/glauber salt or salt/fixation and substitute alkali fabric or yarn.
6. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1; its white silk dyes the step mat woven of fine bamboo strips one cover: room temperature; add enough water; fabric and yarn running are made it fully wetting; add scouring and dyeing Tea Saponin, dyestuff, glauber salt or salt, dye protection agent respectively; bleeding agent is planted fabric or yarn running 10-15 branch, adds fixation alkali then in batches.
7. begin heating afterwards, rise to 60～80 ℃ from room temperature with the speed of 1.5 ℃/min, dye 30 minutes, again with heat up 95 ℃ of white silks 30 minutes of the speed of 2 ℃/min.
8. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its white silk dyes the step mat woven of fine bamboo strips two covers: room temperature, add enough water, fabric and yarn running are made it fully wetting, add to foretell public soap composite tea saponin 40L respectively, penetrating agent JFC 5g/L, scouring agent/hydrogen peroxide stabilizer heat up 95 ℃～100 ℃ and scouring and bleaching; bath raio 1:12; practiced 30～50 minutes, and added 55～60 ℃ of water for cooling, bath raio 1:15; pH value is transferred neutral; add except that oxygenase and add dyestuff again after walking 10 minutes; glauber salt or salt, add fixation alkali after walking 15 minutes, 55～60 ℃ of insulation dyeing 30 minutes; the speed with 2 ℃/min heats up 80 or 90 ℃ again, is incubated 20～-30 minutes.
9. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its described scouring and dyeing are with composite Tea Saponin pre-treatment and reactive dyeing single bath process.
10. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its described deoxidizing, polishing enzyme, it is synchronous to have a deoxidizing, polishing and dyeing, and can dye shallow, in, dark fabric, the light color of special bright color or bleaching.
11. the method for a kind of cotton fabrics REACTIVE DYES scouring and dyeing according to claim 1, its described suitable activity dyestuff be middle high temperature type and double-active radical because of REACTIVE DYES, comprise K type (chloro-s-triazine), M type, KE type, KE type (double-active group).
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| CN103485198A (en) * | 2013-09-11 | 2014-01-01 | 昆山市万丰制衣有限责任公司 | Active dye-decamethylcyclopentasiloxane suspension system dyeing process of cotton fabric |
| CN104099788A (en) * | 2014-07-04 | 2014-10-15 | 无锡市信达染整机械厂 | Environmental-friendly cotton fabric dyeing |
| CN104179041A (en) * | 2014-08-12 | 2014-12-03 | 际华三五四三针织服饰有限公司 | Dyeing technology for carrying out one-bath scouring and dyeing on lycra-containing cotton knitted fabric by active turquoise blue |
| CN104213398A (en) * | 2014-08-14 | 2014-12-17 | 浙江航民股份有限公司 | Production method for polyester cotton oxygen bleaching and disperse dyestuff dyeing one bath process |
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| CN114207212A (en) * | 2019-08-27 | 2022-03-18 | 布尔萨利纺织工业和贸易公司 | Environment-friendly dyeing process of cellulose product |
| CN114318898A (en) * | 2021-12-25 | 2022-04-12 | 绍兴恒利印染有限公司 | Low-temperature dyeing process for knitted fabric |
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| CN104695213A (en) * | 2013-12-04 | 2015-06-10 | 铜陵市永生机电制造有限责任公司 | Pretreatment method of pineapple fiber |
| CN104099788B (en) * | 2014-07-04 | 2016-01-20 | 无锡市信达染整机械厂 | Eco-friendly cotton fabric dyeing process |
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| CN104179041A (en) * | 2014-08-12 | 2014-12-03 | 际华三五四三针织服饰有限公司 | Dyeing technology for carrying out one-bath scouring and dyeing on lycra-containing cotton knitted fabric by active turquoise blue |
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Application publication date: 20130724 |