CN102239933B - Family balance formula oil and preparation method thereof - Google Patents
Family balance formula oil and preparation method thereof Download PDFInfo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000003921 oil Substances 0.000 claims abstract description 163
- 235000019198 oils Nutrition 0.000 claims abstract description 163
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- 239000008170 walnut oil Substances 0.000 claims abstract description 54
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- 239000002994 raw material Substances 0.000 claims abstract description 24
- 235000021281 monounsaturated fatty acids Nutrition 0.000 claims abstract description 8
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- 125000001931 aliphatic group Chemical group 0.000 claims description 85
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 54
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Abstract
The invention belongs to the field of edible oil, particularly relates to nutritive formula oil which is suitable for families in China, and has good stability and functions of promoting growth and development and assisting the blood fat reduction, and a preparation method thereof. The family balance formula oil provided by the invention is characterized by comprising the following raw materials in percentage by mass: 34.96-50% of oil tea camellia seed oil rich in monounsaturated fatty acid, 20-40% of corn oil rich in n-6 fatty acid, 5-10% of grape seed oil rich in n-6 fatty acid, 15-30% of linseed oil rich in n-6 fatty acid, 5-10% of walnut oil rich in n-6 fatty acid and 0.04-0.2% of mixed tocopheryl. The family balance formula oil has good cooking stability, and has the functions of promoting growth and development and assisting the blood fat reduction.
Description
Technical field
The invention belongs to the edible oil and fat fields, relate in particular to a kind of suitable China eating at home the culinary art good stability, have nutrient formulation oil of enhancing development effect and auxiliary antilipemic effect and preparation method thereof.
Background technology
Edible oil and fat more and more come into one's own on the impact of residents ' health, grease absorption structure and intake are unreasonable will cause various modern civilization disease, at present China resident edible oil consumption figure urban and rural residents are respectively 44g and 40.7g, the ground such as Beijing, Shanghai has reached 83-85g, the 25g-30g/ days standards of recommending in the resident's dietary guidelines higher than Chinese Soclety of Nutrition's formulation in 2007 far away; The variation of grease consumption structure is embodied in the animal fat intake rises rapidly, rural area animal fat intake with 10 years before compare and risen 82.7%, palm oil year consumption figure also reached nearly 6,000,000 tons, cause the saturated fatty acid intake too high; The characteristics of modern oil-producing technique also cause a large amount of nutritional labeling losses in grease simultaneously.Under this background, according to the intake standard that NI is recommended, the nutrient formulation oil of the suitable China resident eating at home of development has the meaning of particular importance.
family's balance formula oil should have concurrently and satisfy China resident nutritional need characteristics and culinary art custom, the key population that explicitly points out nutrition improvement in " Chinese food and nutrition development outline " is children crowd, women and children colony and the elderly colony, Chinese mid-aged population diet structure and variation tendency thereof that Nutrition and Food Safety Office of China Disease Prevention and control Centre carries out studies show that, compare with Chinese residents nutrition survey in 1992, obvious variation had occured in town and country mid-aged population diet structure in 2002, the cooking oil consumption figure obviously increases, meals uneven than before 10 years more very.Its direct result is that the present mid-aged population cardiovascular and cerebrovascular disease incidence of disease is high, and sick spectrum is wide, in the serious harm human health, has also caused huge financial burden to society.The crowds such as infant, youngsters and children, pregnant woman and wet nurse are as the class crowd higher to nutritional need, and grease grows, improves intellectual level to keeping it when supplying with energy, replenish brain and neurotrophy composition tool and be of great significance.The intake of wherein strengthening long-chain polyunsaturated fatty acid has very important significance; China resident's cooking method is mainly frying and cooking fried simultaneously, in grease, the nutritional labeling loss is serious under high-temperature heating, the grease firsts and seconds oxidation product that produces will have a negative impact to health, therefore need to solve the thermo oxidative stability problem of nutrient formulation oil.
China is the extremely abundant country of an oil resource, mainly comprise woody oleiferous plants and draft oil plant, wherein camellia seed oil, linseed oil, walnut oil are as the characteristic oil resource of China, among the people extensively edible because having brain-tonifying effect, enhancing development effect and prevention cardiovascular and cerebrovascular disease effect, but the absorption of above single grease is difficult to provide rational aliphatic acid to form; Corn oil is rich in natural VE and phytosterol, and grape-kernel oil is rich in plant polyphenol and phytosterol, and in grease, these endogenous micro-nutrient compositions can significantly improve oil oxidative stability and nutritive value.How effectively allocating these greases is the another one problem that the present invention need to solve to obtain a kind of nutrient formulation oil that is suitable for China family cooking custom and has a functional activity.
Vitamin E is one of most important antioxidant in organism, can prevent proceeding of lipid oxidation chain reaction, and the Cell protection film is the first line of defence of Antioxidation Mechanism, and cardiovascular and cerebrovascular disease is had prevention effect preferably.Vitamin E comprise α-, β-, γ-and the isomers of the multiple configuration such as Delta-Tocopherol, the isomorphism type tocopherol does not have larger difference to the oxidation resistance of grease, existing result of study shows that the formation of peroxide in the rapeseed oil that Gamma-Tocopherol and Delta-Tocopherol cause radiation has significant inhibitory action, and the effect of alpha-tocopherol is not remarkable, and most results of study show that also the antioxidant effect size order of isomorphism type tocopherol is not δ＞γ＞β＞α; But also do not relate at present this respect field in existing patent.
Disclosing a kind of healthy edible blend oil balanced in nutrition with brain-invigorating in patent CN101617721A, be mainly to add algal oil to produce a desired effect in grease, and the mass ratio of n-6 and n-3 aliphatic acid is 4-6: 1;
A kind of health blend oil of balanced fatty acid is disclosed in patent CN101766236A, n-6 aliphatic acid and n-3 fatty acid proportion (3-8): 1, and strengthen oil oxidative stability by adding phytosterol and oryzanol and other antioxidant, there are the problems such as the more and cost of material of adding ingredient is higher;
A kind of ready-mixed oil and preparation method thereof is disclosed in patent CN101664078A, grease is comprised of camellia seed oil, rapeseed oil and soybean oil, and interpolation liposoluble vitamin, prevent the cardiovascular and cerebrovascular disease effect to reach, but do not consider that in grease, rational aliphatic acid forms and the stable problem of grease culinary art;
Disclose a kind of Woody plant blending oil of scientific matching in patent CN101664077A, by several composition the in camellia seed oil, tea seed oil, walnut oil, grape-kernel oil, rubber seed oil and eucommia ulmoides seed oil, but do not solved the oxidation stability of grease;
A kind of edible camellia oil blend oil and preparation method thereof is disclosed in patent CN10119465A, formed by camellia seed oil, rapeseed oil, peanut oil, soybean oil and rose-seed oil, the mass ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1: 6: 1, the mass ratio of n-6 aliphatic acid and n-3 aliphatic acid is (4-6): 1, polyunsaturated fatty acid and n-3 content of fatty acid are lower, and do not solve the oil oxidative stability problem;
A kind of edible vegetable blend oil with balanced fatty acid is disclosed in patent CN101715840A, mainly take refined rapeseed oil, refined maize's oil, squeezing peanut oil, refining sunflower oil, purified soyabean oil, perilla herb oil, camellia seed oil, rice bran oil and sesame oil as feedstock oil, the mass ratio of n-6 and n-3 aliphatic acid is (4-6): 1, the n-3 content of fatty acid is lower, and the target group is indefinite;
disclose a kind of fatty acid component balanced and contain the middle-aged and old type nutrient blend oil of active component in patent CN101720822A, by linseed oil, walnut oil, two low rapeseed oils, soybean oil, wheat-germ oil, corn oil, sesame oil, peanut oil, grape-kernel oil, rice bran oil, camellia seed oil, evening primrose oil, several compositions in sunflower seeds wet goods vegetable oil, mainly produce a desired effect by the gamma-Linolenic acid in grease, saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid ratio are (0.6-0.8): 1: 1, n-6 aliphatic acid and n-3 fatty acid proportion (4-6): 1, saturated fatty acid content is higher, do not meet the nutritional need present situation of China, and the anti-oxidant composition of endogenous that contains by grease self also deficiency so that Oil stability satisfies the culinary art custom of China,
Be foundation mainly with the foreign study result in the patent of existing relevant nutrient blend oil, especially do not need to carry out family's key population nutritional need characteristics and the culinary art custom of nutrition improvement in conjunction with China resident; Therefore edible nutrient formulation oil with culinary art good stability of enhancing development effect and auxiliary antilipemic effect is badly in need of providing the resident of a kind of suitable China family in this area.
Summary of the invention
The object of the present invention is to provide a kind of family balance formula oil and preparation method thereof, this family's balance formula oil is cooked good stability, is had enhancing development effect and and auxiliary antilipemic effect.
To achieve these goals, the technical solution used in the present invention is: a kind of family balance formula oil, it is characterized in that it is prepared from by comprising following raw materials according: the camellia seed oil that is rich in monounsaturated fatty acids, be rich in corn oil and the grape-kernel oil of n-6 aliphatic acid, be rich in linseed oil and walnut oil and the mixed tocopherol of n-3 aliphatic acid; The shared mass percent of each raw material is: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2%;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 76%-83%, linoleic acid mass content during the aliphatic acid of corn oil forms is 45%-60%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 60-75%, alpha-linolenic acid mass content during the aliphatic acid of linseed oil forms is 46%-56%, and the alpha-linolenic acid mass content during the aliphatic acid of walnut oil forms is 7.5%-15%; Gamma-Tocopherol in mixed tocopherol and Delta-Tocopherol gross mass content are 10%-50%.
In described family balance formula oil, saturated aliphatic acid quality is (2-2.9) less than the mass ratio of 12%, n-6 aliphatic acid and n-3 aliphatic acid: 1.
The preparation method of above-mentioned a kind of family balance formula oil is characterized in that it comprises the steps:
1) detect the aliphatic acid of analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material and form and physical and chemical quality, screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 76%-83%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 45%-60%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 60-75%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 46%-56%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 7.5%-15%; Gamma-Tocopherol in mixed tocopherol and Delta-Tocopherol gross mass content are 10%-50% (mass ratio between Gamma-Tocopherol and Delta-Tocopherol for arbitrarily than);
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2%, choose camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and walnut oil, 45-50 ℃ is stirred 45-60min and evenly spreads in grape-kernel oil and walnut oil to mixed tocopherol, obtains mixed material;
4) mixed material is changed in large agitator tank, add camellia seed oil, corn oil and linseed oil, 35-40 ℃ is stirred 25-30min to being uniformly dispersed, obtains a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
Family provided by the invention balance formula oil is suitable for eating at home, can be used for cold and dressed with sauce, steam, boil, fry and cooking method such as appropriateness frying etc.
The invention has the beneficial effects as follows:
1). family of the present invention balance formula oil considers that the key population that explicitly points out nutrition improvement in " Chinese food and nutrition development outline " is children crowd, women and children colony and the elderly colony, and this types of populations is had relatively high expectations to the intake of monounsaturated fatty acids and polyunsaturated fatty acid n-3 class aliphatic acid; Formula oil can satisfy the nutrition of lipids demand of key population, and the ratio of n-6 aliphatic acid and n-3 aliphatic acid forms near human mother's milk aliphatic acid, be conducive to enhancing development, and high n-3 content of fatty acid is to preventing cardiovascular and cerebrovascular disease to have beneficial effect; Have enhancing development effect and auxiliary antilipemic effect through the animal experiment proof; Gained aliphatic acid forms the nutritional need of the key population children crowd meet nutrition improvement, women and children colony and the elderly colony.
2). the present invention forms the crowd who needs emphasis to improve nutrition in needs and family according to aliphatic acid, select the camellia seed oil that has the title of " Yuesao oil " among the people, be of value to the healthy linseed oil with having nootropic effect of cardiovascular and cerebrovascular disease, have the walnut oil of nootropic effect and be rich in phytosterol and the corn oil of vitamin E, be rich in five kinds of oleic acid-induceds of grape pip wet goods of phytosterol and plant polyphenol, the grease of linoleic acid type and flax acid type is allocated, has good nutritive effect effect, and be rich in phytosterol in grease, the anti-oxidant composition of the endogenous such as vitamin E and plant polyphenol has significant antioxidation, can increase the culinary art stability of grease,
3). the present invention contains Delta-Tocopherol and the Gamma-Tocopherol that is rich in 10-50% in the mixed tocopherol of 0.04-0.2%, Delta-Tocopherol and Gamma-Tocopherol are antioxidant effect isomers preferably in tocopherol, can significantly strengthen the culinary art stability of grease, by adding the endogenous antioxidant content that self contains in exogenous antioxidant content and grease, thereby can significantly strengthen the culinary art stability of family's balance formula oil, make grease meet China resident's culinary art custom.
The specific embodiment
Embodiment 1:
The preparation method of above-mentioned a kind of family balance formula oil, it comprises the steps:
1) detect the aliphatic acid of analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material and form and physical and chemical quality, screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 80.4%, linoleic acid mass content during the aliphatic acid of corn oil forms is 49.7%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 71.6%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 52.8%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 10.3%; Delta-Tocopherol in mixed tocopherol and gama tocopherol mass content are 35% (mass ratio between Gamma-Tocopherol and Delta-Tocopherol is not required);
2) the 1.2g mixed tocopherol is added in 60g grape-kernel oil and 60g walnut oil, after 48 ℃ of stirring 55min, mixed material is changed in large agitator tank, add 400g camellia seed oil, 230g corn oil and 250g linseed oil, 38 ℃ are stirred 28min; Obtain a kind of family balance formula oil product.
The aliphatic acid that detects family's balance formula oil product (or claiming nutrient formulation oil) forms, and the mass ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1: 4.3: 4.0, and the mass ratio of n-6 and n-3 aliphatic acid is 2: 1; Detect phytosterol and the polyphenol of family's balance formula oil product, content is respectively 4.96g/kg and 29.5mg/100g.
The culinary art results of stability shows, heating 60min is in the time at 150 ℃ and 210 ℃ of temperature for family's balance formula oil product, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably.Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ in heating-up temperature and has higher culinary art stability under the 30min condition with being no more than heat time heating time.
Detect through the rat animal experiment and show, take in the dosage gavage family balance formula oil product of 25g/d to be equivalent to the people, respectively take distilled water and peanut oil as contrast, gavage is 56 days continuously, result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increasing action (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth Experiment on Function result.
adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, take in the dosage gavage nutrient formulation oil of 25g/d to be equivalent to the people, gavage is 42 days continuously, result shows in the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, this family's balance formula oil auxiliary lipid-lowering function results of animal is positive.
Embodiment 2:
The preparation method of above-mentioned a kind of family balance formula oil, it comprises the steps:
1) detect the aliphatic acid of analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material and form and physical and chemical quality, screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 79.8%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 51.9%, during aliphatic acid in grape-kernel oil forms, the linoleic acid mass content is 68.4%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 53.8%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 8.8%; Delta-Tocopherol in mixed tocopherol and gama tocopherol mass content are 20% (mass ratio between Gamma-Tocopherol and Delta-Tocopherol is not required);
2) the 1g mixed tocopherol is added in 50g grape-kernel oil and 20g walnut oil, after 50 ℃ of stirring 50min, mixed material is changed in large agitator tank, add 400g camellia seed oil, 349g corn oil and 180g linseed oil, 35 ℃ are stirred 25min, obtain a kind of family balance formula oil product.
The aliphatic acid that detects family's balance formula oil forms, and the mass ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1: 4.1: 3.4, and the mass ratio of n-6 and n-3 aliphatic acid is 2.9: 1; Detect phytosterol and the polyphenol of formula oil, content is respectively 6.38g/kg and 15.30mg/100g.
The culinary art results of stability shows, heating 60min is in the time at 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably.Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ in heating-up temperature and has higher culinary art stability under the 30min condition with being no more than heat time heating time.。
Detect through the rat animal experiment and show, take in the dosage gavage family balance formula oil product of 25g/d to be equivalent to the people, respectively take distilled water and peanut oil as contrast, gavage is 56 days continuously, result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increasing action (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth Experiment on Function result.
adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, take in the dosage gavage nutrient formulation oil of 25g/d to be equivalent to the people, gavage is 42 days continuously, result shows in the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, this family's balance formula oil auxiliary lipid-lowering function results of animal is positive.
Embodiment 3:
The preparation method of a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid of detect analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material forms and physical and chemical quality, and screening is complied with the national standard requirements and camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 76%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 45%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 60%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 46%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 7.5%; Delta-Tocopherol in mixed tocopherol and gama tocopherol mass content are 10%;
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%, corn oil 40%, grape-kernel oil 5%, linseed oil 15%, walnut oil 5%, mixed tocopherol 0.04% take camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and walnut oil, 45 ℃ are stirred 45min and evenly spread in grape-kernel oil and walnut oil to mixed tocopherol, obtain mixed material;
4) mixed material is changed in large agitator tank, add camellia seed oil, corn oil and linseed oil, 35 ℃ are stirred 25min to being uniformly dispersed, obtain a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
The culinary art results of stability shows, heating 60min is in the time at 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably.Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ in heating-up temperature and has higher culinary art stability under the 30min condition with being no more than heat time heating time.。
Detect through the rat animal experiment and show, take in the dosage gavage family balance formula oil product of 25g/d to be equivalent to the people, respectively take distilled water and peanut oil as contrast, gavage is 56 days continuously, result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increasing action (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth Experiment on Function result.
adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, take in the dosage gavage nutrient formulation oil of 25g/d to be equivalent to the people, gavage is 42 days continuously, result shows in the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, this family's balance formula oil auxiliary lipid-lowering function results of animal is positive.
Embodiment 4:
The preparation method of a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid of detect analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material forms and physical and chemical quality, and screening is complied with the national standard requirements and camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 83%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 60%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 75%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 56%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 15%; Delta-Tocopherol in mixed tocopherol and gama tocopherol mass content are 50%;
2) by the shared mass percent of each raw material be: camellia seed oil 50%, corn oil 20%, grape-kernel oil 5%, linseed oil 15%, walnut oil 9.8%, mixed tocopherol 0.2%, choose camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and walnut oil, 50 ℃ are stirred 60min and evenly spread in grape-kernel oil and walnut oil to mixed tocopherol, obtain mixed material;
4) mixed material is changed in large agitator tank, add camellia seed oil, corn oil and linseed oil, 40 ℃ are stirred 30min to being uniformly dispersed, obtain a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
The culinary art results of stability shows, heating 60min is in the time at 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably; Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ in heating-up temperature and has higher culinary art stability under the 30min condition with being no more than heat time heating time.。
Detect through the rat animal experiment and show, take in the dosage gavage family balance formula oil product of 25g/d to be equivalent to the people, respectively take distilled water and peanut oil as contrast, gavage is 56 days continuously, result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increasing action (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth Experiment on Function result.
adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, take in the dosage gavage nutrient formulation oil of 25g/d to be equivalent to the people, gavage is 42 days continuously, result shows in the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, this family's balance formula oil auxiliary lipid-lowering function results of animal is positive.
Embodiment 5:
The preparation method of a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid of detect analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material forms and physical and chemical quality, and screening is complied with the national standard requirements and camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 80%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 50%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 70%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 50%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 10%; Delta-Tocopherol in mixed tocopherol and gama tocopherol mass content are 30%;
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%, corn oil 20%, grape-kernel oil 10%, linseed oil 30%, walnut oil 5%, mixed tocopherol 0.04%, choose camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and walnut oil, 45-50 ℃ is stirred 45-60min and evenly spreads in grape-kernel oil and walnut oil to mixed tocopherol, obtains mixed material;
4) mixed material is changed in large agitator tank, add camellia seed oil, corn oil and linseed oil, 35-40 ℃ is stirred 25-30min to being uniformly dispersed, obtains a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
The culinary art results of stability shows, heating 60min is in the time at 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably; Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ in heating-up temperature and has higher culinary art stability under the 30min condition with being no more than heat time heating time.。
Detect through the rat animal experiment and show, take in the dosage gavage family balance formula oil product of 25g/d to be equivalent to the people, respectively take distilled water and peanut oil as contrast, gavage is 56 days continuously, result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increasing action (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth Experiment on Function result.
adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, take in the dosage gavage nutrient formulation oil of 25g/d to be equivalent to the people, gavage is 42 days continuously, result shows in the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, this family's balance formula oil auxiliary lipid-lowering function results of animal is positive.
The above is only preferred embodiment of the present invention, be not to limit essence technology contents scope of the present invention, essence technology contents of the present invention is broadly to be defined in the claim scope of application, any technology entity or method that other people complete, if defined identical with the claim scope of application, also or a kind of change of equivalence, all will be regarded as being covered by among this claim scope.
Claims (2)
1. family's balance formula is oily, it is characterized in that it is prepared from by following raw materials according: the camellia seed oil that is rich in monounsaturated fatty acids, be rich in corn oil and the grape-kernel oil of n-6 aliphatic acid, be rich in linseed oil and walnut oil and the mixed tocopherol of n-3 aliphatic acid; The shared mass percent of each raw material is: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2%;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 76%-83%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 45%-60%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 60-75%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 46%-56%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 7.5%-15%; Gamma-Tocopherol in mixed tocopherol and Delta-Tocopherol gross mass content are 10%-50%;
In described family balance formula oil, saturated aliphatic acid quality is (2-2.9) less than the mass ratio of 12%, n-6 aliphatic acid and n-3 aliphatic acid: 1.
2. the preparation method of a kind of family as claimed in claim 1 balance formula oil, is characterized in that it comprises the steps:
1) detect the aliphatic acid of analyzing in camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol raw material and form and physical and chemical quality, screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
During the aliphatic acid of described camellia seed oil forms, the oleic acid mass content is 76%-83%, during the aliphatic acid of corn oil forms, the linoleic acid mass content is 45%-60%, during the aliphatic acid of grape-kernel oil forms, the linoleic acid mass content is 60-75%, during the aliphatic acid of linseed oil forms, the alpha-linolenic acid mass content is 46%-56%, and during the aliphatic acid of walnut oil forms, the alpha-linolenic acid mass content is 7.5%-15%; In mixed tocopherol, Gamma-Tocopherol and Delta-Tocopherol gross mass content are 10%-50%;
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2% take camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and walnut oil, 45-50 ℃ of stirring 45-60min evenly spreads in grape-kernel oil and walnut oil to mixing fertility, obtains mixed material;
4) mixed material is changed in large agitator tank, add camellia seed oil, corn oil and linseed oil, 35-40 ℃ is stirred 25-30min to being uniformly dispersed, and obtains a kind of family balance formula oil.
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| CN112136905A (en) * | 2020-09-27 | 2020-12-29 | 怀化市富源油业有限公司 | Edible oil |
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| ES2325516B1 (en) * | 2007-12-21 | 2010-06-17 | Consejo Superior De Investigaciones Cientificas | SUNFLOWER OIL WITH HIGH THERMOSTABILITY. |
| CN101690526A (en) * | 2009-09-03 | 2010-04-07 | 祁景泉 | Blend oil with proportional fatty acid prepared by walnut oil and other plant oils |
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Owner name: HUNAN GREAT SANXIANG OIL TEA CAMELLIA TECHNOLOGY C Free format text: FORMER OWNER: INST. OF OIL CROPS, CHINESE ACADEMY OF AGRICULTURAL SCENCES Effective date: 20140305 |
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