CN1709090A - Camellia oil micro capsule, and its preparing method and use - Google Patents
Camellia oil micro capsule, and its preparing method and use Download PDFInfo
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- CN1709090A CN1709090A CNA2005100506334A CN200510050633A CN1709090A CN 1709090 A CN1709090 A CN 1709090A CN A2005100506334 A CNA2005100506334 A CN A2005100506334A CN 200510050633 A CN200510050633 A CN 200510050633A CN 1709090 A CN1709090 A CN 1709090A
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- 239000010495 camellia oil Substances 0.000 title claims abstract description 51
- 239000003094 microcapsule Substances 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- -1 sucrose fatty ester compound Chemical class 0.000 claims abstract description 19
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229930006000 Sucrose Natural products 0.000 claims abstract description 17
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 17
- 239000005720 sucrose Substances 0.000 claims abstract description 17
- 238000002360 preparation method Methods 0.000 claims abstract description 11
- 239000003814 drug Substances 0.000 claims abstract description 4
- 235000013373 food additive Nutrition 0.000 claims abstract description 4
- 239000002778 food additive Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 33
- 239000005913 Maltodextrin Substances 0.000 claims description 16
- 229920002774 Maltodextrin Polymers 0.000 claims description 16
- 229920002472 Starch Polymers 0.000 claims description 16
- 229940035034 maltodextrin Drugs 0.000 claims description 16
- 239000008107 starch Substances 0.000 claims description 16
- 235000019698 starch Nutrition 0.000 claims description 16
- 239000008187 granular material Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000001694 spray drying Methods 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 6
- 239000000839 emulsion Substances 0.000 claims description 5
- 235000008098 Oxalis acetosella Nutrition 0.000 claims description 3
- 235000010240 Paullinia pinnata Nutrition 0.000 claims description 3
- 235000013402 health food Nutrition 0.000 claims description 3
- 241001119522 Paullinia pinnata Species 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 2
- 229920000858 Cyclodextrin Polymers 0.000 abstract 1
- 229920001353 Dextrin Polymers 0.000 abstract 1
- 239000004375 Dextrin Substances 0.000 abstract 1
- 239000001116 FEMA 4028 Substances 0.000 abstract 1
- 229920000881 Modified starch Polymers 0.000 abstract 1
- 239000004368 Modified starch Substances 0.000 abstract 1
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 abstract 1
- 239000003674 animal food additive Substances 0.000 abstract 1
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 abstract 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 abstract 1
- 229960004853 betadex Drugs 0.000 abstract 1
- 235000019425 dextrin Nutrition 0.000 abstract 1
- 235000019426 modified starch Nutrition 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 44
- 239000003921 oil Substances 0.000 description 12
- 235000019198 oils Nutrition 0.000 description 12
- 239000011259 mixed solution Substances 0.000 description 10
- 239000000047 product Substances 0.000 description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000000284 extract Substances 0.000 description 4
- 239000004006 olive oil Substances 0.000 description 4
- 235000008390 olive oil Nutrition 0.000 description 4
- 235000018597 common camellia Nutrition 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 2
- 241000209507 Camellia Species 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 2
- 241001119526 Paullinia Species 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 210000004204 blood vessel Anatomy 0.000 description 2
- 208000026106 cerebrovascular disease Diseases 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 239000008157 edible vegetable oil Substances 0.000 description 2
- 230000002526 effect on cardiovascular system Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- DPUOLQHDNGRHBS-UHFFFAOYSA-N Brassidinsaeure Natural products CCCCCCCCC=CCCCCCCCCCCCC(O)=O DPUOLQHDNGRHBS-UHFFFAOYSA-N 0.000 description 1
- 240000001548 Camellia japonica Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- URXZXNYJPAJJOQ-UHFFFAOYSA-N Erucic acid Natural products CCCCCCC=CCCCCCCCCCCCC(O)=O URXZXNYJPAJJOQ-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- DPUOLQHDNGRHBS-KTKRTIGZSA-N erucic acid Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(O)=O DPUOLQHDNGRHBS-KTKRTIGZSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 239000008141 laxative Substances 0.000 description 1
- 230000002475 laxative effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000021281 monounsaturated fatty acids Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Landscapes
- Medicinal Preparation (AREA)
- General Preparation And Processing Of Foods (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Cosmetics (AREA)
Abstract
The present invention discloses a camellia oil microcapsule, its preparation method and application. Said camellia oil microcapsule (by 1000g prescription raw material) contains 20-90g of beta-cyclodextrin, 130-244g of malt dextrin, 6-14g of modified starch, 2-6g of monoglyceride and sucrose fatty ester compound emulsifying agent, 40-90g of camellia oil and the rest is water. Said camellia oil microcapsule can be used as general food, health-care food, medicine, food additive and feed additive. Besides, said invention also provides the concrete steps of its preparation method.
Description
Technical field
The present invention relates to a kind of camellia oil micro capsule and its production and use.
Background technology
Camellia oil (claims camellia seed oil again, tea oil, Camellia oil) be that the Theaceae with China's special product, the ripe kernel of Camellia (Camellia) plant squeeze a kind of woody edible vegetable oil that obtains, contain monounsaturated fatty acids oleic acid more than 80%, be rich in polyunsaturated fatty acid linoleic acid, leukotrienes of needed by human etc., aliphatic acid is formed similar to olive oil, is similarly the high-quality edible oil with olive oil, is described as the east olive oil.In addition, camellia oil contains the active component that lacks in the olive oil such as micro-camellin, Tsubaki-saponin, Tea Polyphenols, also contains vitamin E, various trace elements, and its one-tenth is grouped into the nutritional need that meets very much human body, is absorbed by the body easily, does not contain erucic acid.Often edible camellia oil has the reduction blood fat, strengthens blood vessel elasticity and toughness, raising immunity, prevention cardiovascular and cerebrovascular disease, anti-ageing, improves looks, promotes nutrition health-care functions such as baby and children's growth.
Camellia oil has only through deodorization, filtration, ungrease treatment at present as a kind of consumable products, and traditional inner wrapping (as barreled) refined oil form for cooking is not seen the other products listing as yet, and application surface is narrow.Become sour by the oxidation of airborne oxygen institute but two keys of the unrighted acid in refining camellia oil are easier, influence the shelf-life.As the edible health-care oil that is rich in unrighted acid, the best edible way of camellia oil is to avoid high-temperature cooking, direct oral drinking, but owing to reasons such as custom and mouthfeels, this mode generally can not be accepted by consumers in general.
Summary of the invention
The purpose of this invention is to provide a kind of camellia oil micro capsule and its production and use.
The formula material of camellia oil micro capsule contains beta-schardinger dextrin-20～90g, maltodextrin 130～244g, converted starch 6～14g, monoglyceride and sucrose fatty ester compound emulsifying agent 2～6g in 1000g, camellia oil 40～90g, and surplus is a water.The preparation method's of camellia oil micro capsule step is as follows:
1) beta-schardinger dextrin-and the water of 20～90g are put into container, be heated to 80～90 ℃, constantly stirring makes it dissolving, adds 130～244g maltodextrin then and continues to stir, and stops heating after treating to dissolve fully, naturally cools to 40～60 ℃, gets a solution;
2) converted starch, monoglyceride and sucrose fatty ester compound emulsifying agent 2～6g, the water of 6～14g are put into container, be heated to 40～60 ℃, stir, add 40～90g camellia oil then, stop heating after continuing to stir, get b solution;
3) adopt cutter that a solution is sheared under 3000～5000rpm, slowly add b solution simultaneously, treat that b solution adds after, at 5000～8000rpm down cut, 5～8min, emulsion c;
4) adopting high-pressure homogeneous equipment is homogeneous 2～3 times under 15～25MPa with above-mentioned emulsion c at pressure, each homogeneous 3～5min;
5) cooling of the mixed liquor homogeneous crossed is that 160～195 ℃, leaving air temp are to carry out spray-drying under 90～110 ℃ of conditions at EAT then, is processed into microcapsule granule.
Camellia oil micro capsule is used for bread and cheese, health food, medicine, food additives, feed addictive.
Technology simple possible of the present invention, prepared camellia oil micro capsule is a kind of powder, embedding rate is more than 80%, has good flowability, wherein camellia oil and extraneous air can be separated, avoid the oxidation of unrighted acid in the camellia oil, can prolong the holding time of camellia oil effectively; Microcapsules employing edibility raw material can directly eat as the wall material, thereby has made things convenient for the use of camellia oil.
The specific embodiment
The present invention is by adopting the wall material of some suitable materials as microcapsules, it is middle as core then camellia oil to be wrapped in the wall material, be made into microcapsule granule by spray drying process at last, the air of camellia oil and outside is separated, avoid the generation of oxidation, thereby reach long preservation camellia oil and the convenient purpose of using, can be used for oral liquid, pulvis, tablet, capsule etc.Because this product has the reduction blood fat, strengthen blood vessel elasticity and toughness, improve immunity, prevention cardiovascular and cerebrovascular disease, anti-ageing, beauty treatment, promote effects such as baby and children's growth, can be used for bread and cheese (as beverage, instant food, powder, cake product etc.), health food, food additives, medicine, feed and other products.
The invention will be further elaborated by the following examples.
Embodiment 1:
Get beta-schardinger dextrin-90g, maltodextrin 190g, converted starch 14g, monoglyceride and sucrose fatty ester compound emulsifying agent 6g, camellia oil 65g, water 635g.
Preparation method: get beta-schardinger dextrin-90g and water 500g puts into the A container, be heated to 90 ℃, constantly stir and make it to be dissolved to solution and be transparence, adding maltodextrin 190g then continues to stir, stop heating after treating to dissolve fully, naturally cool to 60 ℃, get A solution.Other gets the B container, adds converted starch 14g, monoglyceride+sucrose fatty ester compound emulsifying agent 6g, water 135g, is heated to 60 ℃, stirs, and adds camellia oil 65g then, stirs, and as core, this is a B solution.Adopt cutter that A solution is sheared under 3000rpm, slowly add b solution simultaneously, treat that B solution adds after, at 6000rpm down cut 5min, C solution.Adopt high-pressure homogeneous equipment with above-mentioned C solution homogeneous three times under 20MPa pressure, each homogeneous 5min.The mixed liquor that homogeneous is crossed is 0.185 mPas with NDJ-8S digital display viscometer determining viscosity under 25 ℃; The emulsion sampling is moved in the centrifuge tube, and under the 3000rpm condition, centrifugal 15min does not see profit layering and tangible sediment, promptly has good stable.Naturally placing cooling, is that 185 ℃, leaving air temp are 100 ℃ at EAT then, and air draught rate 85% is carried out spray-drying under flow 22% condition, is processed into the microcapsules milky white granules.The gained microcapsules have good flowability and palatability, reconstitute with the boiling water that is higher than 70 ℃, observe reconstituting performance, dash the back slightly through stirring, and can be dissolved in immediately in the aqueous solution, form uniform milky white solution, no floating oil.
The mensuration of microcapsules sample embedding rate:, extract total oil, surface oil by laxative remedy to the sampling of gained microcapsule granule:
(1) surface oil of microcapsule product extracts: accurately take by weighing camellia oil micro capsule (W
1About 2g) to dry triangular flask (W
2) in, adding the 20ml benzinum, vibration 10min is with the filter paper (W of known weight
3) filter, use 10ml petroleum ether twice again, triangular flask and filter paper are moved in 60 ℃ of baking ovens, (W dries to constant weight
4).Surface oil content=(W
1+ W
2+ W
3-W
4)/W
1* 100%, (
(2) extraction of the total oil of microcapsule product: accurately take by weighing camellia oil micro capsule (W
1, about 2g) and to dry triangular flask, add the 20ml hot distilled water, after sample is fully dissolved, add absolute ethyl alcohol, absolute ether, benzinum (volume ratio is 2: 1: 1) extraction camellia oil successively, re-extract three times extracts supernatant liquor in the dry small beaker (W that has weighed
2) in, solvent evaporated in water-bath moves in 60 ℃ of baking ovens again, and (W dries to constant weight
3).Total oil content=(W
3-W
2)/W
11* 100%
Be calculated as follows the microencapsulation embedding rate then:
Microencapsulation embedding rate=[total oil content-surface oil content/total oil content] * 100%
To camellia oil micro capsule sample embedding rate measurement result, by embedding camellia oil content 〉=15%, embedding rate 〉=85% by above-mentioned prescription, technology preparation.
Embodiment 2:
Get beta-schardinger dextrin-75g, maltodextrin 160g, converted starch 9g, monoglyceride and sucrose fatty ester compound emulsifying agent 3g, camellia oil 53g, water 700g.
The preparation method: get beta-schardinger dextrin-75g and water 500g puts into the A container, be heated to 80 ℃, constantly stir and make it dissolving, add maltodextrin 160g then and continue to stir, stop heating after treating to dissolve fully, naturally cool to 50 ℃, A solution.Other gets the B container, adds converted starch 9g, monoglyceride and sucrose fatty ester compound emulsifying agent 3g, water 200g, is heated to 60 ℃, stirs, and temperature adds the 53g camellia oil after reducing to room temperature, stirs, and this is a B solution.Adopt cutter that A solution is sheared under 4000rpm, slowly add b solution simultaneously, treat that B solution adds after, at 8000rpm down cut 3min, mixed solution C.Adopt high-pressure homogeneous equipment with above-mentioned C solution homogeneous three times under 20MPa pressure, each homogeneous 3min.The mixed solution C that homogeneous is crossed is placed cooling naturally, is 180 ℃ at EAT then, and leaving air temp is 110 ℃, and air draught rate 85% is carried out spray-drying under flow 14% condition, is processed into microcapsule granule.
Embodiment 3:
Get beta-schardinger dextrin-58g, maltodextrin 130g, converted starch 9g, monoglyceride and sucrose fatty ester compound emulsifying agent 3g, camellia oil 40g, water 660g.
The preparation method: get beta-schardinger dextrin-58g and water 500g puts into the A container, be heated to 85 ℃, constantly stir and make it dissolving, add maltodextrin 130g then and continue to stir, stop heating after treating to dissolve fully, naturally cool to 40 ℃, A solution.Other gets the B container, adds converted starch 9g, monoglyceride and sucrose fatty ester compound emulsifying agent 3g, water 160g, is heated to 70 ℃, stirs, and adds camellia oil 40g then, stirs, and as core, this is a B solution.Adopt cutter that A solution is sheared under 4000rpm, slowly add b solution simultaneously, treat that B solution adds after, at 7000rpm down cut 4min, mixed solution C.Adopt high-pressure homogeneous equipment with above-mentioned C solution homogeneous secondary, pressure is 25MPa for the first time, and pressure is 15MPa for the second time, each homogeneous 5min.The mixed solution C that homogeneous is crossed is placed cooling naturally, is that 195 ℃, leaving air temp are 105 ℃, air draught rate 85% at EAT then, carries out spray-drying under flow 20% condition, is processed into microcapsule granule.
Embodiment 4:
Get beta-schardinger dextrin-30g, maltodextrin 168g, converted starch 9g, monoglyceride and sucrose fatty ester compound emulsifying agent 3g, camellia oil 90g, water 700g.
The preparation method: get beta-schardinger dextrin-30g and water 500g puts into the A container, be heated to 80 ℃, constantly stir and make it dissolving, add maltodextrin 168g then and continue to stir, stop heating after treating to dissolve fully, naturally cool to 40 ℃, A solution.Other gets the B container, adds converted starch 9g, monoglyceride and sucrose fatty ester compound emulsifying agent 3g, water 200g, is heated to 70 ℃, stirs, and adds camellia oil 90g then, stirs, and as core, this is a B solution.Adopt cutter that A solution is sheared under 4000rpm, slowly add b solution simultaneously, treat that B solution adds after, at 5000rpm down cut 8min, mixed solution C.Adopt high-pressure homogeneous equipment with above-mentioned C solution homogeneous secondary, pressure is 25MPa for the first time, and pressure is 15MPa for the second time, each homogeneous 5min.The mixed solution C that homogeneous is crossed is placed cooling naturally, is that 195 ℃, leaving air temp are 105 ℃, air draught rate 88% at EAT then, carries out spray-drying under flow 18% condition, is processed into microcapsule granule.
Embodiment 5:
Get beta-schardinger dextrin-40g, maltodextrin 244g, converted starch 12g, monoglyceride and sucrose fatty ester compound emulsifying agent 4g, camellia oil 80g, water 620g.
The preparation method: get beta-schardinger dextrin-40g and water 500g puts into the A container, be heated to 85 ℃, constantly stir and make it dissolving, add maltodextrin 244g then and continue to stir, stop heating after treating to dissolve fully, naturally cool to 50 ℃, A solution.Other gets the B container, adds converted starch 12g, monoglyceride and sucrose fatty ester compound emulsifying agent 4g, water 120g, is heated to 70 ℃, stirs, and adds camellia oil 80g then, stirs, and as core, this is a B solution.Adopt cutter that A solution is sheared under 3000rpm, slowly add b solution simultaneously, treat that B solution adds after, at 7000rpm down cut 5min, mixed solution C.Adopt high-pressure homogeneous equipment with above-mentioned C solution homogeneous secondary, pressure is 25MPa for the first time, and pressure is 15MPa for the second time, each homogeneous 5min.The mixed solution C that homogeneous is crossed is placed cooling naturally, is that 185 ℃, leaving air temp are 105 ℃, air draught rate 88% at EAT then, carries out spray-drying under flow 14% condition, is processed into microcapsule granule.
Embodiment 6:
Get beta-schardinger dextrin-20g, maltodextrin 172g, converted starch 6g, monoglyceride and sucrose fatty ester compound emulsifying agent 2g, camellia oil 60g, water 740g.
The preparation method: get beta-schardinger dextrin-20g and water 500g puts into the A container, be heated to 90 ℃, constantly stir and make it dissolving, add maltodextrin 172g then and continue to stir, stop heating after treating to dissolve fully, naturally cool to 60 ℃, A solution.Other gets the B container, adds converted starch 6g, monoglyceride and sucrose fatty ester compound emulsifying agent 2g, water 160g, is heated to 70 ℃, stirs, and adds camellia oil 60g then, stirs, and as core, this is a B solution.Adopt cutter that A solution is sheared under 4000rpm, slowly add b solution simultaneously, treat that B solution adds after, at 8000rpm down cut 4min, mixed solution C.Adopt high-pressure homogeneous equipment with above-mentioned C solution homogeneous secondary, pressure is 25MPa for the first time, and pressure is 15MPa for the second time, each homogeneous 5min.The mixed solution C that homogeneous is crossed is placed cooling naturally, is that 160 ℃, leaving air temp are 90 ℃, air draught rate 88% at EAT then, carries out spray-drying under flow 20% condition, is processed into microcapsule granule.
Claims (3)
1. camellia oil micro capsule, it is characterized in that,, contain beta-schardinger dextrin-20～90g, maltodextrin 130～244g, converted starch 6～14g, monoglyceride and sucrose fatty ester compound emulsifying agent 2～6g in the 1000g formula material, camellia oil 40～90g, surplus is a water.
2. the preparation method of a camellia oil micro capsule as claimed in claim 1 is characterized in that, the step of method is as follows:
1) beta-schardinger dextrin-and the water of 20～90g are put into container, be heated to 80～90 ℃, constantly stirring makes it dissolving, adds 130～244g maltodextrin then and continues to stir, and stops heating after treating to dissolve fully, naturally cools to 40～60 ℃, gets a solution;
2) converted starch, monoglyceride and the sucrose fatty ester compound emulsifying agent 2～6g water of 6～14g are put into container, be heated to 40～60 ℃, stir, add 40～90g camellia oil then, stop heating after continuing to stir, get b solution;
3) adopt cutter that a solution is sheared under 3000～5000rpm, slowly add b solution simultaneously, treat that b solution adds after, at 5000～8000rpm down cut, 5～8min, emulsion c;
4) adopting high-pressure homogeneous equipment is homogeneous 2～3 times under 15～25MPa with above-mentioned emulsion c at pressure, each homogeneous 3～5min;
5) cooling of the mixed liquor homogeneous crossed is that 160～195 ℃, leaving air temp are to carry out spray-drying under 90～110 ℃ of conditions at EAT then, is processed into microcapsule granule.
3. the purposes of a camellia oil micro capsule as claimed in claim 1, it is characterized in that: it is used for bread and cheese, health food, medicine, food additives, feed addictive.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100506334A CN1295970C (en) | 2005-07-08 | 2005-07-08 | Camellia oil micro capsule, and its preparing method and use |
Applications Claiming Priority (1)
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