CN102417309B - 一种非密堆SiO2光子晶体的制备方法 - Google Patents
一种非密堆SiO2光子晶体的制备方法 Download PDFInfo
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- CN102417309B CN102417309B CN 201110242654 CN201110242654A CN102417309B CN 102417309 B CN102417309 B CN 102417309B CN 201110242654 CN201110242654 CN 201110242654 CN 201110242654 A CN201110242654 A CN 201110242654A CN 102417309 B CN102417309 B CN 102417309B
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- 239000004038 photonic crystal Substances 0.000 title claims abstract description 88
- 238000002360 preparation method Methods 0.000 title claims abstract description 34
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title abstract description 15
- 239000000377 silicon dioxide Substances 0.000 title abstract description 7
- 235000012239 silicon dioxide Nutrition 0.000 title abstract description 7
- 229910052681 coesite Inorganic materials 0.000 title abstract 5
- 229910052906 cristobalite Inorganic materials 0.000 title abstract 5
- 229910052682 stishovite Inorganic materials 0.000 title abstract 5
- 229910052905 tridymite Inorganic materials 0.000 title abstract 5
- 238000005530 etching Methods 0.000 claims abstract description 26
- 239000002245 particle Substances 0.000 claims abstract description 21
- 239000000243 solution Substances 0.000 claims description 119
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 69
- 239000000725 suspension Substances 0.000 claims description 67
- 239000012798 spherical particle Substances 0.000 claims description 54
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 49
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 34
- 239000000758 substrate Substances 0.000 claims description 29
- 239000011521 glass Substances 0.000 claims description 28
- 238000002156 mixing Methods 0.000 claims description 28
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 27
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 26
- 239000002253 acid Substances 0.000 claims description 26
- 239000011324 bead Substances 0.000 claims description 26
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 26
- 239000008367 deionised water Substances 0.000 claims description 26
- 229910021641 deionized water Inorganic materials 0.000 claims description 26
- 239000011259 mixed solution Substances 0.000 claims description 26
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 24
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 24
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 23
- 239000002904 solvent Substances 0.000 claims description 15
- 238000001354 calcination Methods 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 14
- 206010013786 Dry skin Diseases 0.000 claims description 13
- 238000013019 agitation Methods 0.000 claims description 13
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 13
- 238000001035 drying Methods 0.000 claims description 13
- MHAJPDPJQMAIIY-UHFFFAOYSA-N hydrogen peroxide Substances OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 13
- 238000007654 immersion Methods 0.000 claims description 13
- 238000001556 precipitation Methods 0.000 claims description 13
- 238000000926 separation method Methods 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 13
- 238000005406 washing Methods 0.000 claims description 13
- 238000005303 weighing Methods 0.000 claims description 13
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 11
- 229910052710 silicon Inorganic materials 0.000 claims description 11
- 239000010703 silicon Substances 0.000 claims description 11
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 8
- 229960004756 ethanol Drugs 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 5
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 18
- 239000013078 crystal Substances 0.000 description 7
- 238000001338 self-assembly Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000000084 colloidal system Substances 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 239000011022 opal Substances 0.000 description 3
- 230000000737 periodic effect Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 230000010412 perfusion Effects 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000012858 resilient material Substances 0.000 description 1
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CN 201110242654 CN102417309B (zh) | 2011-08-23 | 2011-08-23 | 一种非密堆SiO2光子晶体的制备方法 |
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CN 201110242654 CN102417309B (zh) | 2011-08-23 | 2011-08-23 | 一种非密堆SiO2光子晶体的制备方法 |
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CN102417309A CN102417309A (zh) | 2012-04-18 |
CN102417309B true CN102417309B (zh) | 2013-10-09 |
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103288491B (zh) * | 2013-05-29 | 2014-06-04 | 陕西科技大学 | 一种蓝绿色光子晶体结构色薄膜的制备方法 |
CN103352255B (zh) * | 2013-06-23 | 2016-03-02 | 安泰科技股份有限公司 | 一种具有反蛋白石结构的光子晶体的制备方法 |
CN103880013B (zh) * | 2014-02-19 | 2015-09-30 | 陕西科技大学 | 一种氧化硅-氧化铁异质胶体晶体的制备方法 |
CN103803562B (zh) * | 2014-02-19 | 2015-09-30 | 陕西科技大学 | 一种双尺寸氧化硅胶体晶体的制备方法 |
CN103880016B (zh) * | 2014-02-19 | 2015-11-18 | 陕西科技大学 | 一种SiO2-Fe2O3双尺寸胶体晶体的制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1880519A (zh) * | 2006-04-30 | 2006-12-20 | 陕西科技大学 | 一种图案化二氧化钛反蛋白石光子晶体的制备方法 |
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Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1880519A (zh) * | 2006-04-30 | 2006-12-20 | 陕西科技大学 | 一种图案化二氧化钛反蛋白石光子晶体的制备方法 |
Non-Patent Citations (2)
Title |
---|
"二氧化硅胶体球的制备、改性及其胶体晶体的组装";伍媛婷等;《功能材料与器件学报》;20110630;第17卷(第3期);323-326 * |
伍媛婷等."二氧化硅胶体球的制备、改性及其胶体晶体的组装".《功能材料与器件学报》.2011,第17卷(第3期),323-326. |
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