CN102246830B - Prawn ecological water quality modifier - Google Patents

Prawn ecological water quality modifier Download PDF

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Publication number
CN102246830B
CN102246830B CN 201110086004 CN201110086004A CN102246830B CN 102246830 B CN102246830 B CN 102246830B CN 201110086004 CN201110086004 CN 201110086004 CN 201110086004 A CN201110086004 A CN 201110086004A CN 102246830 B CN102246830 B CN 102246830B
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China
Prior art keywords
weight portion
oyster shell
shell powder
prawn
water quality
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Expired - Fee Related
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CN 201110086004
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Chinese (zh)
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CN102246830A (en
Inventor
陈景河
何大旭
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Beihai Fulin Green Biological Fertilizer Co Ltd
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Individual
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Priority to CN 201110086004 priority Critical patent/CN102246830B/en
Publication of CN102246830A publication Critical patent/CN102246830A/en
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Publication of CN102246830B publication Critical patent/CN102246830B/en
Expired - Fee Related legal-status Critical Current
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  • Medicines Containing Plant Substances (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention discloses a prawn ecological water quality modifier which is characterized in that: prawn ecological water quality modifier is prepared by taking the activated shuck powder as a carrier and the high-activity secondary metabolism product medicine extracted from the fermentation liquid of Chinese herbal medicine as active ingredient. The prawn ecological water quality modifier disclosed by the invention has the advantages of simple preparation method, low cost and strong disease resistance, maintains stability of the ecological environment of prawn pond, and avoids pollution.

Description

A kind of prawn ecological water quality improving agent
Technical field
The invention belongs to aquaculture field, particularly the technology of a kind of prawn ecological water quality improving agent Formula Design and preparation.
Background technology
Supporting the shrimp people all knows, when prawn enters artificial concentrating the breed stage, because prawn grows fast, prawn density continues to increase, and the water quality of breed is more and more worsened, and causes the prawn quality to descend, disease is frequently broken out, disease is on the rise, even mortality, so seriously influences the development of shrimp farming.Its water quality of prawn culturing and disease management at present, still a difficult problem.China especially Chinese herbal medicine resource in Guangxi is very abundant, and Chinese herbal medicine is that China's veterinary preciousness of tradition is sent product, utilizes the disease of herbal control aquatic animal that long history is also arranged.Develop a kind of nuisanceless green ecotype, can improve the modifying agent of prawn resistance against diseases again to the improving effect of prawn culturing water quality, be significant.
Summary of the invention
The purpose of this invention is to provide a kind of prawn ecological water quality improving agent, influence the shortcoming of shrimp farming development owing to water quality deterioration to overcome present prawn culturing.
In order to realize above-mentioned purpose, technical scheme of the present invention is: be that the high activity secondary metabolite medicine effective ingredient that carrier and Chinese herbal medicine fermented liquid extract is prepared from the activation oyster shell powder;
A. activate the preparation method of oyster shell powder carrier: earlier oyster shell alkali bubble, washing, air-dry back are pulverized, according to application target and requirement, after process 100-200 mesh sieve is sieved and washed, activation is 5-10 hour under 100-200 ℃ of temperature, oyster shell powder after the activation, select the auxiliary agent sodium sulfonate to mix, oyster shell powder is carried out the hole modified 10 hours;
B. Chinese herb medicine prescription:
Sweet wormwood 10% weight portion isatis root 10% weight portion rheum officinale 5% weight portion
Herba houttuyniae 15% weight portion Radix Glycyrrhizae 10% weight portion kitchen garden 10% weight portion
Coptis root 5% weight portion China tree 10% weight portion mother chrysanthemum 5% weight portion
Folium isatidis 15% weight portion castor-oil plant 5% weight portion;
C. Chinese herb medicine effective ingredient extracting method:
Earlier Chinese herb medicine is pulverized, after the screening of 50-100 mesh sieve, add Trichoderma viride, saccharomycete and lactic acid bacteria beneficial microbe colony ferment, fermentation temperature control is at 25-40 ℃, after 24-48 hour, obtain Chinese herbal medicine high activity secondary metabolite medicine effective ingredient, again with above-mentioned Chinese herbal medicine effective ingredient, stirred 2-3 hour with the boiled water backflow, through concentrating, alcohol precipitation, after filtration and the drying, place in the 50-60 ℃ of saturated limewash, the extraction that stirs is waited for after 50 minutes, evenly making its pH value with the hydrochloric acid accent again is 5, when temperature was down to 30 ℃, making pH value through washing was 6.5 o'clock, obtains flavones after the oven dry, alkaloid, the active substance of polysaccharide and saponin class; The active substance of flavones, alkaloid, polysaccharide and the saponin class that Chinese herbal medicine is extracted with a certain amount of methyl alcohol dissolving after, add an amount of water, add 70% activation oyster shell powder again, be heated to 50-60 ℃ of stirring 3-4 hour again, it fully mixed and adsorb; Add 10% calper calcium peroxide at last and 10% carboxymethyl cellulose fully mixes.
Adopt the present invention of above-mentioned measure to have that method is simple, cost is low, keep the advantage that shrimp pool ecotope is stable, pollution-free, resistance against diseases is strong.
Embodiment
Prawn ecological water quality improving agent of the present invention, embodiment: be that the high activity secondary metabolite medicine effective ingredient that carrier and Chinese herbal medicine fermented liquid extract is prepared from the activation oyster shell powder;
A. activate the preparation method of oyster shell powder carrier: earlier oyster shell alkali bubble, washing, air-dry back are pulverized, according to application target and requirement, after process 100-200 mesh sieve is sieved and washed, activation is 5-10 hour under 100-200 ℃ of temperature, oyster shell powder after the activation, select the auxiliary agent sodium sulfonate to mix, oyster shell powder is carried out the hole modified 10 hours;
B. Chinese herb medicine prescription:
Sweet wormwood 10% weight portion isatis root 10% weight portion rheum officinale 5% weight portion
Herba houttuyniae 15% weight portion Radix Glycyrrhizae 10% weight portion kitchen garden 10% weight portion
Coptis root 5% weight portion China tree 10% weight portion mother chrysanthemum 5% weight portion
Folium isatidis 15% weight portion castor-oil plant 5% weight portion;
C. Chinese herb medicine effective ingredient extracting method:
Earlier Chinese herb medicine is pulverized, after the screening of 50-100 mesh sieve, add Trichoderma viride, saccharomycete and lactic acid bacteria beneficial microbe colony ferment, fermentation temperature control is at 25-40 ℃, after 24-48 hour, obtain Chinese herbal medicine high activity secondary metabolite medicine effective ingredient, again with above-mentioned Chinese herbal medicine effective ingredient, stirred 2-3 hour with the boiled water backflow, through concentrating, alcohol precipitation, after filtration and the drying, place in the 50-60 ℃ of saturated limewash, the extraction that stirs is waited for after 50 minutes, evenly making its pH value with the hydrochloric acid accent again is 5, when temperature was down to 30 ℃, making pH value through washing was 6.5 o'clock, obtains flavones after the oven dry, alkaloid, the active substance of polysaccharide and saponin class; The active substance of flavones, alkaloid, polysaccharide and the saponin class that Chinese herbal medicine is extracted with a certain amount of methyl alcohol dissolving after, add an amount of water, add 70% activation oyster shell powder again, be heated to 50-60 ℃ of stirring 3-4 hour again, it fully mixed and adsorb; Add 10% calper calcium peroxide at last and 10% carboxymethyl cellulose fully mixes.

Claims (1)

1. prawn ecological water quality improving agent is characterized in that: be that the high activity secondary metabolite medicine effective ingredient that carrier and Chinese herbal medicine fermented liquid extract is prepared from the activation oyster shell powder;
A. activate the preparation method of oyster shell powder carrier: earlier oyster shell alkali bubble, washing, air-dry back are pulverized, according to application target and requirement, after process 100-200 mesh sieve is sieved and washed, activation is 5-10 hour under 100-200 ℃ of temperature, oyster shell powder after the activation, select the auxiliary agent sodium sulfonate to mix, oyster shell powder is carried out the hole modified 10 hours;
B. Chinese herb medicine prescription:
Sweet wormwood 10% weight portion isatis root 10% weight portion rheum officinale 5% weight portion
Herba houttuyniae 15% weight portion Radix Glycyrrhizae 10% weight portion kitchen garden 10% weight portion
Coptis root 5% weight portion China tree 10% weight portion mother chrysanthemum 5% weight portion
Folium isatidis 15% weight portion castor-oil plant 5% weight portion;
C. Chinese herb medicine effective ingredient extracting method:
Earlier Chinese herb medicine is pulverized, after the screening of 50-100 mesh sieve, add Trichoderma viride, saccharomycete and lactic acid bacteria beneficial microbe colony ferment, fermentation temperature control is at 25-40 ℃, after 24-48 hour, obtain Chinese herbal medicine high activity secondary metabolite medicine effective ingredient, again with above-mentioned Chinese herbal medicine effective ingredient, stirred 2-3 hour with the boiled water backflow, through concentrating, alcohol precipitation, after filtration and the drying, place in the 50-60 ℃ of saturated limewash, the extraction that stirs is waited for after 50 minutes, evenly making its pH value with the hydrochloric acid accent again is 5, when temperature was down to 30 ℃, making the pH value through washing was 6.5 o'clock, obtains flavones after the oven dry, alkaloid, the active substance of polysaccharide and saponin class; The active substance of flavones, alkaloid, polysaccharide and the saponin class that Chinese herbal medicine is extracted with a certain amount of methyl alcohol dissolving after, add an amount of water, add 70% activation oyster shell powder again, be heated to 50-60 ℃ of stirring 3-4 hour again, it fully mixed and adsorb; Add 10% calper calcium peroxide at last and 10% carboxymethyl cellulose fully mixes.
CN 201110086004 2011-03-28 2011-03-28 Prawn ecological water quality modifier Expired - Fee Related CN102246830B (en)

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CN102246830B true CN102246830B (en) 2013-08-14

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103156096B (en) * 2013-04-02 2014-06-04 陈景河 Pigeon feed additive
CN105347408A (en) * 2015-10-29 2016-02-24 鲁宝典 Fishpond water cleaning agent
CN106615694A (en) * 2016-12-16 2017-05-10 田德远 Water quality improver for aquaculture and preparation method thereof
CN106581485A (en) * 2016-12-16 2017-04-26 田德远 Water quality modifier and preparation method thereof
CN106922750A (en) * 2017-02-17 2017-07-07 浙江万里学院 A kind of fermentation of Chinese herbal medicine improver of water quality for improving mud blood clam seed rearing and its preparation application method
CN107226533A (en) * 2017-07-04 2017-10-03 合肥仙之峰农业科技有限公司 It is a kind of to be used to support improver of water quality of shrimp and preparation method thereof
CN109292833A (en) * 2017-11-10 2019-02-01 天津地天科技发展有限公司 A kind of green agriculture antitoxin improver of water quality of book on Chinese herbal medicine used for aquiculture
CN108423774B (en) * 2018-04-10 2021-03-16 上海海洋大学 Dual-function agent for removing snails and purifying water and application thereof

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Publication number Priority date Publication date Assignee Title
CN1088833A (en) * 1993-10-15 1994-07-06 杨玉忠 Prawn high-efficiency sterilizing and disinfecting agent and preparation process thereof
CN1704362A (en) * 2004-05-25 2005-12-07 上海泓宝绿色水产科技发展有限公司 Preparation of probiotics bacterium and method for rehabilitation of aquaculture environment
CN1907872A (en) * 2005-08-05 2007-02-07 陕西宏扬镇海生物防护有限公司 Water quality modifying agent
CN101664116A (en) * 2008-09-04 2010-03-10 李活 Method for preparing multifunctional shrimp feed additive by using oyster shell powder and gracilaria powder as carriers
CN101715742A (en) * 2009-11-16 2010-06-02 大连金砣水产食品有限公司 Holothurian cultivation pond water quality modifier and preparation method thereof

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JP5135637B2 (en) * 2005-04-04 2013-02-06 広嗣 横沢 Water quality improving material comprising porous material laminate, and water quality improving method using the same

Patent Citations (5)

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Publication number Priority date Publication date Assignee Title
CN1088833A (en) * 1993-10-15 1994-07-06 杨玉忠 Prawn high-efficiency sterilizing and disinfecting agent and preparation process thereof
CN1704362A (en) * 2004-05-25 2005-12-07 上海泓宝绿色水产科技发展有限公司 Preparation of probiotics bacterium and method for rehabilitation of aquaculture environment
CN1907872A (en) * 2005-08-05 2007-02-07 陕西宏扬镇海生物防护有限公司 Water quality modifying agent
CN101664116A (en) * 2008-09-04 2010-03-10 李活 Method for preparing multifunctional shrimp feed additive by using oyster shell powder and gracilaria powder as carriers
CN101715742A (en) * 2009-11-16 2010-06-02 大连金砣水产食品有限公司 Holothurian cultivation pond water quality modifier and preparation method thereof

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于明超 等.饲料中添加芽孢杆菌和中草药制剂对凡纳滨对虾生长及肠道菌群的影响.《热带海洋学报》.2010,第29卷(第4期),132-137.
温周瑞 等.中草药对水产动物免疫作用研究进展.《水利渔业》.2004,第24卷(第2期),1-3.
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Application publication date: 20111123

Assignee: Beihai Fulin green biological fertilizer Co., Ltd.

Assignor: Chen Jinghe

Contract record no.: 2014450000001

Denomination of invention: Prawn ecological water quality modifier

Granted publication date: 20130814

License type: Exclusive License

Record date: 20140120

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TR01 Transfer of patent right

Effective date of registration: 20170509

Address after: 536100 Hepu County Industrial Park, the Guangxi Zhuang Autonomous Region, Beihai

Patentee after: Beihai Fulin green biological fertilizer Co., Ltd.

Address before: 536000, the Guangxi Zhuang Autonomous Region Beihai Evergreen Road East No. 52 Forestry Bureau flint company

Patentee before: Chen Jinghe

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130814

Termination date: 20210328