CN102239933A - Family balance formula oil and preparation method thereof - Google Patents
Family balance formula oil and preparation method thereof Download PDFInfo
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- CN102239933A CN102239933A CN2011101698515A CN201110169851A CN102239933A CN 102239933 A CN102239933 A CN 102239933A CN 2011101698515 A CN2011101698515 A CN 2011101698515A CN 201110169851 A CN201110169851 A CN 201110169851A CN 102239933 A CN102239933 A CN 102239933A
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- 239000003921 oil Substances 0.000 claims abstract description 164
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- 239000008170 walnut oil Substances 0.000 claims abstract description 54
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- 239000002285 corn oil Substances 0.000 claims abstract description 48
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- 235000021388 linseed oil Nutrition 0.000 claims abstract description 48
- 239000002994 raw material Substances 0.000 claims abstract description 24
- 235000021281 monounsaturated fatty acids Nutrition 0.000 claims abstract description 8
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 54
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- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 claims description 36
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- 235000020778 linoleic acid Nutrition 0.000 claims description 19
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 claims description 19
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- 239000002478 γ-tocopherol Substances 0.000 claims description 10
- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 claims description 10
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Landscapes
- Edible Oils And Fats (AREA)
Abstract
The invention belongs to the field of edible oil, particularly relates to nutritive formula oil which is suitable for families in China, and has good stability and functions of promoting growth and development and assisting the blood fat reduction, and a preparation method thereof. The family balance formula oil provided by the invention is characterized by comprising the following raw materials in percentage by mass: 34.96-50% of oil tea camellia seed oil rich in monounsaturated fatty acid, 20-40% of corn oil rich in n-6 fatty acid, 5-10% of grape seed oil rich in n-6 fatty acid, 15-30% of linseed oil rich in n-6 fatty acid, 5-10% of walnut oil rich in n-6 fatty acid and 0.04-0.2% of mixed tocopheryl. The family balance formula oil has good cooking stability, and has the functions of promoting growth and development and assisting the blood fat reduction.
Description
Technical field
The invention belongs to the edible oil and fat field, relate in particular to a kind of suitable China eating at home the culinary art good stability, have nutrient formulation oil that promotes effect of growing and auxiliary antilipemic effect and preparation method thereof.
Background technology
Edible oil and fat more and more come into one's own to the influence of residents ' health, grease absorption structure and intake are unreasonable will to cause various modern civilization disease, China resident edible oil consumption figure urban and rural residents are respectively 44g and 40.7g at present, ground such as Beijing, Shanghai has reached 83-85g, is higher than the 25g-30g/ days standards of recommending in resident's dietary guidelines of Chinese Soclety of Nutrition's formulation in 2007 far away; The variation of grease consumption structure is embodied in the animal fat intake rises rapidly, rural area animal fat intake with 10 years before compare and risen 82.7%, palm oil year consumption figure also reached nearly 6,000,000 tons, cause the saturated fatty acid intake too high; The characteristics of modern oil-producing technique also cause a large amount of nutritional labeling losses in the grease simultaneously.Under this background, according to the intake standard that NI is recommended, the nutrient formulation oil of the suitable China resident eating at home of development has the meaning of particular importance.
Family's balance formula oil should have concurrently and satisfy China resident nutritional need characteristics and culinary art custom, the key population that spells out nutrition improvement in " Chinese food and nutrition development outline " is children crowd, women and children colony and the elderly colony, Chinese mid-aged population diet structure and variation tendency thereof that Nutrition and Food Safety Office of China Disease Prevention and control Centre carries out studies show that, compare with Chinese residents nutrition survey in 1992, obvious variation had taken place in town and country mid-aged population diet structure in 2002, cooking oily consumption figure then obviously increases, meals uneven than before 10 years more very.Its direct result is present mid-aged population cardiovascular and cerebrovascular disease incidence of disease height, and sick spectrum is wide, in the serious harm human health, has also caused huge financial burden to society.Crowds such as infant, youngsters and children, pregnant woman and wet nurse are as the class crowd higher to nutritional need, and grease grows, improves intellectual level to keeping it in energize, replenish brain and neurotrophy composition and have crucial meaning.The intake of wherein strengthening long-chain polyunsaturated fatty acid then has very important significance; China resident's cooking method mainly is frying and cooks stir-fry simultaneously, the nutritional labeling loss is serious in the grease under the high temperature heating, the grease firsts and seconds oxidation product that produces will have a negative impact to health, therefore need to solve the thermo oxidative stability problem of nutrient formulation oil.
China is the extremely abundant country of an oil resource, mainly comprise woody oleiferous plants and draft oil plant, wherein camellia seed oil, linseed oil, walnut oil are as the characteristic oil resource of China, among the people extensively edible because have brain-tonifying effect, promote the effect of growing and prevent the cardiovascular and cerebrovascular disease effect, but the absorption of above single grease is difficult to provide rational aliphatic acid to be formed; Corn oil is rich in natural VE and phytosterol, and grape-kernel oil is rich in plant polyphenol and phytosterol, and these endogenous micro-nutrient compositions can significantly improve oil oxidative stability and nutritive value in the grease.How effectively allocating these greases is the another one problem that the present invention need solve to obtain a kind of nutrient formulation oil that is suitable for China family cooking custom and has a functional activity.
Vitamin E is one of most important antioxidant in the organism, can prevent proceeding of lipid oxidation chain reaction, and the protection cell membrane is the first line of defence of anti-oxidant mechanism, and cardiovascular and cerebrovascular disease is had prevention effect preferably.Vitamin E comprise α-, β-, γ-and the isomers of multiple configuration such as Delta-Tocopherol, the isomorphism type tocopherol does not have than big-difference the oxidation resistance of grease, existing result of study shows that the formation of peroxide in the rapeseed oil that Gamma-Tocopherol and Delta-Tocopherol cause radiation has significant inhibitory effect, and the effect of alpha-tocopherol is not remarkable, and most results of study show that also the antioxidant effect size order of isomorphism type tocopherol is not δ＞γ＞β＞α; But in existing patent, also do not relate to this respect field at present.
Disclosing a kind of healthy edible blend oil balanced in nutrition with brain-invigorating in patent CN101617721A, mainly be to add algal oil to produce a desired effect in grease, and the mass ratio of n-6 and n-3 aliphatic acid is 4-6: 1;
A kind of health blend oil of balanced fatty acid is disclosed in patent CN101766236A, n-6 aliphatic acid and n-3 fatty acid proportion (3-8): 1, and strengthen oil oxidative stability by adding phytosterol and oryzanol and other antioxidant, exist the more and cost of material of adding ingredient than problems such as height;
A kind of ready-mixed oil and preparation method thereof is disclosed in patent CN101664078A, grease is made up of camellia seed oil, rapeseed oil and soybean oil, and interpolation liposoluble vitamin, prevent the cardiovascular and cerebrovascular disease effect to reach, but do not consider that rational aliphatic acid is formed and the stable problem of grease culinary art in the grease;
In patent CN101664077A, disclose a kind of Woody plant blending oil of scientific matching,, but do not solved the oxidation stability of grease by several composition the in camellia seed oil, tea seed oil, walnut oil, grape-kernel oil, rubber seed oil and the eucommia ulmoides seed oil;
A kind of edible camellia oil blend oil and preparation method thereof is disclosed in patent CN10119465A, form by camellia seed oil, rapeseed oil, peanut oil, soybean oil and rose-seed oil, the mass ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1: 6: 1, the mass ratio of n-6 aliphatic acid and n-3 aliphatic acid is (4-6): 1, polyunsaturated fatty acid and n-3 content of fatty acid are lower, and do not solve the oil oxidative stability problem;
A kind of edible vegetable blend oil with balanced fatty acid is disclosed in patent CN101715840A, be feedstock oil mainly with refined rapeseed oil, refined maize's oil, squeezing peanut oil, refining sunflower oil, purified soyabean oil, perilla herb oil, camellia seed oil, rice bran oil and sesame oil, the mass ratio of n-6 and n-3 aliphatic acid is (4-6): 1, the n-3 content of fatty acid is lower, and the target group is indeterminate;
In patent CN101720822A, disclose a kind of fatty acid component balanced and contain the middle-aged and old type nutrient blend oil of active component, by linseed oil, walnut oil, two low rapeseed oils, soybean oil, wheat-germ oil, corn oil, sesame oil, peanut oil, grape-kernel oil, rice bran oil, camellia seed oil, evening primrose oil, several compositions in the sunflower seeds wet goods vegetable oil, mainly produce a desired effect by the gamma-Linolenic acid in the grease, saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid ratio are (0.6-0.8): 1: 1, n-6 aliphatic acid and n-3 fatty acid proportion (4-6): 1, saturated fatty acid content is higher, do not meet the nutritional need present situation of China, and the anti-oxidant composition of endogenous that contains by grease self also deficiency so that grease stability satisfies the culinary art custom of China;
Many in the patent of existing relevant nutrient blend oil is foundation with the foreign study result, does not especially need to carry out the family's key population nutritional need characteristics and the culinary art custom of nutrition improvement in conjunction with China resident; Therefore edible nutrient formulation oil with the culinary art good stability that promotes effect of growing and auxiliary antilipemic effect is badly in need of providing the resident of a kind of suitable China family in this area.
Summary of the invention
The object of the present invention is to provide a kind of family balance formula oil and preparation method thereof, this family's balance formula oil is cooked good stability, is had promotion effect of growing and and auxiliary antilipemic effect.
To achieve these goals, the technical solution used in the present invention is: a kind of family balance formula oil, it is characterized in that it is prepared from by comprising following raw materials according: the camellia seed oil that is rich in monounsaturated fatty acids, be rich in the corn oil and the grape-kernel oil of n-6 aliphatic acid, be rich in linseed oil and the walnut oil and the mixed tocopherol of n-3 aliphatic acid; The shared mass percent of each raw material is: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2%;
The oleic acid mass content was 76%-83% during the aliphatic acid of described camellia seed oil was formed, linoleic acid mass content during the aliphatic acid of corn oil is formed is 45%-60%, the linoleic acid mass content was 60-75% during the aliphatic acid of grape-kernel oil was formed, alpha-linolenic acid mass content during the aliphatic acid of linseed oil is formed is 46%-56%, and the alpha-linolenic acid mass content during the aliphatic acid of walnut oil is formed is 7.5%-15%; Gamma-Tocopherol in the mixed tocopherol and Delta-Tocopherol gross mass content are 10%-50%.
Saturated aliphatic acid quality is less than 12% in the described family balance formula oil, and the mass ratio of n-6 aliphatic acid and n-3 aliphatic acid is (2-2.9): 1.
The preparation method of above-mentioned a kind of family balance formula oil is characterized in that it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 76%-83% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 45%-60% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 60-75% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 46%-56% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 7.5%-15% during the aliphatic acid of walnut oil was formed; Gamma-Tocopherol in the mixed tocopherol and Delta-Tocopherol gross mass content are 10%-50% (mass ratio between Gamma-Tocopherol and the Delta-Tocopherol for arbitrarily than);
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2%, choose camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and the walnut oil, 45-50 ℃ is stirred 45-60min and evenly spreads in grape-kernel oil and the walnut oil to mixed tocopherol, obtains mixed material;
4) mixed material is changed in the big agitator tank, add camellia seed oil, corn oil and linseed oil, 35-40 ℃ is stirred 25-30min to being uniformly dispersed, obtains a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
Family provided by the invention balance formula oil is suitable for eating at home, can be used for cold and dressed with sauce, steam, boil, fry and cooking method such as appropriateness frying etc.
The invention has the beneficial effects as follows:
1). family of the present invention balance formula oil considers that the key population that spells out nutrition improvement in " Chinese food and nutrition development outline " is children crowd, women and children colony and the elderly colony, and this types of populations is had relatively high expectations to the intake of monounsaturated fatty acids and polyunsaturated fatty acid n-3 class aliphatic acid; Prescription oil can satisfy the grease nutritional need of key population, and the ratio of n-6 aliphatic acid and n-3 aliphatic acid help promoting to grow, and high n-3 content of fatty acid has beneficial effect to the prevention cardiovascular and cerebrovascular disease near human mother's milk aliphatic acid composition; Have promotion effect of growing and auxiliary antilipemic effect through the animal experiment proof; Gained aliphatic acid is formed the nutritional need of the key population children crowd, women and children colony and the elderly colony that meet nutrition improvement.
2). the present invention forms the crowd who needs emphasis to improve nutrition in needs and the family according to aliphatic acid, select the camellia seed oil that has the title of " Yuesao oil " among the people for use, be of value to cardiovascular and cerebrovascular disease health and linseed oil with nootropic effect, have the walnut oil of nootropic effect and be rich in phytosterol and the corn oil of vitamin E, be rich in five kinds of oleic acid-induceds of grape pip wet goods of phytosterol and plant polyphenol, the grease of linoleic acid type and flax acid type is allocated, has good nutritive effect effect, and be rich in phytosterol in the grease, the anti-oxidant composition of endogenous such as vitamin E and plant polyphenol has significant antioxidant role, can increase the culinary art stability of grease;
3). the present invention contains Delta-Tocopherol and the Gamma-Tocopherol that is rich in 10-50% in the mixed tocopherol of 0.04-0.2%, Delta-Tocopherol and Gamma-Tocopherol are antioxidant effect isomers preferably in the tocopherol, can significantly strengthen the culinary art stability of grease, by adding the endogenous antioxidant content that self contains in exogenous antioxidant content and the grease, thereby can significantly strengthen the culinary art stability of family's balance formula oil, make grease meet China resident's culinary art custom.
The specific embodiment
Embodiment 1:
The preparation method of above-mentioned a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 80.4% during the aliphatic acid of described camellia seed oil was formed, linoleic acid mass content during the aliphatic acid of corn oil is formed is 49.7%, the linoleic acid mass content was 71.6% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 52.8% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 10.3% during the aliphatic acid of walnut oil was formed; Delta-Tocopherol in the mixed tocopherol and gama tocopherol mass content are 35% (mass ratio between Gamma-Tocopherol and the Delta-Tocopherol is not required);
2) the 1.2g mixed tocopherol is added in 60g grape-kernel oil and the 60g walnut oil, behind 48 ℃ of stirring 55min, mixed material is changed in the big agitator tank, add 400g camellia seed oil, 230g corn oil and 250g linseed oil, 38 ℃ are stirred 28min; Obtain a kind of family balance formula oil product.
Detect the aliphatic acid of family's balance formula oil product (or claiming nutrient formulation oil) and form, the mass ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1: 4.3: 4.0, and the mass ratio of n-6 and n-3 aliphatic acid is 2: 1; Detect the phytosterol and the polyphenol of family's balance formula oil product, content is respectively 4.96g/kg and 29.5mg/100g.
The culinary art results of stability shows, heating 60min is in the time under 150 ℃ and 210 ℃ of temperature for family's balance formula oil product, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably.Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ and heat time heating time and is no more than in heating-up temperature and has higher culinary art stability under the 30min condition.
Show through rat animal experiment detection, to be equivalent to the dosage filling stomach family balance formula oil product that the people takes in 25g/d, be contrast with distilled water and peanut oil respectively, continuous irrigation stomach 56 days, the result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increase effect (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth effect result of the test.
Adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, to be equivalent to the dosage filling stomach nutrient formulation oil that the people takes in 25g/d, continuous irrigation stomach 42 days, the result shows under the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, balance formula oil auxiliary lipid-lowering function zoopery result is positive in this family.
Embodiment 2:
The preparation method of above-mentioned a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 79.8% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 51.9% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 68.4% during aliphatic acid in the grape-kernel oil was formed, the alpha-linolenic acid mass content was 53.8% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 8.8% during the aliphatic acid of walnut oil was formed; Delta-Tocopherol in the mixed tocopherol and gama tocopherol mass content are 20% (mass ratio between Gamma-Tocopherol and the Delta-Tocopherol is not required);
2) the 1g mixed tocopherol is added in 50g grape-kernel oil and the 20g walnut oil, behind 50 ℃ of stirring 50min, mixed material is changed in the big agitator tank, add 400g camellia seed oil, 349g corn oil and 180g linseed oil, 35 ℃ are stirred 25min, obtain a kind of family balance formula oil product.
Detect the aliphatic acid of family's balance formula oil and form, the mass ratio of saturated fatty acid, monounsaturated fatty acids and polyunsaturated fatty acid is 1: 4.1: 3.4, and the mass ratio of n-6 and n-3 aliphatic acid is 2.9: 1; Detect the phytosterol and the polyphenol of prescription oil, content is respectively 6.38g/kg and 15.30mg/100g.
The culinary art results of stability shows, heating 60min is in the time under 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably.Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ and heat time heating time and is no more than in heating-up temperature and has higher culinary art stability under the 30min condition.。
Show through rat animal experiment detection, to be equivalent to the dosage filling stomach family balance formula oil product that the people takes in 25g/d, be contrast with distilled water and peanut oil respectively, continuous irrigation stomach 56 days, the result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increase effect (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth effect result of the test.
Adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, to be equivalent to the dosage filling stomach nutrient formulation oil that the people takes in 25g/d, continuous irrigation stomach 42 days, the result shows under the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, balance formula oil auxiliary lipid-lowering function zoopery result is positive in this family.
Embodiment 3:
The preparation method of a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening is complied with the national standard requirements and camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 76% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 45% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 60% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 46% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 7.5% during the aliphatic acid of walnut oil was formed; Delta-Tocopherol in the mixed tocopherol and gama tocopherol mass content are 10%;
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%, corn oil 40%, grape-kernel oil 5%, linseed oil 15%, walnut oil 5%, mixed tocopherol 0.04% take by weighing camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and the walnut oil, 45 ℃ are stirred 45min and evenly spread in grape-kernel oil and the walnut oil to mixed tocopherol, obtain mixed material;
4) mixed material is changed in the big agitator tank, add camellia seed oil, corn oil and linseed oil, 35 ℃ are stirred 25min to being uniformly dispersed, obtain a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
The culinary art results of stability shows, heating 60min is in the time under 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably.Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ and heat time heating time and is no more than in heating-up temperature and has higher culinary art stability under the 30min condition.。
Show through rat animal experiment detection, to be equivalent to the dosage filling stomach family balance formula oil product that the people takes in 25g/d, be contrast with distilled water and peanut oil respectively, continuous irrigation stomach 56 days, the result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increase effect (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth effect result of the test.
Adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, to be equivalent to the dosage filling stomach nutrient formulation oil that the people takes in 25g/d, continuous irrigation stomach 42 days, the result shows under the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, balance formula oil auxiliary lipid-lowering function zoopery result is positive in this family.
Embodiment 4:
The preparation method of a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening is complied with the national standard requirements and camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 83% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 60% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 75% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 56% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 15% during the aliphatic acid of walnut oil was formed; Delta-Tocopherol in the mixed tocopherol and gama tocopherol mass content are 50%;
2) by the shared mass percent of each raw material be: camellia seed oil 50%, corn oil 20%, grape-kernel oil 5%, linseed oil 15%, walnut oil 9.8%, mixed tocopherol 0.2%, choose camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and the walnut oil, 50 ℃ are stirred 60min and evenly spread in grape-kernel oil and the walnut oil to mixed tocopherol, obtain mixed material;
4) mixed material is changed in the big agitator tank, add camellia seed oil, corn oil and linseed oil, 40 ℃ are stirred 30min to being uniformly dispersed, obtain a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
The culinary art results of stability shows, heating 60min is in the time under 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably; Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ and heat time heating time and is no more than in heating-up temperature and has higher culinary art stability under the 30min condition.。
Show through rat animal experiment detection, to be equivalent to the dosage filling stomach family balance formula oil product that the people takes in 25g/d, be contrast with distilled water and peanut oil respectively, continuous irrigation stomach 56 days, the result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increase effect (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth effect result of the test.
Adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, to be equivalent to the dosage filling stomach nutrient formulation oil that the people takes in 25g/d, continuous irrigation stomach 42 days, the result shows under the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, balance formula oil auxiliary lipid-lowering function zoopery result is positive in this family.
Embodiment 5:
The preparation method of a kind of family balance formula oil, it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening is complied with the national standard requirements and camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 80% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 50% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 70% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 50% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 10% during the aliphatic acid of walnut oil was formed; Delta-Tocopherol in the mixed tocopherol and gama tocopherol mass content are 30%;
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%, corn oil 20%, grape-kernel oil 10%, linseed oil 30%, walnut oil 5%, mixed tocopherol 0.04%, choose camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and the walnut oil, 45-50 ℃ is stirred 45-60min and evenly spreads in grape-kernel oil and the walnut oil to mixed tocopherol, obtains mixed material;
4) mixed material is changed in the big agitator tank, add camellia seed oil, corn oil and linseed oil, 35-40 ℃ is stirred 25-30min to being uniformly dispersed, obtains a kind of family balance formula oil product; After product meets national standard and company standard after testing, the can warehouse-in.
The culinary art results of stability shows, heating 60min is in the time under 150 ℃ and 210 ℃ of temperature for family's balance formula oil, and acid value and aliphatic acid composition are not affected, and do not observe the generation of trans-fatty acid yet; And do not produce oxypolymer; Show that grease has heat endurance preferably; Grease is at 150 ℃ and surpass 30min 210 ℃ of heat time heating times, has produced a little aldehydes oxidation product and bad flavor material, and content of vitamin E and oxidation induction time decline; Show that family's balance formula oil product is no more than 210 ℃ and heat time heating time and is no more than in heating-up temperature and has higher culinary art stability under the 30min condition.。
Show through rat animal experiment detection, to be equivalent to the dosage filling stomach family balance formula oil product that the people takes in 25g/d, be contrast with distilled water and peanut oil respectively, continuous irrigation stomach 56 days, the result shows that rat body weight was significantly higher than distilled water control group and peanut oil control group at the 28th day and the 56th day, shows that family's balance formula oil product has increase effect (P＜0.05) to rat body weight; The rat height significantly was longer than distilled water control group and peanut oil control group (P＜0.05) at the 28th day, the 42nd day, the 56th day, show that family's balance formula oil product has accretion to the rat height; According to grow function assessment process regulation of improvement, it is positive that this family's balance formula oil product improves animal growth effect result of the test.
Adopt SPF level Wistar male rat, be divided into 4 groups according to serum cholesterol level, it is the basal feed group, the hyperlipidemia model control group, peanut oil control group and family's balance formula oil control group, to be equivalent to the dosage filling stomach nutrient formulation oil that the people takes in 25g/d, continuous irrigation stomach 42 days, the result shows under the situation that the high fat of blood animal model is set up, compare with hyperlipidemia model control group and peanut oil control group, family balance formula oil group serum total cholesterol and content of triglyceride significantly descend (P＜0.05), HDL-C content significantly raise (P＜0.05), learn the assessment process regulation according to auxiliary lipid-lowering function, balance formula oil auxiliary lipid-lowering function zoopery result is positive in this family.
The above only is preferred embodiment of the present invention, be not in order to limit essence technology contents scope of the present invention, essence technology contents of the present invention is broadly to be defined in the claim scope of application, any technology entity or method that other people finish, if it is defined identical with the claim scope of application, also or a kind of change of equivalence, all will be regarded as being covered by among this claim scope.
Claims (3)
1. family's balance formula oil, it is characterized in that it is prepared from by comprising following raw materials according: the camellia seed oil that is rich in monounsaturated fatty acids, be rich in the corn oil and the grape-kernel oil of n-6 aliphatic acid, be rich in linseed oil and the walnut oil and the mixed tocopherol of n-3 aliphatic acid; The shared mass percent of each raw material is: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2%;
The oleic acid mass content was 76%-83% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 45%-60% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 60-75% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 46%-56% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 7.5%-15% during the aliphatic acid of walnut oil was formed; Gamma-Tocopherol in the mixed tocopherol and Delta-Tocopherol gross mass content are 10%-50%.
2. a kind of family according to claim 1 balance formula oil is characterized in that: saturated aliphatic acid quality is less than 12% in the described family balance formula oil, and the mass ratio of n-6 aliphatic acid and n-3 aliphatic acid is (2-2.9): 1.
3. the preparation method of a kind of family as claimed in claim 1 balance formula oil is characterized in that it comprises the steps:
1) aliphatic acid in check and analysis camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material is formed and physical and chemical quality, and screening obtains meeting camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and the mixed tocopherol raw material of following requirement;
The oleic acid mass content was 76%-83% during the aliphatic acid of described camellia seed oil was formed, the linoleic acid mass content was 45%-60% during the aliphatic acid of corn oil was formed, the linoleic acid mass content was 60-75% during the aliphatic acid of grape-kernel oil was formed, the alpha-linolenic acid mass content was 46%-56% during the aliphatic acid of linseed oil was formed, and the alpha-linolenic acid mass content was 7.5%-15% during the aliphatic acid of walnut oil was formed; Gamma-Tocopherol and Delta-Tocopherol gross mass content are 10%-50% in the mixed tocopherol;
2) by the shared mass percent of each raw material be: camellia seed oil 34.96%-50%, corn oil 20%-40%, grape-kernel oil 5%-10%, linseed oil 15%-30%, walnut oil 5%-10%, mixed tocopherol 0.04-0.2% take by weighing camellia seed oil, corn oil, grape-kernel oil, linseed oil, walnut oil and mixed tocopherol;
3) mixed tocopherol is added in grape-kernel oil and the walnut oil, 45-50 ℃ of stirring 45-60min evenly spreads in grape-kernel oil and the walnut oil to mixing fertility, obtains mixed material;
4) mixed material is changed in the big agitator tank, add camellia seed oil, corn oil and linseed oil, 35-40 ℃ is stirred 25-30min to being uniformly dispersed, obtains a kind of family balance formula oil.
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Address after: 421101, Hunan Hengyang Hengnan County Industrial Park gathered Patentee after: Hunan Dasanxiang Camellia Oil Technology Co., Ltd. Address before: 421101, Hunan Hengyang Hengnan County Industrial Park gathered Patentee before: Hunan Great Sanxiang Camellia Technology Co., Ltd. |
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