CN102256923B - 制备羧酸酯的方法 - Google Patents

制备羧酸酯的方法 Download PDF

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Publication number
CN102256923B
CN102256923B CN2009801506516A CN200980150651A CN102256923B CN 102256923 B CN102256923 B CN 102256923B CN 2009801506516 A CN2009801506516 A CN 2009801506516A CN 200980150651 A CN200980150651 A CN 200980150651A CN 102256923 B CN102256923 B CN 102256923B
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organic phase
alcohol
reaction system
acid
recycled
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CN102256923A (zh
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W·迪斯特多尔夫
J·彼得斯
T·沙福尔
K·弗里泽
C·于布勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
CN2009801506516A 2008-12-16 2009-12-15 制备羧酸酯的方法 Expired - Fee Related CN102256923B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP08171796.9 2008-12-16
EP08171796 2008-12-16
PCT/EP2009/067177 WO2010076192A1 (de) 2008-12-16 2009-12-15 Verfahren zur herstellung von carbonsäureestern

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CN102256923A CN102256923A (zh) 2011-11-23
CN102256923B true CN102256923B (zh) 2013-12-04

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CN2009801506516A Expired - Fee Related CN102256923B (zh) 2008-12-16 2009-12-15 制备羧酸酯的方法

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US (2) US8901343B2 (https=)
EP (1) EP2379481B1 (https=)
JP (1) JP5780967B2 (https=)
KR (1) KR101757936B1 (https=)
CN (1) CN102256923B (https=)
CA (1) CA2746599A1 (https=)
ES (1) ES2554518T3 (https=)
MY (1) MY158588A (https=)
WO (1) WO2010076192A1 (https=)

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CN107074720B (zh) 2014-09-24 2021-01-08 巴斯夫欧洲公司 以反应混合物的循环制备对苯二甲酸二酯的方法
KR102138788B1 (ko) 2017-09-07 2020-07-28 주식회사 엘지화학 에스터 조성물의 제조 시스템 및 이를 이용한 에스터 조성물의 제조 방법
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US12428364B2 (en) 2019-02-25 2025-09-30 Basf Se Method for processing benzene polycarboxylic acid esters and use of same to produce cyclohexane polycarboxylic acid esters
US11512166B2 (en) 2019-04-04 2022-11-29 Lg Chem, Ltd. Method and system for manufacturing ester-based composition
KR102162202B1 (ko) * 2019-04-04 2020-10-06 주식회사 엘지화학 에스터계 조성물의 제조 시스템 및 방법
JP7342320B2 (ja) * 2019-04-04 2023-09-12 エルジー・ケム・リミテッド エステル系組成物の製造方法及び製造システム
CN112955427B (zh) * 2019-04-04 2024-04-19 株式会社Lg化学 用于连续纯化酯化反应产物的系统
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KR102489174B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 방법
KR102488351B1 (ko) * 2019-07-04 2023-01-13 주식회사 엘지화학 디에스터계 물질의 연속식 제조방법
KR102489173B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 열교환 시스템 및 이를 포함하는 디에스터계 조성물 제조 시스템
KR102489171B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
KR102489172B1 (ko) * 2019-07-04 2023-01-18 주식회사 엘지화학 디에스터계 물질의 제조 유닛 및 이를 포함하는 디에스터계 물질의 제조 시스템
CN112239405B (zh) * 2019-07-17 2023-05-02 中国石油化工股份有限公司 2,6-萘二甲酸二甲酯的合成方法
KR102595882B1 (ko) 2019-09-25 2023-10-30 주식회사 엘지화학 디에스터계 조성물의 제조 시스템 및 제조방법
KR102501597B1 (ko) 2019-09-25 2023-02-20 주식회사 엘지화학 디에스테르계 조성물의 제조 시스템 및 제조방법
KR102819374B1 (ko) * 2020-08-13 2025-06-11 주식회사 엘지화학 에스터의 제조방법
JP2023534443A (ja) * 2020-09-24 2023-08-09 エルジー・ケム・リミテッド エステル系組成物の製造方法
EP4219441A4 (en) * 2020-09-24 2024-04-24 Lg Chem, Ltd. METHOD FOR PREPARING AN ESTER-BASED COMPOSITION
EP4219442B1 (en) * 2020-09-24 2025-06-04 Lg Chem, Ltd. Method for producing ester-based composition
EP4219440A4 (en) * 2020-09-24 2024-04-10 Lg Chem, Ltd. DISCONTINUOUS PREPARATION PROCESS FOR ESTER-BASED MATERIAL
KR102797136B1 (ko) * 2020-11-17 2025-04-18 주식회사 엘지화학 디에스터계 화합물의 제조방법
KR102797134B1 (ko) 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 화합물의 제조방법
KR102915059B1 (ko) * 2020-11-17 2026-01-19 주식회사 엘지화학 디에스터계 물질의 제조방법
KR102797150B1 (ko) * 2020-11-17 2025-04-21 주식회사 엘지화학 디에스터계 물질의 제조방법
CN112439216A (zh) * 2020-12-14 2021-03-05 河南久圣化工有限公司 一种从己二酸废液中回收二元羧酸的三级蒸发系统
EP4095123A1 (de) * 2021-05-28 2022-11-30 Evonik Operations GmbH Verfahren zum ausschleusen der leichtsieder bei der herstellung von dialkylterephthalaten oder dialkylphthalaten
KR102865300B1 (ko) * 2022-10-04 2025-09-26 한화솔루션 주식회사 에스테르계 조성물의 제조 방법
CN119657021A (zh) * 2024-12-18 2025-03-21 中国石油化工股份有限公司 一种撬装式邻苯二甲酸二异壬酯合成装置及合成方法

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CN1355780A (zh) * 1999-06-17 2002-06-26 联合碳化化学及塑料技术公司 进行平衡限制反应的方法
CN1400963A (zh) * 2000-02-17 2003-03-05 巴斯福股份公司 制备α,β－不饱和羧酸酯的方法
US20040192957A1 (en) * 2003-03-31 2004-09-30 Wickens Danita Inez Method of recovering 2-ethylhexyl alcohol from a mixture comprising 2-ethylhexyl acrylate

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CN1400963A (zh) * 2000-02-17 2003-03-05 巴斯福股份公司 制备α,β－不饱和羧酸酯的方法
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US20040192957A1 (en) * 2003-03-31 2004-09-30 Wickens Danita Inez Method of recovering 2-ethylhexyl alcohol from a mixture comprising 2-ethylhexyl acrylate

Also Published As

Publication number Publication date
EP2379481B1 (de) 2015-08-26
CN102256923A (zh) 2011-11-23
JP2012512229A (ja) 2012-05-31
MY158588A (en) 2016-10-31
JP5780967B2 (ja) 2015-09-16
KR20110101205A (ko) 2011-09-15
US20150141691A1 (en) 2015-05-21
US8901343B2 (en) 2014-12-02
KR101757936B1 (ko) 2017-07-13
CA2746599A1 (en) 2010-07-08
ES2554518T3 (es) 2015-12-21
US20110251420A1 (en) 2011-10-13
EP2379481A1 (de) 2011-10-26
WO2010076192A1 (de) 2010-07-08
US9260373B2 (en) 2016-02-16

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