CN105010574A - Novel linseed oil /grape seed oil /camellia oil microcapsule powder and preparation method thereof - Google Patents
Novel linseed oil /grape seed oil /camellia oil microcapsule powder and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of food processing, and particularly relates to novel linseed oil /grape seed oil /camellia oil microcapsule powder and a preparation method thereof. The novel linseed oil /grape seed oil /camellia oil microcapsule powder is prepared through the steps: using linseed oil, grape seed oil, and camellia oil which are uniformly mixed according to a certain proportion as a core material, performing oil phase preparation, performing aqueous phase preparation, performing emulsification on the core material after oil phase preparation and aqueous phase preparation, homogenizing the emulsified core material, and spray drying the homogenized core material. The linseed oil /grape seed oil /camellia oil microcapsule powder is balanced in the nutrition of unsaturated fatty acid, good in taste, high in embedding rate, high in stability, high in antioxidant ability, and high in absorptivity; air is insulated, so that the unsaturated fatty acid is protected, and the microcapsule powder is convenient to eat. The microcapsule powder and the preparation method thereof, disclosed by the invention, are convenient for mass production, and provide an effective and simple-to-eat manner for balancing the unsaturated fatty acid of human bodies.
Description
Technical field
The invention belongs to food processing technology field, relate to a kind of novel linseed oil, grape-kernel oil, camellia oil microcapsule powder and preparation method thereof.
Background technology
Linseed (flaxseed & linseed) is commonly called as flaxseed, is the seed of herbaceous plant flax.Material containing various useful health in linseed body.Linseed contains abundant grease and protein, and the content of dietary fibre, mineral matter, lignan, lecithin and the nutritional labeling such as vitamin A, B, D, E is also higher.Linseed oil is produced by linseed, wherein the content of unrighted acid accounts for 91% of primary fat acid content, the content of omega-fatty acid is up to 49%, and omega-fatty acid is alpha-linolenic acid, EPA (eicosapentaenoic acid) and DHA (DHA) mainly.Alpha-linolenic acid has reducing blood lipid and hypotensive, strengthens autoimmunity, prevention diabetes, the effects such as antiatherosclerosis, anti-inflammatory, anti-malignant tumor, anti-senile dementia and cosmetic slimming.Alpha-linolenic acid is the precursor substance of EPA and DHA simultaneously, EPA can help the content reducing cholesterol and triglycerides, promote saturated fat acid metabolic in body, reduce blood viscosity, promote blood circulation, improve and organize oxygen supply and dispelling fatigue, prevent fat in the deposition of vascular wall, the angiocardiopathies such as the formation and development that prevention of arterial is atherosis, prevention cerebral thrombus, cerebral hemorrhage, hypertension.DHA to cranial nerve, eyesight and intelligence development most important, can antiallergy and develop immunitypty.
Grape pip, as the accessory substance of wine industry, is a kind of edible oil resource of high-quality.Grape-kernel oil contains abundant unrighted acid, mainly oleic acid and linoleic acid, and wherein linoleic content can reach more than 70%.Also containing abundant Ve in grape-kernel oil, OPC, has stronger non-oxidizability, anti-ageing, the functions such as radioresistance, and self performance is more stable, not easily because of light, heat or contact with air and oxidative rancidity occurs.Linoleic acid is essential fatty acid, is easily absorbed by the body, and can resist free radical, anti-ageing, reduces uv damage, the collagen in protection skin, prevention melanin deposition etc.
Camellia oil is squeezed by the seed of tea oil tree to obtain, and is a kind of fully natural green edible oil.The functions such as camellia oil can anti-lipid peroxidation, regulates cardiovascular function, immunoloregulation function, prevention of obesity, protection liver.In camellia oil, the content of monounsaturated fatty acids-oleic acid is higher, and about 80%, oleic acid can reduce LDL-C, can harden by prevention of arterial, and does not reduce the High-density Lipoprotein-cholesterol useful to human body.Camellianin in camellia oil has cardiotonic, and tsubakisaponin has thrombus dissolving effect, and Tea Polyphenols has pre-preventing tumor and reduces the functional activity effects such as cholesterol, and squalene has antitumor and immunoregulation effect.
Therefore, linseed oil, grape-kernel oil, camellia oil are mixed and make oleic acid, linoleic acid, linolenic acid content ratio suitable, more easily digested, nutritive value is higher.Linseed oil, grape-kernel oil, camellia oil microcapsule powder stability are strong, good fluidity, and edible easy to carry, wherein unrighted acid is not easily destroyed, and range of application is wider.
Summary of the invention
The object of this invention is to provide a kind of unrighted acid balanced, taste is good, and embedding rate is high, and stability is strong, novel linseed oil/grape-kernel oil/camellia oil microcapsule powder that absorptivity is high and preparation method thereof.
According to novel linseed oil/grape-kernel oil/camellia oil microcapsule powder of the present invention, it comprises:
Containing refining linseed oil, grape-kernel oil, camellia oil;
Containing at least one emulsifying agent;
Containing at least one stabilizing agent;
Containing at least one dextrin or starch or protein as wall material;
The consumption (mass percent) 0.1% ~ 10% of wherein said emulsifying agent, is preferably 0.5% ~ 5%; The consumption (mass percent) 0.01% ~ 2% of described stabilizing agent, is preferably %0.1 ~ 0.5%; The consumption (mass percent) 0.01% ~ 10% of wall material, is preferably 1% ~ 5%.
According to the another aspect of invention, described novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, it is characterized in that described refining linseed oil (Flaxseed Oil) is the seed flax seed of flax family (Linaceae) plant flax (Linum usitatissimum L.), through cold pressing squeezing or hot pressing squeeze Hydrolysis kinetics form oily liquids.Grape-kernel oil is the oily liquids of grape pip through cold pressing squeezing or hot pressing squeezing Hydrolysis kinetics; Camellia oil is from the sub oily liquids through cold pressing squeezing or hot pressing squeezing Hydrolysis kinetics of Theaceae (Theaceae) Camellia (Camellia) oil tea (Camellia oleifera Abel.) seeds.
According to the another aspect of invention, described novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, is characterized in that content >=1% of alpha-linolenic acid in described powder, linoleic acid content >=1%, oleic acid content >=1%.
According to the another aspect of invention, described novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, is characterized in that described stabilizing agent is selected from one in CSL, stearoyl lactate, dipotassium hydrogen phosphate, sodium alginate, carboxymethyl cellulose (CMC), sodium carboxymethylcellulose (CMC-Na), carragheen, xanthans, agar or several.
According to the another aspect of invention, described novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, is characterized in that described emulsifying agent is selected from one in monoglyceride, single, double stearine, sucrose ester, sorbitan monostearate, sorbitol monooleate, octadecanoic acid ester of polyethylene glycol, egg yolk lecithin, soybean lecithin, casein sodium, sucrose ester or several.
According to the another aspect of invention, described novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, is characterized in that one or more that described wall material is selected from maltodextrin, cyclodextrin, CMS, Arabic gum, pure glue, casein sodium.
According to the another aspect of invention, the preparation method of described novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, is characterized in that comprising the following steps:
1) aqueous phase preparation: wall material and stabilizing agent are added to the water successively, keeps temperature 40 DEG C ~ 90 DEG C and stirs 15 ~ 30min to dissolving, obtained aqueous phase;
2) oil phase preparation: by linseed oil, grape-kernel oil and camellia oil mixing after with emulsifying agent miscible at temperature 40 DEG C ~ 90 DEG C, obtain oil phase;
3) just emulsification: slowly added in aqueous phase by oil phase and obtain mixture, adopts cutter to form O/W type emulsion to the emulsification of mixture high speed shear;
4) homogeneous: adopt secondary pressure homogenizer to carry out homogeneous to emulsion, first time homogenizing time 15 ~ 50min, homogenization pressure is 20 ~ 40Mpa, and second time homogenizing time is 15 ~ 50min, and homogenization pressure is 20 ~ 50Mpa.
5) granulating: adopt spray-dired method, keep emulsion temperature to be 50 ~ 80 DEG C, by spray-dried for emulsion rear obtained particle, spray-dired EAT is 150 ~ 180 DEG C, and spray-dired leaving air temp is 60 ~ 90 DEG C.
Novel linseed oil/grape-kernel oil/camellia oil microcapsule powder of the present invention, oleic acid contained by it, linoleic acid, linolenic acid content ratio are suitable, more easily digested, and nutritive value is higher.Linseed oil, grape-kernel oil, camellia oil microcapsule powder stability are strong, good fluidity, edible easy to carry; wherein unrighted acid is not easily destroyed, and grape-kernel oil procyanidins can scavenging free radicals, oxidation-resisting and caducity; Improving memory power, vision protection.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but protection scope of the present invention is not limited to this.
Embodiment 1
In linseed oil/grape-kernel oil/camellia oil microcapsule powder, the quality of each composition is:
Refining linseed oil 30g, grape-kernel oil 30g, camellia oil 30g, stabilizing agent (CSL/stearoyl lactate) 0.1g, emulsifying agent (monoglyceride: sucrose ester=1: 1) 4.9g, wall material (casein sodium: maltodextrin=1: 1) 4g.
1) aqueous phase preparation: wall material and stabilizing agent are added to the water successively, keeps temperature 80 DEG C and stirs 15 ~ 30min to dissolving, obtained aqueous phase;
2) oil phase preparation: by linseed oil, grape-kernel oil and camellia oil mixing after with emulsifying agent miscible at temperature 40 DEG C ~ 90 DEG C, obtain oil phase;
3) just emulsification: slowly added in aqueous phase by oil phase and obtain mixture, adopts cutter to form O/W type emulsion to the emulsification of mixture high speed shear;
4) homogeneous: adopt secondary pressure homogenizer to carry out homogeneous to emulsion, first time homogenizing time 30min, homogenization pressure is 30Mpa, and second time homogenizing time is 25min, and homogenization pressure is 40Mpa.
5) granulating: adopt spray-dired method, keep emulsion temperature to be 60 DEG C, by spray-dried for emulsion rear obtained particle, spray-dired EAT is 165 DEG C, and spray-dired leaving air temp is 80 DEG C.
Embodiment 2
In linseed oil/grape-kernel oil/camellia oil microcapsule powder, the quality of each composition is:
Refining linseed oil 40g, grape-kernel oil 30g, camellia oil 25g, stabilizing agent (CSL/stearoyl lactate) 0.2g, emulsifying agent (monoglyceride: sucrose ester=1: 1) 2.8g, wall material (casein sodium: maltodextrin=1: 1) 2g.
1) aqueous phase preparation: wall material and stabilizing agent are added to the water successively, keeps temperature 60 C and stirs 25min to dissolving, obtained aqueous phase;
2) oil phase preparation: by linseed oil, grape-kernel oil and camellia oil mixing after with emulsifying agent miscible at temperature 40 DEG C ~ 90 DEG C, obtain oil phase;
3) just emulsification: slowly added in aqueous phase by oil phase and obtain mixture, adopts cutter to form O/W type emulsion to the emulsification of mixture high speed shear;
4) homogeneous: adopt secondary pressure homogenizer to carry out homogeneous to emulsion, first time homogenizing time 20min, homogenization pressure is 30Mpa, and second time homogenizing time is 25min, and homogenization pressure is 30Mpa.
5) granulating: adopt spray-dired method, keep emulsion temperature to be 70 DEG C, by spray-dried for emulsion rear obtained particle, spray-dired EAT is 160 DEG C, and spray-dired leaving air temp is 70 DEG C.
Embodiment 3
In linseed oil/grape-kernel oil/camellia oil microcapsule powder, the quality of each composition is:
Refining linseed oil 50g, grape-kernel oil 25g, camellia oil 20g, stabilizing agent (CSL/stearoyl lactate) 0.2g, emulsifying agent (monoglyceride: sucrose ester=1: 1) 1.8g, (casein sodium: maltodextrin=1: 1) 3g, sweetener is appropriate, and flavoring essence is appropriate for wall material.
1) aqueous phase preparation: wall material and stabilizing agent are added to the water successively, keeps temperature 70 C and stirs 20min to dissolving, obtained aqueous phase;
2) oil phase preparation: by linseed oil, grape-kernel oil and camellia oil mixing after with emulsifying agent miscible at temperature 40 DEG C ~ 90 DEG C, obtain oil phase;
3) just emulsification: slowly added in aqueous phase by oil phase and obtain mixture, adopts cutter to form O/W type emulsion to the emulsification of mixture high speed shear;
4) homogeneous: adopt secondary pressure homogenizer to carry out homogeneous to emulsion, first time homogenizing time 35min, homogenization pressure is 35Mpa, and second time homogenizing time is 20min, and homogenization pressure is 35Mpa.
5) granulating: adopt spray-dired method, keep emulsion temperature to be 65 DEG C, by spray-dried for emulsion rear obtained particle, spray-dired EAT is 175 DEG C, and spray-dired leaving air temp is 65 DEG C.
Claims (8)
1. novel linseed oil/grape-kernel oil/camellia oil microcapsule powder, it comprises:
Containing refining linseed oil, grape-kernel oil, camellia oil;
Containing at least one emulsifying agent;
Containing at least one stabilizing agent;
Containing at least one dextrin or starch or protein as wall material;
The consumption (mass percent) 0.1% ~ 10% of wherein said emulsifying agent, is preferably 0.5% ~ 5%; The consumption (mass percent) 0.01% ~ 2% of described stabilizing agent, is preferably %0.1 ~ 0.5%; The consumption (mass percent) 0.01% ~ 10% of wall material, is preferably 1% ~ 5%.
2. novel linseed oil/grape-kernel oil/camellia oil microcapsule powder according to claim 1, it is characterized in that described refining linseed oil (Flaxseed Oil) is the seed flax seed of flax family (Linaceae) plant flax (Linum usitatissimum L.), through the oily liquids of cold pressing squeezing or hot pressing squeezing Hydrolysis kinetics.Grape-kernel oil is the oily liquids of grape pip through cold pressing squeezing or hot pressing squeezing Hydrolysis kinetics; Camellia oil is from the sub oily liquids through cold pressing squeezing or hot pressing squeezing Hydrolysis kinetics of Theaceae (Theaceae) Camellia (Camellia) oil tea (Camellia oleifera Abel.) seeds.
3. novel linseed oil/grape-kernel oil/camellia oil microcapsule powder according to claim 1, is characterized in that content >=1% of alpha-linolenic acid in described powder, linoleic acid content >=1%, oleic acid content >=1%.
4. novel linseed oil/grape-kernel oil/camellia oil microcapsule powder according to claim 1, is characterized in that described stabilizing agent is selected from one in CSL, stearoyl lactate, dipotassium hydrogen phosphate, sodium alginate, carboxymethyl cellulose (CMC), sodium carboxymethylcellulose (CMC-Na), carragheen, xanthans, agar or several.
5. novel linseed oil/grape-kernel oil/camellia oil microcapsule powder according to claim 1, is characterized in that described emulsifying agent is selected from one in monoglyceride, single, double stearine, sucrose ester, sorbitan monostearate, sorbitol monooleate, octadecanoic acid ester of polyethylene glycol, egg yolk lecithin, soybean lecithin, casein sodium, sucrose ester or several.
6. novel linseed oil/grape-kernel oil/camellia oil microcapsule powder according to claim 1, is characterized in that one or more that described wall material is selected from maltodextrin, cyclodextrin, CMS, Arabic gum, pure glue, casein sodium.
7. the preparation method of the novel linseed oil/grape-kernel oil/camellia oil microcapsule powder according to claim 1-6, is characterized in that comprising the following steps:
1) aqueous phase preparation: wall material and stabilizing agent are added to the water successively, keeps temperature 40 DEG C ~ 90 DEG C and stirs 15 ~ 30min to dissolving, obtained aqueous phase;
2) oil phase preparation: by linseed oil, grape-kernel oil and camellia oil mixing after with emulsifying agent miscible at temperature 40 DEG C ~ 90 DEG C, obtain oil phase;
3) just emulsification: slowly added in aqueous phase by oil phase and obtain mixture, adopts cutter to form O/W type emulsion to the emulsification of mixture high speed shear;
4) homogeneous: adopt secondary pressure homogenizer to carry out homogeneous to emulsion, first time homogenizing time 15 ~ 50min, homogenization pressure is 20 ~ 40Mpa, and second time homogenizing time is 15 ~ 50min, and homogenization pressure is 20 ~ 50Mpa.
5) granulating: adopt spray-dired method, keep emulsion temperature to be 50 ~ 80 DEG C, by spray-dried for emulsion rear obtained particle, spray-dired EAT is 150 ~ 180 DEG C, and spray-dired leaving air temp is 60 ~ 90 DEG C.
8., according to the novel linseed oil/grape-kernel oil/camellia oil microcapsule powder of claim 1-7, it is characterized in that, unrighted acid is balanced in nutrition, features good taste, absorptivity is high, and stability is better, and have stronger anti-oxidant, radioresistance, the functions such as anti-solarization moisturizing.
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