CN102348637B - 制备金刚石立方纳米晶体的方法 - Google Patents

制备金刚石立方纳米晶体的方法 Download PDF

Info

Publication number
CN102348637B
CN102348637B CN201080011981.XA CN201080011981A CN102348637B CN 102348637 B CN102348637 B CN 102348637B CN 201080011981 A CN201080011981 A CN 201080011981A CN 102348637 B CN102348637 B CN 102348637B
Authority
CN
China
Prior art keywords
diamond
nanocrystals
powder
equal
less
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201080011981.XA
Other languages
English (en)
Chinese (zh)
Other versions
CN102348637A (zh
Inventor
帕特里克·屈尔米
让-保罗·布杜
阿兰·托雷尔
费尔多·热勒佐科
莫汉姆德·塞努尔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Method And Industrial Processing Research And Development Association
Institut National de la Sante et de la Recherche Medicale INSERM
Original Assignee
Method And Industrial Processing Research And Development Association
Institut National de la Sante et de la Recherche Medicale INSERM
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Method And Industrial Processing Research And Development Association, Institut National de la Sante et de la Recherche Medicale INSERM filed Critical Method And Industrial Processing Research And Development Association
Publication of CN102348637A publication Critical patent/CN102348637A/zh
Application granted granted Critical
Publication of CN102348637B publication Critical patent/CN102348637B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/25—Diamond
    • C01B32/26—Preparation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/25—Diamond
    • C01B32/28—After-treatment, e.g. purification, irradiation, separation or recovery
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/30—Active carbon
    • C01B32/354—After-treatment
    • C01B32/384—Granulation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/48—Biological material, e.g. blood, urine; Haemocytometers
    • G01N33/50—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing
    • G01N33/58—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing involving labelled substances
    • G01N33/582—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing involving labelled substances with fluorescent label
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/70—Nanostructure
    • Y10S977/773—Nanoparticle, i.e. structure having three dimensions of 100 nm or less
    • Y10S977/775—Nanosized powder or flake, e.g. nanosized catalyst
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
    • Y10T428/2991—Coated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T436/00—Chemistry: analytical and immunological testing
    • Y10T436/14—Heterocyclic carbon compound [i.e., O, S, N, Se, Te, as only ring hetero atom]
    • Y10T436/142222—Hetero-O [e.g., ascorbic acid, etc.]
    • Y10T436/143333—Saccharide [e.g., DNA, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Materials Engineering (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Hematology (AREA)
  • Urology & Nephrology (AREA)
  • Molecular Biology (AREA)
  • Biomedical Technology (AREA)
  • Immunology (AREA)
  • Composite Materials (AREA)
  • Manufacturing & Machinery (AREA)
  • Medicinal Chemistry (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • Food Science & Technology (AREA)
  • Cell Biology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
CN201080011981.XA 2009-03-09 2010-03-08 制备金刚石立方纳米晶体的方法 Expired - Fee Related CN102348637B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09305216.5 2009-03-09
EP09305216 2009-03-09
PCT/EP2010/052910 WO2010102977A1 (en) 2009-03-09 2010-03-08 Method for manufacturing cubic diamond nanocrystals

Publications (2)

Publication Number Publication Date
CN102348637A CN102348637A (zh) 2012-02-08
CN102348637B true CN102348637B (zh) 2015-01-28

Family

ID=41171110

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080011981.XA Expired - Fee Related CN102348637B (zh) 2009-03-09 2010-03-08 制备金刚石立方纳米晶体的方法

Country Status (7)

Country Link
US (2) US8932553B2 (https=)
EP (1) EP2406179A1 (https=)
JP (1) JP5676494B2 (https=)
KR (1) KR101754270B1 (https=)
CN (1) CN102348637B (https=)
RU (1) RU2547009C2 (https=)
WO (1) WO2010102977A1 (https=)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10258959B2 (en) 2010-08-11 2019-04-16 Unit Cell Diamond Llc Methods of producing heterodiamond and apparatus therefor
CN102583361B (zh) * 2012-02-23 2013-10-02 燕山大学 振动球磨膨胀石墨制备纳米金刚石的方法
US8940267B2 (en) * 2012-06-28 2015-01-27 The Arizona Board Of Regents On Behalf Of The University Of Arizona Method of purifying nanodiamond powder and purified nanodiamond powder
CN109765257A (zh) 2012-08-22 2019-05-17 哈佛学院院长及董事 纳米级扫描传感器
US10364389B1 (en) * 2013-09-12 2019-07-30 Adámas Nanotechnologies, lnc. Fluorescent diamond particles
TWI514825B (zh) * 2013-09-23 2015-12-21 Promise Tecnnology Inc 具有內部儲存區域網路交換模組之資料儲存單元以及包含該資料儲存單元之備援式資料儲存系統
KR102301536B1 (ko) 2015-03-10 2021-09-14 삼성전자주식회사 고해상도 전자 현미경 이미지로부터 결정을 분석하는 방법 및 그 시스템
JP6416048B2 (ja) * 2015-07-01 2018-10-31 株式会社神戸製鋼所 グラファイト群、該グラファイト群を含む炭素粒子
CN105384160B (zh) * 2015-09-25 2017-11-03 郑州华晶金刚石股份有限公司 一种纳米碳晶
CN105384168A (zh) * 2015-09-25 2016-03-09 郑州华晶金刚石股份有限公司 一种新型纳米金刚石制备工艺
GB201522512D0 (en) * 2015-12-21 2016-02-03 Element Six Ltd Flourescent diamond particles and methods of fabricating the same
JP6497784B2 (ja) * 2016-05-24 2019-04-10 株式会社リガク 結晶相同定方法、結晶相同定装置、及びｘ線回折測定システム
US9978401B1 (en) 2016-08-19 2018-05-22 Seagate Technology Llc Chirped current profile with undershoot feature
JP6775777B2 (ja) * 2017-08-29 2020-10-28 株式会社リガク Ｘ線回折測定における測定結果の表示方法
CN107802379A (zh) * 2017-11-10 2018-03-16 中科钢研节能科技有限公司 人工关节用的金刚石复合片、人工关节和人工关节组件
RU2680512C1 (ru) * 2017-11-21 2019-02-21 Федеральное государственное бюджетное учреждение науки Институт физики высоких давлений им. Л.Ф. Верещагина Российской академии наук (ИФВД РАН) Способ получения наноразмерных алмазов
CN109384222B (zh) * 2018-09-29 2020-08-07 河南省力量钻石股份有限公司 一种金刚石的提取方法
KR102806657B1 (ko) * 2019-03-26 2025-05-14 주식회사 다이셀 이원자 도프 나노다이아몬드
CN116457308B (zh) * 2020-11-05 2024-11-29 港大科桥有限公司 用于纳米金刚石的高效纯化方法
JP2023091834A (ja) * 2021-12-21 2023-07-03 国立研究開発法人物質・材料研究機構 ダイヤモンド粒子、および、その製造方法
CN114853006A (zh) * 2022-06-24 2022-08-05 河南省豫星碳材有限公司 一种纳米级金刚石超细微粉的生产方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4828582A (en) * 1983-08-29 1989-05-09 General Electric Company Polycrystalline abrasive grit
RU2051092C1 (ru) * 1991-12-25 1995-12-27 Научно-производственное объединение "Алтай" Алмазсодержащее вещество и способ его получения
JP4245310B2 (ja) * 2001-08-30 2009-03-25 忠正 藤村 分散安定性に優れたダイヤモンド懸濁水性液、このダイヤモンドを含む金属膜及びその製造物
US7140567B1 (en) * 2003-03-11 2006-11-28 Primet Precision Materials, Inc. Multi-carbide material manufacture and use as grinding media
JP2005131711A (ja) * 2003-10-28 2005-05-26 Nihon Micro Coating Co Ltd ダイヤモンド研磨粒子及びその製造方法
US7217386B2 (en) * 2004-08-02 2007-05-15 The Regents Of The University Of California Preparation of nanocomposites of alumina and titania
JP4874751B2 (ja) * 2006-09-27 2012-02-15 株式会社イオンテクノセンター Ｍｒ画像法に利用する生体標識用ナノダイヤモンド
JP5010945B2 (ja) * 2007-03-01 2012-08-29 ビジョン開発株式会社 ナノダイヤモンド−貴金属複合薄膜層、これを含む複合金属材料及び燃料電池
EP1990313A1 (en) 2007-05-10 2008-11-12 INSERM (Institut National de la Santé et de la Recherche Médicale) Method to produce light-emitting nano-particles of diamond
WO2009094481A2 (en) * 2008-01-25 2009-07-30 The Regents Of The University Of California Nanodiamonds and diamond-like particles from carbonaceous material
US20090203789A1 (en) * 2008-01-31 2009-08-13 Multi Formulations Ltd. Fast Dissolution Amino Acid Composition
US8927101B2 (en) * 2008-09-16 2015-01-06 Diamond Innovations, Inc Abrasive particles having a unique morphology
US8348409B2 (en) * 2008-11-17 2013-01-08 Xerox Corporation Ink jet inks containing nanodiamond black colorants
US20100272627A1 (en) * 2009-04-23 2010-10-28 Chien-Min Sung Multi-Faceted Diamond and Associated Methods
US10273598B2 (en) * 2009-12-22 2019-04-30 Element Six Technologies Limited Synthetic CVD diamond

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Synthesis and luminescence of nanodiamonds from carbon black;Shengliang Hu et al.;《Materials Science and Engineering: B》;20090215;第157卷(第1-3期);11–14 *

Also Published As

Publication number Publication date
EP2406179A1 (en) 2012-01-18
JP2012519647A (ja) 2012-08-30
JP5676494B2 (ja) 2015-02-25
KR20110137344A (ko) 2011-12-22
US8932553B2 (en) 2015-01-13
US20120022231A1 (en) 2012-01-26
KR101754270B1 (ko) 2017-07-06
US20150104804A1 (en) 2015-04-16
WO2010102977A1 (en) 2010-09-16
RU2547009C2 (ru) 2015-04-10
RU2011140941A (ru) 2013-05-20
CN102348637A (zh) 2012-02-08

Similar Documents

Publication Publication Date Title
CN102348637B (zh) 制备金刚石立方纳米晶体的方法
Boudou et al. High yield fabrication of fluorescent nanodiamonds
Shrestha et al. Fullerene nanoarchitectonics: from zero to higher dimensions
US20110285992A1 (en) Methods of fabricating surface enhanced raman scattering substrates
CN107001049B (zh) 爆轰纳米金刚石的分离方法
Lu et al. High-yield synthesis of silicon carbide nanowires by solar and lamp ablation
Jiang et al. Poly (vinyl pyrrolidone)-capped five-fold twinned gold particles with sizes from nanometres to micrometres
Shen et al. Sub-4 nm nanodiamonds from graphene-oxide and nitrated polycyclic aromatic hydrocarbons at 423 K
Hasaneen et al. Characterization of carbon nanotubes loaded with nitrogen, phosphorus and potassium fertilizers
Terranova et al. Self-assembly of N-diamond nanocrystals into supercrystals
Girard et al. Tuning surface properties of detonation and milled nanodiamonds by gas phase modifications
Rahman et al. An expanded plasma jet assisted technique for very high-rate synthesis of 2D α-MoO3 nanomaterials, with surface oxygen vacancies and robust induced ferromagnetism
Shen et al. A simple route for the synthesis of coral-like accretion of hollow carbon microspheres with thin walls
Mayoral et al. Gold clusters showing pentagonal atomic arrays revealed by aberration-corrected scanning transmission electron microscopy
Sedov et al. Diamond deposition on non-diamond microparticles: Toward the development of core-shell optical materials
Ismatov et al. ANNEALING-INDUCED MORPHOLOGICAL EVOLUTION OF IRON NANOCATALYSTS FOR CARBON NANOTUBE GROWTH
Astuti et al. Evaporation and alignment of 1-undecene functionalised nanodiamonds
Shah et al. Zinc oxide nanoparticles prepared by the reaction of zinc metal with ethanol
Cabioc'h et al. Electron microscopy study of carbon onions synthesized by ion implantation
Boudou et al. High yield fabrication of fluorescent
Sharma Green Synthesis Approaches for Lanthanum Nanorods and Their Physicochemical Characterization
UA92556C2 (uk) Спосіб одержання наночастинок системи метал-кисень із заданим складом електронно-променевим випаровуванням і конденсацією у вакуумі
Dimovski Structure, characterization and exploration of synthesis of conical and polyhedral crystals of graphite
Chen Electron microscopy of some inorganic crystals with novel morphologies
Anjum et al. Cryo-transmission electron microscopy of Ag nanoparticles grown on an ionic liquid substrate

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150128

Termination date: 20190308