CN105124594A - Multi-nutrient anti-ageing rice-bran-oil microcapsule and preparation method thereof - Google Patents
Multi-nutrient anti-ageing rice-bran-oil microcapsule and preparation method thereof Download PDFInfo
- Publication number
- CN105124594A CN105124594A CN201510368944.9A CN201510368944A CN105124594A CN 105124594 A CN105124594 A CN 105124594A CN 201510368944 A CN201510368944 A CN 201510368944A CN 105124594 A CN105124594 A CN 105124594A
- Authority
- CN
- China
- Prior art keywords
- rice bran
- oil
- capsule
- ageing
- micro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000008165 rice bran oil Substances 0.000 title claims abstract description 70
- 235000019774 Rice Bran oil Nutrition 0.000 title claims abstract description 69
- 239000003094 microcapsule Substances 0.000 title claims abstract description 65
- 230000003712 anti-aging effect Effects 0.000 title claims abstract description 59
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 239000000463 material Substances 0.000 claims abstract description 152
- 239000003921 oil Substances 0.000 claims abstract description 54
- 235000019198 oils Nutrition 0.000 claims abstract description 54
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 24
- 240000008042 Zea mays Species 0.000 claims abstract description 20
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims abstract description 20
- 244000000626 Daucus carota Species 0.000 claims abstract description 19
- 235000002767 Daucus carota Nutrition 0.000 claims abstract description 19
- 244000178231 Rosmarinus officinalis Species 0.000 claims abstract description 19
- 240000007594 Oryza sativa Species 0.000 claims abstract description 15
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 15
- 238000012545 processing Methods 0.000 claims abstract description 15
- 235000009566 rice Nutrition 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 239000002699 waste material Substances 0.000 claims abstract description 9
- 238000005119 centrifugation Methods 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 103
- 235000016709 nutrition Nutrition 0.000 claims description 54
- 230000035764 nutrition Effects 0.000 claims description 52
- 102000004190 Enzymes Human genes 0.000 claims description 32
- 108090000790 Enzymes Proteins 0.000 claims description 32
- 238000004945 emulsification Methods 0.000 claims description 32
- 229940088598 enzyme Drugs 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 244000052707 Camellia sinensis Species 0.000 claims description 21
- 235000006468 Thea sinensis Nutrition 0.000 claims description 21
- 241000723418 Carya Species 0.000 claims description 20
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 claims description 19
- 238000009413 insulation Methods 0.000 claims description 19
- 235000009973 maize Nutrition 0.000 claims description 19
- 235000017965 Asarum canadense Nutrition 0.000 claims description 18
- 241000522254 Cassia Species 0.000 claims description 18
- 235000000385 Costus speciosus Nutrition 0.000 claims description 18
- 240000006509 Gynostemma pentaphyllum Species 0.000 claims description 18
- 235000002956 Gynostemma pentaphyllum Nutrition 0.000 claims description 18
- 244000241872 Lycium chinense Species 0.000 claims description 18
- 235000015468 Lycium chinense Nutrition 0.000 claims description 18
- 241000606265 Valeriana jatamansi Species 0.000 claims description 18
- 235000009754 Vitis X bourquina Nutrition 0.000 claims description 18
- 235000012333 Vitis X labruscana Nutrition 0.000 claims description 18
- 240000006365 Vitis vinifera Species 0.000 claims description 18
- 235000014787 Vitis vinifera Nutrition 0.000 claims description 18
- 235000014687 Zingiber zerumbet Nutrition 0.000 claims description 18
- 235000013399 edible fruits Nutrition 0.000 claims description 18
- 238000009472 formulation Methods 0.000 claims description 18
- 239000000839 emulsion Substances 0.000 claims description 12
- 238000005507 spraying Methods 0.000 claims description 8
- 108010010803 Gelatin Proteins 0.000 claims description 7
- 229920002774 Maltodextrin Polymers 0.000 claims description 7
- 108010009736 Protein Hydrolysates Proteins 0.000 claims description 7
- 108010073771 Soybean Proteins Proteins 0.000 claims description 7
- 229930006000 Sucrose Natural products 0.000 claims description 7
- 238000004140 cleaning Methods 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 230000008030 elimination Effects 0.000 claims description 7
- 238000003379 elimination reaction Methods 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229920000159 gelatin Polymers 0.000 claims description 7
- 239000008273 gelatin Substances 0.000 claims description 7
- 235000019322 gelatine Nutrition 0.000 claims description 7
- 235000011852 gelatine desserts Nutrition 0.000 claims description 7
- 239000012535 impurity Substances 0.000 claims description 7
- 238000012805 post-processing Methods 0.000 claims description 7
- 239000003531 protein hydrolysate Substances 0.000 claims description 7
- 235000019710 soybean protein Nutrition 0.000 claims description 7
- 239000007921 spray Substances 0.000 claims description 7
- 239000005720 sucrose Substances 0.000 claims description 7
- -1 sucrose fatty ester Chemical class 0.000 claims description 7
- 108010059892 Cellulase Proteins 0.000 claims description 6
- 108091005804 Peptidases Proteins 0.000 claims description 6
- 239000004365 Protease Substances 0.000 claims description 6
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 229940106157 cellulase Drugs 0.000 claims description 6
- 239000012153 distilled water Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 239000005913 Maltodextrin Substances 0.000 claims description 4
- 229940035034 maltodextrin Drugs 0.000 claims description 4
- 230000000630 rising effect Effects 0.000 claims description 2
- 238000010008 shearing Methods 0.000 abstract description 2
- 244000269722 Thea sinensis Species 0.000 abstract 2
- 240000004875 Carya cathayensis Species 0.000 abstract 1
- 235000005663 Carya cathayensis Nutrition 0.000 abstract 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 abstract 1
- 235000005822 corn Nutrition 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 6
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 6
- 239000002253 acid Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 3
- 229930003427 Vitamin E Natural products 0.000 description 3
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 3
- 235000020778 linoleic acid Nutrition 0.000 description 3
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 235000019165 vitamin E Nutrition 0.000 description 3
- 229940046009 vitamin E Drugs 0.000 description 3
- 239000011709 vitamin E Substances 0.000 description 3
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 2
- 208000034189 Sclerosis Diseases 0.000 description 2
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 2
- 229930003316 Vitamin D Natural products 0.000 description 2
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 description 2
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 2
- 230000002605 anti-dotal effect Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 235000012000 cholesterol Nutrition 0.000 description 2
- 235000005687 corn oil Nutrition 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 150000002617 leukotrienes Chemical class 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 235000019155 vitamin A Nutrition 0.000 description 2
- 239000011719 vitamin A Substances 0.000 description 2
- 235000019166 vitamin D Nutrition 0.000 description 2
- 239000011710 vitamin D Substances 0.000 description 2
- 150000003710 vitamin D derivatives Chemical class 0.000 description 2
- 229940045997 vitamin a Drugs 0.000 description 2
- 229940046008 vitamin d Drugs 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 235000019495 Pecan oil Nutrition 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003026 anti-oxygenic effect Effects 0.000 description 1
- 210000001367 artery Anatomy 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000010470 pecan oil Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a multi-nutrient anti-ageing rice-bran-oil microcapsule. The raw materials of the microcapsule comprise rice bran, tea seed, carya cathayensis kernel, corn germ, carrot, tea leaf, rosemary, fructus lycii, herba asari, herba gynostemmatis pentaphylli, radix et caulis acanthopanacis senticosi, fructus tsaoko, radix glycyrrhizae, cortex acanthopanacis, cortex cinnamomi, a microcapsule wall material and an emulsifying agent. The invention also discloses a preparation method of the multi-nutrient anti-ageing rice-bran-oil microcapsule. The preparation method comprises performing raw-material processing and steam enzyme-killing processing on raw materials, then pouring the raw materials into first processing equipment, performing ultrasonic processing and enzymolysis, so as to obtain dissociate oil 1, a forth material and waste residue; pouring the forth material into second processing equipment, heating, and performing warm keeping and centrifugation, so as to obtain dissociate oil 2; then pouring dissociate oil 1 and dissociate oil 2 into third processing equipment, and performing dewaxing, degumming, depickling and decolouring, so as to obtain multi-nutrient anti-ageing rice-bran oil; and then mixing the multi-nutrient anti-ageing rice-bran oil, the microcapsule wall material and the emulsifying agent, shearing, and drying, so as to obtain the multi-nutrient anti-ageing rice-bran-oil microcapsule.
Description
Technical field
The present invention relates to vegetable oil technical field, particularly relate to anti-ageing rice bran oil micro-capsule of a kind of many nutrition and preparation method thereof.
Background technology
Rice bran is the byproduct of Rice producing, accounts for about 8% of paddy weight, and China is that big country is beaten in a paddy production, but most of rice bran is all used to use as feed, greatly wastes resource.Research shows, Rice Bran is worth abundant, the rice bran oil of being squeezed out by it is especially containing the abundant nutriment such as unrighted acid, leukotrienes, linoleic acid and liposoluble vitamin, phytosterol, oryzanol, often ediblely can reduce human cholesterol content, prevent artery sclerosis and anti-ageing.
The processing of rice bran oil is primarily of squeezing, solvent extraction and aqueous enzymatic extraction three kinds of modes; no matter which kind of mode all easily produces loss to the nutriment in rice bran oil; therefore; nutriment in the employing various ways protection of rice bran oil manufacturing and processing enterprise, interpolation rice bran oil is to strengthen the competitiveness of product, and effect is not but clearly.Trace it to its cause, although the nutriment in rice bran oil enriches, edible in a large number is also a kind of burden to human body, and the nutriment simultaneously in rice bran oil is very easily affected by the external environment, thus loses inherent value.How while raising rice bran oil edibility, prevent nutriment from losing, the problem that Ye Shi rice bran oil manufacturing and processing enterprise should consider.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes anti-ageing rice bran oil micro-capsule of a kind of many nutrition and preparation method thereof, the high and ratio uniform of unsaturated fatty acid content of the present invention, containing multiple nutrients, people's interior free yl can be eliminated, antidotal effect, be applicable to long-term edible.
The anti-ageing rice bran oil micro-capsule of the many nutrition of one that the present invention proposes, its raw material comprises 100 serving material K, 20-30 part micro-capsule wall material and 1-2 part emulsifying agents by weight;
Material K comprises by weight: rice bran 160-180 part, Seed of Camellia Sinensis 50-60 part, grape pip 45-50 part, hickory kernel 22-25 part, maize germ 17-20 part, carrot 15-18 part, tealeaves 12-15 part, rosemary 8-12 part, fruit of Chinese wolfberry 8-10 part, root of Chinese wild ginger 6-9 part, gynostemma pentaphylla 3-6 part, wilsonii 2-4 part, tsaoko 1-3 part, Radix Glycyrrhizae 1.5-2.5 part, cortex acanthopanacis 1-2 part, Chinese cassia tree 1-2 part.
Preferably, in material K, the weight ratio of rice bran, Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ is 170-175:55-58:46-48:23-24:18-19.
Preferably, in material K, the weight ratio of carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree is 16-17:13-14:9-10:8.5-9:7-8:4-5:2.5-3:1.5-2:1.8-2.2:1.5-1 .8:1.2-1.6.
Preferably, material K comprises by weight: rice bran 170-175 part, Seed of Camellia Sinensis 55-58 part, grape pip 46-48 part, hickory kernel 23-24 part, maize germ 18-19 part, carrot 16-17 part, tealeaves 13-14 part, rosemary 9-10 part, fruit of Chinese wolfberry 8.5-9 part, root of Chinese wild ginger 7-8 part, gynostemma pentaphylla 4-5 part, wilsonii 2.5-3 part, tsaoko 1.5-2 part, Radix Glycyrrhizae 1.8-2.2 part, cortex acanthopanacis 1.5-1.8 part, Chinese cassia tree 1.2-1.6 part.
Preferably, the preparation method of micro-capsule wall material is: in the 4th process equipment, add 10-15 part gelatin, 22-25 part soy bean protein hydrolysate, 50-60 part maltodextrin and 260-280 part distilled water by weight, raise the 4th process equipment and contents temperature thereof to 62-65 DEG C, insulation 12-15min obtains micro-capsule wall material.
Preferably, emulsifying agent comprises the single hard fatty acids glyceride of 0.1-0.3 part, 0.3-0.6 part sucrose fatty ester by weight.
The preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition that the present invention also proposes, comprises the steps:
S1, Feedstock treating: mix after Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 40-50 mesh sieve and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is 100-105 DEG C, and go out time of enzyme of steam is 40-50s;
S3, single treatment: obtain free oil 1,4 materials and waste residue by after the ultrasonic process of the second material, enzymolysis;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature thereof to 97-100 DEG C, and after insulation 30-35min, centrifugation obtains free oil 2;
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: anti-ageing for many nutrition rice bran oil, micro-capsule wall material, emulsifying agent are carried out mixing is sheared, drying obtains the anti-ageing rice bran oil micro-capsule of many nutrition.
Preferably, in S3, comprise the steps: A, ultrasonic process; B, enzymolysis.
Preferably, the process of steps A is: the second material and water are put into the first process vessel, then carries out ultrasonic process to material in the first process vessel and obtains 3 material, and the frequency of ultrasonic process is 55-60kHz, the power 450-550W of ultrasonic process, the time of ultrasonic process is 20-23min.
Preferably, the process of step B is: regulate 3 material pH value to 7.8-8.2, then adds complex enzyme formulation to containing in the first process vessel of 3 material, after stirring, leaves standstill 3.5-4.5h.
Preferably, in S3, the weight ratio of the second material, water and complex enzyme formulation is 100:600-800:4.
Preferably, complex enzyme formulation is made up of cellulase and alkali protease.
Preferably, in S6, comprise the steps: C, mixing shearing; D, spraying dry.
Preferably, the process of step C is: dropwise added by emulsifying agent in the anti-ageing rice bran oil of many nutrition and obtain oil emulsion, added by oil emulsion containing wall material to the 4th process equipment, then rising the 4th process equipment and contents temperature thereof are to 60-63 DEG C, after insulation 21-24min; Carry out emulsification pretreatment to the content of the 4th processing and obtain material after emulsification, the speed of emulsification pretreatment is 1.2 × 104-1.5 × 10
4r/min, the time of emulsification pretreatment is 55-60min.
Preferably, the process of step D is: spraying dry after material homogeneous after emulsification is obtained the anti-ageing rice bran oil micro-capsule of many nutrition, spray-dired EAT is 200-230 DEG C, and spray-dired leaving air temp is 76-80 DEG C.
The present invention adopts the rice bran of special ratios, Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ as oils raw material, use specific preparation method simultaneously, make the present invention based on rice bran oil, comprise Seed of Camellia Sinensis oil, grape-kernel oil, hickory kernel oil, maize germ oil simultaneously, significantly improve the content of unrighted acid in the present invention, optimize the ratio of unrighted acid of the present invention, make it be easy to absorb, reach the effect reducing blood fat performance, eliminate cholesterol, resist aging; Simultaneously, containing nutriments such as abundant oryzanol, phytosterol, vitamin E and tannin in Seed of Camellia Sinensis oil, grape-kernel oil, hickory kernel oil, maize germ oil, the nutriment loss of rice bran oil in process can be made up, increase the nutritional labeling in the present invention simultaneously, significantly improve the content of Middle nutrition material of the present invention; Wherein, Seed of Camellia Sinensis oil not only contains unrighted acid, the oleic acid of more than 80%, the linoleic acid of 10% up to more than 90%, simultaneously also containing the abundant nutriment such as vitamin A, vitamin D, cerebrovascular sclerosis can be prevented, reduce blood fat, anti-ageing; Then containing a large amount of linoleic acid in grape-kernel oil, effectively cholesterol level can be reduced; And pecan oil and maize germ oil contain abundant phytosterol and the abundant liposoluble vitamin such as vitamin E, vitamin A, vitamin D; Containing a large amount of lipid fractions matter in the carrot of adding, tealeaves, rosemary, antioxygenic property of the present invention can be strengthened on the one hand, extend the shelf-life of the present invention, eliminate people's interior free yl on the other hand, thus reach antidotal effect; The interpolation of the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, the effect have nourishing liver and kidney, reinforcement drag, Buzhong, delaying senility, greatly strengthen nutritional health function of the present invention; And tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree collocation use, make the present invention have the fragrance of levels are rich, improve edibility of the present invention.In preparation process, select the gelatin of special ratios, soy bean protein hydrolysate, maltodextrin as wall material, there is the features such as filming performance is good, embedding rate is high, viscosity is low, easy to digest, can available protecting the present invention before consumption not by ambient light, heat, wet to affect, thus improve effectiveness of the present invention; Emulsifying agent list hard fatty acids glyceride, sucrose fatty ester can effective emulsification rice bran oils, and under the effect of emulsification pretreatment, are evenly distributed among wall material; Drop is fully dry to select specific air intake, leaving air temp to ensure, prevents micro-capsule from getting damp again, and greatly improves embedding rate of the present invention and yield rate.
Accompanying drawing explanation
Fig. 1 is the process chart of the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition that the present invention proposes.
Detailed description of the invention
As shown in Figure 1, Fig. 1 is the process chart of the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition that the present invention proposes.
With reference to Fig. 1, the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition that the present invention proposes, comprises the steps:
S1, Feedstock treating: mix after Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 40-50 mesh sieve and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is 100-105 DEG C, and go out time of enzyme of steam is 40-50s;
S3, single treatment: obtain free oil 1,4 materials and waste residue by after the ultrasonic process of the second material, enzymolysis;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature thereof to 97-100 DEG C, and after insulation 30-35min, centrifugation obtains free oil 2;
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: anti-ageing for many nutrition rice bran oil, micro-capsule wall material, emulsifying agent are carried out mixing is sheared, drying obtains the anti-ageing rice bran oil micro-capsule of many nutrition.
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The anti-ageing rice bran oil micro-capsule of the many nutrition of one that the present invention proposes, its raw material comprises 100 serving material K, 20 parts of micro-capsule wall materials and 2 parts of emulsifying agents by weight;
Material K comprises by weight: 180 parts, rice bran, Seed of Camellia Sinensis 50 parts, grape pip 50 parts, hickory kernel 22 parts, maize germ 20 parts, 15 parts, carrot, tealeaves 15 parts, rosemary 8 parts, the fruit of Chinese wolfberry 10 parts, the root of Chinese wild ginger 6 parts, gynostemma pentaphylla 6 parts, wilsonii 2 parts, tsaoko 3 parts, 1.5 parts, Radix Glycyrrhizae, cortex acanthopanacis 2 parts, Chinese cassia tree 1 part; Emulsifying agent comprises 0.3 part of single hard fatty acids glyceride, 0.3 part of sucrose fatty ester by weight;
Wherein, the preparation method of micro-capsule wall material is: in the 4th process equipment, add 15 parts of gelatin, 22 parts of soy bean protein hydrolysates, 60 portions of maltodextrins and 260 parts of distilled water by weight, raise the 4th process equipment and contents temperature to 65 DEG C thereof, insulation 12min obtains micro-capsule wall material.
The invention allows for the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition, comprise the steps:
S1, Feedstock treating: mix after Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 50 mesh sieves and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is 100 DEG C, and go out time of enzyme of steam is 50s;
S3, single treatment: just the second material and water put into the first process vessel, then ultrasonic process is carried out to material in the first process vessel and obtain 3 material, the frequency of ultrasonic process is 55kHz, the power 550W of ultrasonic process, and the time of ultrasonic process is 20min; Then regulate 3 material pH value to 8.2, then add complex enzyme formulation to containing in the first process vessel of 3 material, after stirring, standing 3.5h obtains free oil 1,4 materials and waste residue; Wherein, the weight ratio of the second material, water and complex enzyme formulation is 100:800:4; Complex enzyme formulation is made up of cellulase and alkali protease;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature to 97 DEG C thereof, and after insulation 35min, centrifugation obtains free oil 2;
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: dropwise added by emulsifying agent in the anti-ageing rice bran oil of many nutrition and obtain oil emulsion, add containing wall material to the 4th process equipment by oil emulsion, then raise the 4th process equipment and contents temperature to 63 DEG C thereof, after insulation 21min; Carry out emulsification pretreatment to the content of the 4th processing and obtain material after emulsification, the speed of emulsification pretreatment is 1.5 × 10
4r/min, the time of emulsification pretreatment is 55min; Then spraying dry after material homogeneous after emulsification is obtained the anti-ageing rice bran oil micro-capsule of many nutrition, spray-dired EAT is 230 DEG C, and spray-dired leaving air temp is 76 DEG C.
Embodiment 2
The anti-ageing rice bran oil micro-capsule of the many nutrition of one that the present invention proposes, its raw material comprises 100 serving material K, 30 parts of micro-capsule wall materials and 1 part of emulsifying agent by weight;
Material K comprises by weight: 160 parts, rice bran, Seed of Camellia Sinensis 60 parts, grape pip 45 parts, hickory kernel 25 parts, maize germ 17 parts, 18 parts, carrot, tealeaves 12 parts, rosemary 12 parts, the fruit of Chinese wolfberry 8 parts, the root of Chinese wild ginger 9 parts, gynostemma pentaphylla 3 parts, wilsonii 4 parts, tsaoko 1 part, 2.5 parts, Radix Glycyrrhizae, cortex acanthopanacis 1 part, Chinese cassia tree 2 parts; Emulsifying agent comprises 0.1 part of single hard fatty acids glyceride, 0.6 part of sucrose fatty ester by weight;
The preparation method of micro-capsule wall material is: in the 4th process equipment, add 10 parts of gelatin, 25 parts of soy bean protein hydrolysates, 50 portions of maltodextrins and 280 parts of distilled water by weight, raise the 4th process equipment and contents temperature to 62 DEG C thereof, insulation 15min obtains micro-capsule wall material.
The invention allows for the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition, comprise the steps:
S1, Feedstock treating: mix after Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 40 mesh sieves and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is 105 DEG C, and go out time of enzyme of steam is 40s;
S3, single treatment: just the second material and water put into the first process vessel, then ultrasonic process is carried out to material in the first process vessel and obtain 3 material, the frequency of ultrasonic process is 60kHz, the power 450W of ultrasonic process, and the time of ultrasonic process is 23min; Then regulate 3 material pH value to 7.8, then add complex enzyme formulation to containing in the first process vessel of 3 material, after stirring, standing 4.5h obtains free oil 1,4 materials and waste residue; Wherein, the weight ratio of the second material, water and complex enzyme formulation is 100:600:4; Complex enzyme formulation is made up of cellulase and alkali protease;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature to 100 DEG C thereof, and after insulation 30min, centrifugation obtains free oil 2;
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: dropwise added by emulsifying agent in the anti-ageing rice bran oil of many nutrition and obtain oil emulsion, add containing wall material to the 4th process equipment by oil emulsion, then raise the 4th process equipment and contents temperature to 60 DEG C thereof, after insulation 24min; Carry out emulsification pretreatment to the content of the 4th processing and obtain material after emulsification, the speed of emulsification pretreatment is 1.2 × 10
4r/min, the time of emulsification pretreatment is 60min; Then spraying dry after material homogeneous after emulsification is obtained the anti-ageing rice bran oil micro-capsule of many nutrition, spray-dired EAT is 200 DEG C, and spray-dired leaving air temp is 80 DEG C.
Embodiment 3
The anti-ageing rice bran oil micro-capsule of the many nutrition of one that the present invention proposes, its raw material comprises 100 serving material K, 24 parts of micro-capsule wall materials and 1.2 parts of emulsifying agents by weight;
Material K comprises by weight: 175 parts, rice bran, Seed of Camellia Sinensis 55 parts, grape pip 48 parts, hickory kernel 23 parts, maize germ 19 parts, 16 parts, carrot, tealeaves 14 parts, rosemary 9 parts, the fruit of Chinese wolfberry 9 parts, the root of Chinese wild ginger 7 parts, gynostemma pentaphylla 5 parts, wilsonii 2.5 parts, tsaoko 2 parts, 1.8 parts, Radix Glycyrrhizae, cortex acanthopanacis 1.8 parts, Chinese cassia tree 1.2 parts; Emulsifying agent comprises 0.2 part of single hard fatty acids glyceride, 0.4 part of sucrose fatty ester by weight;
The preparation method of micro-capsule wall material is: in the 4th process equipment, add 12-13 part gelatin, 23-24 part soy bean protein hydrolysate, 54-58 part maltodextrin and 270-275 part distilled water by weight, raise the 4th process equipment and contents temperature thereof to 63-64 DEG C, insulation 13-14min obtains micro-capsule wall material.
The invention allows for the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition, comprise the steps:
S1, Feedstock treating: by Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves,
Mix after rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 50 mesh sieves and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is 102 DEG C, and go out time of enzyme of steam is 48s;
S3, single treatment: just the second material and water put into the first process vessel, then ultrasonic process is carried out to material in the first process vessel and obtain 3 material, the frequency of ultrasonic process is 56kHz, the power 520W of ultrasonic process, and the time of ultrasonic process is 22min; Then regulate 3 material pH value to 7.9, then add complex enzyme formulation to containing in the first process vessel of 3 material, after stirring, standing 4.2h obtains free oil 1,4 materials and waste residue; Wherein, the weight ratio of the second material, water and complex enzyme formulation is 100:660:4; Complex enzyme formulation is made up of cellulase and alkali protease;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature to 99 DEG C thereof, and after insulation 32min, centrifugation obtains free oil 2;
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: dropwise added by emulsifying agent in the anti-ageing rice bran oil of many nutrition and obtain oil emulsion, add containing wall material to the 4th process equipment by oil emulsion, then raise the 4th process equipment and contents temperature to 61 DEG C thereof, after insulation 23min; Carry out emulsification pretreatment to the content of the 4th processing and obtain material after emulsification, the speed of emulsification pretreatment is 1.3 × 10
4r/min, the time of emulsification pretreatment is 58min; Then spraying dry after material homogeneous after emulsification is obtained the anti-ageing rice bran oil micro-capsule of many nutrition, spray-dired EAT is 210 DEG C, and spray-dired leaving air temp is 78 DEG C.
Embodiment 4
The anti-ageing rice bran oil micro-capsule of the many nutrition of one that the present invention proposes, its raw material comprises 100 serving material K, 28 parts of micro-capsule wall materials and 1.4 parts of emulsifying agents by weight;
Material K comprises by weight: 170 parts, rice bran, Seed of Camellia Sinensis 58 parts, grape pip 46 parts, hickory kernel 24 parts, maize germ 18 parts, 17 parts, carrot, tealeaves 13 parts, rosemary 10 parts, the fruit of Chinese wolfberry 8.5 parts, the root of Chinese wild ginger 8 parts, gynostemma pentaphylla 4 parts, wilsonii 3 parts, tsaoko 1.5 parts, 2.2 parts, Radix Glycyrrhizae, cortex acanthopanacis 1.5 parts, Chinese cassia tree 1.6 parts; Emulsifying agent comprises 0.15 part of single hard fatty acids glyceride, 0.5 part of sucrose fatty ester by weight;
The preparation method of micro-capsule wall material is: in the 4th process equipment, add 12 parts of gelatin, 24 parts of soy bean protein hydrolysates, 54 portions of maltodextrins and 275 parts of distilled water by weight, raise the 4th process equipment and contents temperature to 63 DEG C thereof, insulation 14min obtains micro-capsule wall material.
The invention allows for the preparation method of the anti-ageing rice bran oil micro-capsule of a kind of many nutrition, comprise the steps:
S1, Feedstock treating: by Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves,
Mix after rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 40 mesh sieves and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is-103 DEG C, and go out time of enzyme of steam is 43s;
S3, single treatment: just the second material and water put into the first process vessel, then ultrasonic process is carried out to material in the first process vessel and obtain 3 material, the frequency of ultrasonic process is 58kHz, the power 480W of ultrasonic process, and the time of ultrasonic process is 21min; Then regulate 3 material pH value to 8.1, then add complex enzyme formulation to containing in the first process vessel of 3 material, after stirring, standing 3.8h obtains free oil 1,4 materials and waste residue; Wherein, the weight ratio of the second material, water and complex enzyme formulation is 100:740:4; Complex enzyme formulation is made up of cellulase and alkali protease;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature to 98 DEG C thereof, and after insulation 33min, centrifugation obtains free oil 2;
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: dropwise added by emulsifying agent in the anti-ageing rice bran oil of many nutrition and obtain oil emulsion, add containing wall material to the 4th process equipment by oil emulsion, then raise the 4th process equipment and contents temperature to 62 DEG C thereof, after insulation 22min; Carry out emulsification pretreatment to the content of the 4th processing and obtain material after emulsification, the speed of emulsification pretreatment is 1.4 × 10
4r/min, the time of emulsification pretreatment is 56min; Then spraying dry after material homogeneous after emulsification is obtained the anti-ageing rice bran oil micro-capsule of many nutrition, spray-dired EAT is 220 DEG C, and spray-dired leaving air temp is 77 DEG C.
Detect embodiment of the present invention 1-4, adopt commercially available rice bran oil micro-capsule as a control group, its result is as shown in the table:
| Test item | Embodiment 1-4 mean value | Control group |
| Linoleic acid, % | 57 | 44 |
| Leukotrienes, % | 5.1 | 2.6 |
| Content of vitamin E, mg/kg | 104.3 | 93.7 |
| Oryzanol content, % | 2.68 | 1.48 |
| Holding time, year | 3 | 1.5 |
The above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (10)
1. the anti-ageing rice bran oil micro-capsule of nutrition more than, is characterized in that, its raw material comprises 100 serving material K, 20-30 part micro-capsule wall material and 1-2 part emulsifying agents by weight;
Material K comprises by weight: rice bran 160-180 part, Seed of Camellia Sinensis 50-60 part, grape pip 45-50 part, hickory kernel 22-25 part, maize germ 17-20 part, carrot 15-18 part, tealeaves 12-15 part, rosemary 8-12 part, fruit of Chinese wolfberry 8-10 part, root of Chinese wild ginger 6-9 part, gynostemma pentaphylla 3-6 part, wilsonii 2-4 part, tsaoko 1-3 part, Radix Glycyrrhizae 1.5-2.5 part, cortex acanthopanacis 1-2 part, Chinese cassia tree 1-2 part.
2. the anti-ageing rice bran oil micro-capsule of many nutrition according to claim 1, is characterized in that, in material K, the weight ratio of rice bran, Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ is 170-175:55-58:46-48:23-24:18-19.
3. the anti-ageing rice bran oil micro-capsule of many nutrition according to claim 1 or 2, it is characterized in that, in material K, the weight ratio of carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree is 16-17:13-14:9-10:8.5-9:7-8:4-5:2.5-3:1.5-2:1.8-2.2:1.5-1 .8:1.2-1.6.
4. the anti-ageing rice bran oil micro-capsule of many nutrition according to any one of claim 1-3, it is characterized in that, material K comprises by weight: rice bran 170-175 part, Seed of Camellia Sinensis 55-58 part, grape pip 46-48 part, hickory kernel 23-24 part, maize germ 18-19 part, carrot 16-17 part, tealeaves 13-14 part, rosemary 9-10 part, fruit of Chinese wolfberry 8.5-9 part, root of Chinese wild ginger 7-8 part, gynostemma pentaphylla 4-5 part, wilsonii 2.5-3 part, tsaoko 1.5-2 part, Radix Glycyrrhizae 1.8-2.2 part, cortex acanthopanacis 1.5-1.8 part, Chinese cassia tree 1.2-1.6 part.
5. the anti-ageing rice bran oil micro-capsule of many nutrition according to any one of claim 1-4, it is characterized in that, the preparation method of micro-capsule wall material is: in the 4th process equipment, add 10-15 part gelatin, 22-25 part soy bean protein hydrolysate, 50-60 part maltodextrin and 260-280 part distilled water by weight, raise the 4th process equipment and contents temperature thereof to 62-65 DEG C, insulation 12-15min obtains micro-capsule wall material.
6. the anti-ageing rice bran oil micro-capsule of many nutrition according to any one of claim 1-5, is characterized in that, emulsifying agent comprises the single hard fatty acids glyceride of 0.1-0.3 part, 0.3-0.6 part sucrose fatty ester by weight.
7. the preparation method of the anti-ageing rice bran oil micro-capsule of many nutrition as described in any one of claim 1-6, is characterized in that, comprise the steps:
S1, Feedstock treating: mix after Seed of Camellia Sinensis, grape pip, hickory kernel, maize germ, carrot, tealeaves, rosemary, the fruit of Chinese wolfberry, the root of Chinese wild ginger, gynostemma pentaphylla, wilsonii, tsaoko, Radix Glycyrrhizae, cortex acanthopanacis, Chinese cassia tree cleaning impurity elimination, pulverize, cross 40-50 mesh sieve and obtain mixed material, with Water spray wet mix material, leave standstill and obtain the first material;
S2, steam go out ferment treatment: carry out the steam ferment treatment that goes out to the first material and obtain the second material, and the go out temperature of enzyme of steam is 100-105 DEG C, and go out time of enzyme of steam is 40-50s;
S3, single treatment: obtain free oil 1,4 materials and waste residue by after the ultrasonic process of the second material, enzymolysis;
S4, after-treatment: 4 materials is dropped into the second process equipment, raise the second process equipment and contents temperature thereof to 97-100 DEG C, and after insulation 30-35min, centrifugation obtains free oil 2.
S5, post processing: free oil 1, free oil 2 are dropped into the 3rd process equipment, dewaxing, comes unstuck, depickling, and decolouring obtains the anti-ageing rice bran oil of many nutrition;
S6, microencapsulation: anti-ageing for many nutrition rice bran oil, micro-capsule wall material, emulsifying agent are carried out mixing is sheared, drying obtains the anti-ageing rice bran oil micro-capsule of many nutrition.
8. the preparation method of the anti-ageing rice bran oil micro-capsule of many nutrition according to claim 7, is characterized in that, in S3, comprise the steps: A, ultrasonic process; B, enzymolysis;
Preferably, the process of steps A is: the second material and water are put into the first process vessel, then carries out ultrasonic process to material in the first process vessel and obtains 3 material, and the frequency of ultrasonic process is 55-60kHz, the power 450-550W of ultrasonic process, the time of ultrasonic process is 20-23min;
Preferably, the process of step B is: regulate 3 material pH value to 7.8-8.2, then adds complex enzyme formulation to containing in the first process vessel of 3 material, after stirring, leaves standstill 3.5-4.5h.
9. the preparation method of the anti-ageing rice bran oil micro-capsule of many nutrition according to any one of claim 5-8, it is characterized in that, in S3, the weight ratio of the second material, water and complex enzyme formulation is 100:600-800:4; Preferably, complex enzyme formulation is made up of cellulase and alkali protease.
10. the preparation method of the anti-ageing rice bran oil micro-capsule of many nutrition according to any one of claim 5-9, is characterized in that, in S6, comprises the steps: C, mixing shears; D, spraying dry;
Preferably, the process of step C is: dropwise added by emulsifying agent in the anti-ageing rice bran oil of many nutrition and obtain oil emulsion, added by oil emulsion containing wall material to the 4th process equipment, then rising the 4th process equipment and contents temperature thereof are to 60-63 DEG C, after insulation 21-24min; Carry out emulsification pretreatment to the content of the 4th processing and obtain material after emulsification, the speed of emulsification pretreatment is 1.2 × 10
4-1.5 × 10
4r/min, the time of emulsification pretreatment is 55-60min;
Preferably, the process of step D is: spraying dry after material homogeneous after emulsification is obtained the anti-ageing rice bran oil micro-capsule of many nutrition, spray-dired EAT is 200-230 DEG C, and spray-dired leaving air temp is 76-80 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510368944.9A CN105124594A (en) | 2015-06-26 | 2015-06-26 | Multi-nutrient anti-ageing rice-bran-oil microcapsule and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510368944.9A CN105124594A (en) | 2015-06-26 | 2015-06-26 | Multi-nutrient anti-ageing rice-bran-oil microcapsule and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105124594A true CN105124594A (en) | 2015-12-09 |
Family
ID=54710471
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510368944.9A Pending CN105124594A (en) | 2015-06-26 | 2015-06-26 | Multi-nutrient anti-ageing rice-bran-oil microcapsule and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105124594A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108902361A (en) * | 2018-08-04 | 2018-11-30 | 望江县振兴植物油厂（普通合伙） | A kind of preparation method of health care ready-mixed oil |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1739368A (en) * | 2005-07-27 | 2006-03-01 | 山东新良油脂有限公司 | Vitamin-rich nutritive vegetable oil and its prepn process |
| CN101279049A (en) * | 2007-04-06 | 2008-10-08 | 王洪飞 | Soft capsules for resisting altitude stress |
| CN102206542A (en) * | 2011-01-30 | 2011-10-05 | 山东西王食品有限公司 | Method for preparing maize germ oil through enzymatic degumming |
| CN102239933A (en) * | 2011-06-23 | 2011-11-16 | 中国农业科学院油料作物研究所 | Family balance formula oil and preparation method thereof |
| CN102488026A (en) * | 2011-11-24 | 2012-06-13 | 西华大学 | Manufacturing method of composite oil dispersible powder |
| CN103254989A (en) * | 2012-02-15 | 2013-08-21 | 河源市绿康生态农业科技有限公司 | Method for extraction of tea seed oil by ultrasound-assisted enzymatic process |
| CN104190334A (en) * | 2014-09-05 | 2014-12-10 | 南京泽朗生物科技有限公司 | Method for preparing mikania micrantha volatile oil microcapsules |
-
2015
- 2015-06-26 CN CN201510368944.9A patent/CN105124594A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1739368A (en) * | 2005-07-27 | 2006-03-01 | 山东新良油脂有限公司 | Vitamin-rich nutritive vegetable oil and its prepn process |
| CN101279049A (en) * | 2007-04-06 | 2008-10-08 | 王洪飞 | Soft capsules for resisting altitude stress |
| CN102206542A (en) * | 2011-01-30 | 2011-10-05 | 山东西王食品有限公司 | Method for preparing maize germ oil through enzymatic degumming |
| CN102239933A (en) * | 2011-06-23 | 2011-11-16 | 中国农业科学院油料作物研究所 | Family balance formula oil and preparation method thereof |
| CN102488026A (en) * | 2011-11-24 | 2012-06-13 | 西华大学 | Manufacturing method of composite oil dispersible powder |
| CN103254989A (en) * | 2012-02-15 | 2013-08-21 | 河源市绿康生态农业科技有限公司 | Method for extraction of tea seed oil by ultrasound-assisted enzymatic process |
| CN104190334A (en) * | 2014-09-05 | 2014-12-10 | 南京泽朗生物科技有限公司 | Method for preparing mikania micrantha volatile oil microcapsules |
Non-Patent Citations (5)
| Title |
|---|
| 刘春光: "香辛料的应用现状及存在问题", 《中国调味品》 * |
| 刘燕 等: "天然抗氧化剂的研究现状", 《粮油加工》 * |
| 史素伟 等: "米糠油微胶囊产品的制备及其稳定性研究", 《食品科技》 * |
| 夏文水: "《食品工艺学》", 31 January 2007, 中国轻工业出版社 * |
| 梅蒙: "抗缺氧中药的研究现状", 《云南中医中药杂志》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108902361A (en) * | 2018-08-04 | 2018-11-30 | 望江县振兴植物油厂（普通合伙） | A kind of preparation method of health care ready-mixed oil |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103609753B (en) | A kind of polynary nutritious vegetable oil and preparation method thereof | |
| CN101455243B (en) | Edible mixed oil containing highland barley bran oil | |
| CN100427576C (en) | Extraction of hickory nut oil from water enzyme | |
| CN1709090A (en) | Camellia oil micro capsule, and its preparing method and use | |
| CN105942525A (en) | Olive oil microcapsule powder and preparation method thereof | |
| CN104982558A (en) | Novel camellia oil microcapsule powder and preparation method thereof | |
| CN105331438A (en) | Method for preparing rapeseed oil by using semi-solid aqueous enzymatic method | |
| CN103651942B (en) | The preparation method of the rare cream of natural plants, plant dilute cream and defatted vegetable protein matter powder | |
| CN103815395A (en) | Propolis-safflower oil soft capsule and preparation method thereof | |
| CN105996028A (en) | Ginger extract, ginger fiber and preparation method of ginger extract and ginger fiber | |
| CN104771347A (en) | Eye cream and preparation method thereof | |
| CN107286068B (en) | A method of preparing lutein crystal oil suspending agent | |
| CN104450170A (en) | Nutrition and health anticancer rapeseed oil | |
| CN105124594A (en) | Multi-nutrient anti-ageing rice-bran-oil microcapsule and preparation method thereof | |
| CN104970114A (en) | High nutrition antioxidant compound rice bran oil and preparation method thereof | |
| CN104095081B (en) | A kind of seed of Flos Moutan mixed oil of rich in vitamin E and preparation method thereof | |
| CN105685262A (en) | Edible canola oil microcapsule and preparation method thereof | |
| CN102907603B (en) | Composite micro-capsule powder containing badam extractive and preparation method of composite micro-capsule powder | |
| CN104726276A (en) | Method for brewing low-alcohol lily wine | |
| CN106387098A (en) | Healthy nutritive vegetable oil | |
| CN103766732A (en) | Peanut rice cake and processing method thereof | |
| CN105941663A (en) | Grease composition with blood fat reducing function | |
| CN106234652A (en) | A kind of vegetable oil composition balanced in nutrition | |
| CN104886267A (en) | Rice bran crude oil with high nutritive value and preparation method of rice bran crude oil | |
| CN104522666A (en) | Dahurian rose fruit seed oil and purple perilla seed oil composite microcapsule capable of assisting in reducing blood fat and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151209 |
|
| RJ01 | Rejection of invention patent application after publication |