CN109452650A - A kind of novel linseed oil microcapsules and preparation method thereof - Google Patents
A kind of novel linseed oil microcapsules and preparation method thereof Download PDFInfo
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- CN109452650A CN109452650A CN201811417440.1A CN201811417440A CN109452650A CN 109452650 A CN109452650 A CN 109452650A CN 201811417440 A CN201811417440 A CN 201811417440A CN 109452650 A CN109452650 A CN 109452650A
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- linseed oil
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- 239000000944 linseed oil Substances 0.000 title claims abstract description 60
- 235000021388 linseed oil Nutrition 0.000 title claims abstract description 60
- 239000003094 microcapsule Substances 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims description 17
- 239000000463 material Substances 0.000 claims abstract description 22
- 229940088594 vitamin Drugs 0.000 claims abstract description 21
- 229930003231 vitamin Natural products 0.000 claims abstract description 21
- 235000013343 vitamin Nutrition 0.000 claims abstract description 21
- 239000011782 vitamin Substances 0.000 claims abstract description 21
- 150000003722 vitamin derivatives Chemical class 0.000 claims abstract description 21
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 19
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 18
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 18
- 239000000843 powder Substances 0.000 claims abstract description 16
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims abstract description 15
- 241000218231 Moraceae Species 0.000 claims abstract description 15
- 235000008708 Morus alba Nutrition 0.000 claims abstract description 15
- 244000078534 Vaccinium myrtillus Species 0.000 claims abstract description 15
- 235000017537 Vaccinium myrtillus Nutrition 0.000 claims abstract description 15
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 15
- 239000004006 olive oil Substances 0.000 claims abstract description 15
- 235000008390 olive oil Nutrition 0.000 claims abstract description 15
- 229940083466 soybean lecithin Drugs 0.000 claims abstract description 15
- 239000000203 mixture Substances 0.000 claims description 40
- 229920001353 Dextrin Polymers 0.000 claims description 19
- 239000004375 Dextrin Substances 0.000 claims description 19
- 108010010803 Gelatin Proteins 0.000 claims description 19
- 235000019425 dextrin Nutrition 0.000 claims description 19
- 229920000159 gelatin Polymers 0.000 claims description 19
- 239000008273 gelatin Substances 0.000 claims description 19
- 235000019322 gelatine Nutrition 0.000 claims description 19
- 235000011852 gelatine desserts Nutrition 0.000 claims description 19
- 229920002472 Starch Polymers 0.000 claims description 18
- 239000006210 lotion Substances 0.000 claims description 18
- 239000008107 starch Substances 0.000 claims description 18
- 235000019698 starch Nutrition 0.000 claims description 18
- 235000006708 antioxidants Nutrition 0.000 claims description 17
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 10
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 8
- 238000005520 cutting process Methods 0.000 claims description 6
- 239000008187 granular material Substances 0.000 claims description 6
- 238000000265 homogenisation Methods 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 238000001694 spray drying Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 229930006000 Sucrose Natural products 0.000 claims description 5
- 229930003270 Vitamin B Natural products 0.000 claims description 5
- 229930003427 Vitamin E Natural products 0.000 claims description 5
- 235000013871 bee wax Nutrition 0.000 claims description 5
- 239000012166 beeswax Substances 0.000 claims description 5
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 5
- 239000005720 sucrose Substances 0.000 claims description 5
- 235000019156 vitamin B Nutrition 0.000 claims description 5
- 239000011720 vitamin B Substances 0.000 claims description 5
- 235000019165 vitamin E Nutrition 0.000 claims description 5
- 229940046009 vitamin E Drugs 0.000 claims description 5
- 239000011709 vitamin E Substances 0.000 claims description 5
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 4
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims description 4
- QRYRORQUOLYVBU-VBKZILBWSA-N Carnosic acid Natural products CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 claims description 4
- XUSYGBPHQBWGAD-PJSUUKDQSA-N Carnosol Chemical compound CC([C@@H]1C2)(C)CCC[C@@]11C(=O)O[C@@H]2C2=C1C(O)=C(O)C(C(C)C)=C2 XUSYGBPHQBWGAD-PJSUUKDQSA-N 0.000 claims description 4
- MMFRMKXYTWBMOM-UHFFFAOYSA-N Carnosol Natural products CCc1cc2C3CC4C(C)(C)CCCC4(C(=O)O3)c2c(O)c1O MMFRMKXYTWBMOM-UHFFFAOYSA-N 0.000 claims description 4
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 4
- 244000269722 Thea sinensis Species 0.000 claims description 4
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims description 4
- 229930003268 Vitamin C Natural products 0.000 claims description 4
- OENHQHLEOONYIE-UKMVMLAPSA-N all-trans beta-carotene Natural products CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C OENHQHLEOONYIE-UKMVMLAPSA-N 0.000 claims description 4
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims description 4
- 235000013734 beta-carotene Nutrition 0.000 claims description 4
- TUPZEYHYWIEDIH-WAIFQNFQSA-N beta-carotene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2=CCCCC2(C)C TUPZEYHYWIEDIH-WAIFQNFQSA-N 0.000 claims description 4
- 239000011648 beta-carotene Substances 0.000 claims description 4
- 229960002747 betacarotene Drugs 0.000 claims description 4
- 235000004654 carnosol Nutrition 0.000 claims description 4
- 239000000787 lecithin Substances 0.000 claims description 4
- 235000010445 lecithin Nutrition 0.000 claims description 4
- 229940067606 lecithin Drugs 0.000 claims description 4
- 235000019155 vitamin A Nutrition 0.000 claims description 4
- 239000011719 vitamin A Substances 0.000 claims description 4
- 235000019154 vitamin C Nutrition 0.000 claims description 4
- 239000011718 vitamin C Substances 0.000 claims description 4
- 229940045997 vitamin a Drugs 0.000 claims description 4
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 claims description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 2
- DNXHEGUUPJUMQT-CBZIJGRNSA-N Estrone Chemical compound OC1=CC=C2[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CCC2=C1 DNXHEGUUPJUMQT-CBZIJGRNSA-N 0.000 claims 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims 1
- 235000014113 dietary fatty acids Nutrition 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 229930195729 fatty acid Natural products 0.000 claims 1
- 239000000194 fatty acid Substances 0.000 claims 1
- 150000004665 fatty acids Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 239000002775 capsule Substances 0.000 abstract description 4
- 235000016709 nutrition Nutrition 0.000 abstract description 2
- 230000035764 nutrition Effects 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 235000004431 Linum usitatissimum Nutrition 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 150000002978 peroxides Chemical class 0.000 description 4
- -1 sucrose fatty ester Chemical class 0.000 description 4
- 240000006240 Linum usitatissimum Species 0.000 description 3
- 235000004426 flaxseed Nutrition 0.000 description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 description 3
- 235000013824 polyphenols Nutrition 0.000 description 3
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 description 2
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000020673 eicosapentaenoic acid Nutrition 0.000 description 2
- 229960005135 eicosapentaenoic acid Drugs 0.000 description 2
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- DVSZKTAMJJTWFG-SKCDLICFSA-N (2e,4e,6e,8e,10e,12e)-docosa-2,4,6,8,10,12-hexaenoic acid Chemical compound CCCCCCCCC\C=C\C=C\C=C\C=C\C=C\C=C\C(O)=O DVSZKTAMJJTWFG-SKCDLICFSA-N 0.000 description 1
- GZJLLYHBALOKEX-UHFFFAOYSA-N 6-Ketone, O18-Me-Ussuriedine Natural products CC=CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O GZJLLYHBALOKEX-UHFFFAOYSA-N 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 241000208202 Linaceae Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000001409 beta-carotene group Chemical group 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000008162 cooking oil Substances 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000020669 docosahexaenoic acid Nutrition 0.000 description 1
- KAUVQQXNCKESLC-UHFFFAOYSA-N docosahexaenoic acid (DHA) Natural products COC(=O)C(C)NOCC1=CC=CC=C1 KAUVQQXNCKESLC-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
- A23L19/09—Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
- A23L29/045—Organic compounds containing nitrogen as heteroatom
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
- A23L29/35—Degradation products of starch, e.g. hydrolysates, dextrins; Enzymatically modified starches
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
- A23L33/155—Vitamins A or D
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
The invention discloses a kind of novel linseed oil microcapsules, are made of linseed oil, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, wall material, antioxidant, emulsifier, and the capsule is not oxidizable, has good storage-stable；The capsule includes olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, and nutrition comprehensive and abundant is in good taste；It is easy to operate that this production process is simple, high production efficiency.
Description
Technical field
The present invention relates to novel linseed oil microcapsules, more particularly to a kind of novel linseed oil microcapsules and its preparation
Method
Background technique
Linseed oil (linseed oil or siritch), is the drying grease obtained by producing in linseed, is in yellow transparent shape,
With unique fragrance.Oil content is about 35%-45% in linseed, wherein alpha-linolenic acid rich content, it can be dynamic
It is converted into the unsaturated fatty acids such as eicosapentaenoic acid (EPA), docosahexaenoic acid (DHA) in object, there is high battalion
Value and important physiological function are supported, there is reducing blood lipid, blood pressure lowering improves cardiovascular and cerebrovascular disease, prevents diabetes, rheumatism, class
Rheumatism, tumour and other effects, therefore gradually obtain the concern of people.Linseed oil is mainly packed with traditional cooking oil in the market
Form, application range are narrow.Easily generation aoxidizes, is rancid polyunsaturated fatty acid during the cooking process, and its oxidation product may
Many adverse effects can be generated to human body, it is seen that high-temperature cooking method is not the best edible way of linseed oil.In addition, flax
The unique flavor of seed oil is difficult to receive in southern area, it is caused to take in the limitation of form, therefore the inhibition for its flavor
It is also critical issue urgently to be solved with such flavor is covered.The peculiar flavour of linseed oil, unstable and oil-soluble feature
Greatly limit its extensive use in various food and health care product.And the generation of microcapsules is not only easier to take, Er Qieyou
Conducive to wide popularization and application, but existing linseed microcapsules are oxidizable in storage, and dissolubility is poor, it is difficult to guarantee product
Shelf-life.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of novel linseed oil microcapsules, which is not easy oxygen
Change, dissolubility is good, long shelf-life；The preparation method high production efficiency, it is easy to operate.
The purpose of the present invention is what is be achieved through the following technical solutions:
A kind of novel linseed oil microcapsules, are made of the raw material of following mass fraction: 20-50 parts of linseed oil, olive oil 10-
30 parts, 5-10 parts of mulberries powder, 8-14 parts of Bilberry fruit P.E, 2-6 parts of vitamin, 1-5 parts of soybean lecithin, 40-90 parts of wall material, antioxygen
0.5-1.5 parts of agent, 0.3-2 parts of emulsifier.
Further, the vitamin is by one or more of vitamin E, vitamin B, vitamin A, vitamin C group
At.
Further, the wall material is made of dextrin, starch, gelatin, the dextrin, starch, gelatin mass fraction be
5-20 parts of dextrin, 6-10 parts of starch, 1-5 parts of gelatin.
Further, the antioxidant is made of one or more of tea polyphenols, beta carotene, carnosol.
Further, the emulsifier by one of sucrose fatty ester, beeswax, lecithin or a variety of forms.
A kind of preparation method of novel linseed oil microcapsules, preparation step are as follows:
(1) wall material of formula ratio, antioxidant are successively poured into blender, the water of 90-100 mass fraction is added, is heated to
It 40 DEG C~70 DEG C of temperature, keeps the temperature and 20~60min of high-speed stirred is allowed to be completely dissolved, mixture A is made；
(2) by the linseed oil of formula ratio, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, emulsifier, mixed
It closes uniformly, is heated to 45-75 DEG C, heat preservation is persistently stirred 20-50 minutes, and mixture B is made；
(3) mixture B is poured slowly into mixture A and obtains mixture C, using cutter to mixture C high speed shear, cut
Cutting speed degree is 15000rpm~21000rpm, and shear time is 20-40 minutes, obtains lotion；
(4) second homogenate, homogenization pressure 40-75Mpa are carried out to lotion obtained by step (3) using homogenizer, homogenizing time is
30- 60min；
(5) lotion obtained by step (4) is spray-dried, 175-185 DEG C of spray drying EAT, leaving air temp 65-75
DEG C, obtain linseed oil microcapsule granule.
Beneficial effect
The novel linseed oil microcapsules use a certain proportion of gelatin, dextrin, starch for the main of linseed oil microencapsulation
Wall material not only has high efficiency, high yield, not oxidizable, good storage-stable, and has preferable dissolubility, should
Main wall material can improve the compactness of microcapsule membrane；Improve the quality guarantee period of capsule.The capsule includes olive oil, mulberries simultaneously
Powder, Bilberry fruit P.E, vitamin, soybean lecithin, nutrition comprehensive and abundant are in good taste；It is easy to operate that this production process is simple, production effect
Rate is high.
Detailed description of the invention
Fig. 1 is linseed oil and microcapsules peroxide value variation diagram obtained by embodiment 1；
Fig. 2 is linseed oil and microcapsules peroxide value variation diagram obtained by embodiment 2；
Fig. 3 is linseed oil and microcapsules peroxide value variation diagram obtained by embodiment 3；
Fig. 4 is linseed oil and microcapsules peroxide value variation diagram obtained by embodiment 4.
Specific embodiment
The present invention is described below by specific embodiment, unless stated otherwise, technological means used in the present invention
It is method known in those skilled in the art.In addition, embodiment is interpreted as illustrative, it is not intended to limit the present invention
Range, the spirit and scope of the invention are limited only by the claims that follow.To those skilled in the art, without departing substantially from this
Under the premise of invention spirit and scope, to the various changes or change of material component and dosage progress in these embodiments
It belongs to the scope of protection of the present invention.
Embodiment 1
A kind of novel linseed oil microcapsules, are made of the raw material of following mass fraction: 20 parts of linseed oil, 10 parts of olive oil,
5 parts of mulberries powder, 8 parts of Bilberry fruit P.E, 2 parts of vitamin, 1 part of soybean lecithin, 40 parts of wall material, 0.5 part of antioxidant, emulsifier
0.3 part；The vitamin is by vitamin E；The wall material is made of dextrin, starch, gelatin, the matter of the dextrin, starch, gelatin
Measuring number is 5 parts of dextrin, 6 parts of starch, 1 part of gelatin；The antioxidant is tea polyphenols；The emulsifier is sucrose fatty ester.
A kind of preparation method of novel linseed oil microcapsules, preparation step are as follows:
(1) wall material of formula ratio, antioxidant are successively poured into blender, the water of 90 mass fractions is added, is heated to temperature
It 40 DEG C, keeps the temperature and high-speed stirred 20min is allowed to be completely dissolved, mixture A is made；
(2) by the linseed oil of formula ratio, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, emulsifier, mixed
It closes uniformly, is heated to 45 DEG C, heat preservation is persistently stirred 20 minutes, and mixture B is made；
(3) mixture B is poured slowly into mixture A and obtains mixture C, using cutter to mixture C high speed shear, cut
Cutting speed degree is 15000rpm, and shear time is 20 minutes, obtains lotion；
(4) second homogenate, homogenization pressure 40Mpa are carried out to lotion obtained by step (3) using homogenizer, homogenizing time is
30min；
(5) lotion obtained by step (4) is spray-dried, 175 DEG C of spray drying EAT, 65 DEG C of leaving air temp, is obtained
Linseed oil microcapsule granule.
Linseed oil microcapsules in embodiment 1 are placed into 10d in 68 DEG C of insulating box, is equivalent to and stores at room temperature
10 months, linseed oil microcapsules quality kept good, saw Fig. 1.
Embodiment 2
A kind of novel linseed oil microcapsules, are made of the raw material of following mass fraction: 50 parts of linseed oil, 30 parts of olive oil,
10 parts of mulberries powder, 14 parts of Bilberry fruit P.E, 6 parts of vitamin, 5 parts of soybean lecithin, 90 parts of wall material, 1.5 parts of antioxidant, emulsifier
2 parts；The vitamin is vitamin B；The wall material is made of dextrin, starch, gelatin, the quality of the dextrin, starch, gelatin
Number is 20 parts of dextrin, 10 parts of starch, 5 parts of gelatin；The antioxidant is beta carotene；The emulsifier is beeswax.
A kind of preparation method of novel linseed oil microcapsules, preparation step are as follows:
(1) wall material of formula ratio, antioxidant are successively poured into blender, the water of 100 mass fractions is added, is heated to temperature
It 70 DEG C, keeps the temperature and high-speed stirred 60min is allowed to be completely dissolved, mixture A is made；
(2) by the linseed oil of formula ratio, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, emulsifier, mixed
It closes uniformly, is heated to 75 DEG C, heat preservation is persistently stirred 50 minutes, and mixture B is made；
(3) mixture B is poured slowly into mixture A and obtains mixture C, using cutter to mixture C high speed shear, cut
Cutting speed degree is 21000rpm, and shear time is 40 minutes, obtains lotion；
(4) second homogenate, homogenization pressure 75Mpa are carried out to lotion obtained by step (3) using homogenizer, homogenizing time is
60min；
(5) lotion obtained by step (4) is spray-dried, 185 DEG C of spray drying EAT, 75 DEG C of leaving air temp, is obtained
Linseed oil microcapsule granule.
Linseed oil microcapsules in embodiment 2 are placed into 10d in 68 DEG C of insulating box, is equivalent to and stores at room temperature
10 months, linseed oil microcapsules quality kept good, saw Fig. 2.
Embodiment 3
A kind of novel linseed oil microcapsules, are made of the raw material of following mass fraction: 30 parts of linseed oil, 20 parts of olive oil,
8 parts of mulberries powder, 11 parts of Bilberry fruit P.E, 4 parts of vitamin, 3 parts of soybean lecithin, 60 parts of wall material, 1 part of antioxidant, emulsifier 2
Part；The vitamin is made of 5 parts of vitamin E, 6 parts of vitamin B, 3 parts of vitamin A, 1 part of vitamin C；The wall material by
Dextrin, starch, gelatin composition, the dextrin, starch, gelatin mass fraction be 15 parts of dextrin, 8 parts of starch, 4 parts of gelatin；Institute
Stating antioxidant is carnosol；The emulsifier is made of 2 parts of sucrose fatty ester, 3 parts of beeswax, 1 part of lecithin.
A kind of preparation method of novel linseed oil microcapsules, preparation step are as follows:
(1) wall material of formula ratio, antioxidant are successively poured into blender, the water of 95 mass fractions is added, is heated to temperature
It 50 DEG C, keeps the temperature and high-speed stirred 50min is allowed to be completely dissolved, mixture A is made；
(2) by the linseed oil of formula ratio, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, emulsifier, mixed
It closes uniformly, is heated to 60 DEG C, heat preservation is persistently stirred 35 minutes, and mixture B is made；
(3) mixture B is poured slowly into mixture A and obtains mixture C, using cutter to mixture C high speed shear, cut
Cutting speed degree is 20000rpm, and shear time is 30 minutes, obtains lotion；
(4) second homogenate, homogenization pressure 60Mpa are carried out to lotion obtained by step (3) using homogenizer, homogenizing time is
50min；
(5) lotion obtained by step (4) is spray-dried, 185 DEG C of spray drying EAT, 75 DEG C of leaving air temp, is obtained
Linseed oil microcapsule granule.
Linseed oil microcapsules in embodiment 3 are placed into 10d in 68 DEG C of insulating box, is equivalent to and stores at room temperature
10 months, linseed oil microcapsules quality kept good, saw Fig. 3.
Embodiment 4
A kind of novel linseed oil microcapsules, are made of the raw material of following mass fraction: 40 parts of linseed oil, 25 parts of olive oil,
9 parts of mulberries powder, 13 parts of Bilberry fruit P.E, 5 parts of vitamin, 4 parts of soybean lecithin, 80 parts of wall material, 1.5 parts of antioxidant, emulsifier 2
Part；The vitamin is made of 2 parts of vitamin E, 1 part of vitamin B, 2 parts of vitamin A, 1 part of vitamin C；The wall material by
Dextrin, starch, gelatin composition, the dextrin, starch, gelatin mass fraction be 20 parts of dextrin, 10 parts of starch, 5 parts of gelatin；Institute
It states antioxidant to be made of the component of following mass fraction, 2 parts of tea polyphenols, 0.5 part of beta carotene, 0.8 part of carnosol；
The emulsifier is made of 2 parts of sucrose fatty ester, 1 part of beeswax, 1 part of lecithin.
A kind of preparation method of novel linseed oil microcapsules, preparation step are as follows:
(1) wall material of formula ratio, antioxidant are successively poured into blender, the water of 95 mass fractions is added, is heated to temperature
It 70 DEG C, keeps the temperature and high-speed stirred 60min is allowed to be completely dissolved, mixture A is made；
(2) by the linseed oil of formula ratio, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, emulsifier, mixed
It closes uniformly, is heated to 75 DEG C, heat preservation is persistently stirred 50 minutes, and mixture B is made；
(3) mixture B is poured slowly into mixture A and obtains mixture C, using cutter to mixture C high speed shear, cut
Cutting speed degree is 21000rpm, and shear time is 30 minutes, obtains lotion；
(4) second homogenate, homogenization pressure 60Mpa are carried out to lotion obtained by step (3) using homogenizer, homogenizing time is
50min；
(5) lotion obtained by step (4) is spray-dried, 185 DEG C of spray drying EAT, 75 DEG C of leaving air temp, is obtained
Linseed oil microcapsule granule.
Linseed oil microcapsules in embodiment 4 are placed into 10d in 68 DEG C of insulating box, is equivalent to and stores at room temperature
10 months, linseed oil microcapsules quality kept good, saw Fig. 4.
The microcapsule stability is good, and product has a good taste and flavor, and quality safety is reliable, long shelf-life, the system
Preparation Method simple process, easy to operate, good film-forming property, high production efficiency.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and
Made any modifications, equivalent replacements and improvements within principle, should all fall within the scope and spirit of the invention.
Claims (6)
1. a kind of novel linseed oil microcapsules, which is characterized in that be made of the raw material of following mass fraction: linseed oil 20-
50 parts, 10-30 parts of olive oil, 5-10 parts of mulberries powder, 8-14 parts of Bilberry fruit P.E, 2-6 parts of vitamin, 1-5 parts of soybean lecithin, wall
40-90 parts of material, 0.5-1.5 parts of antioxidant, 0.3-2 parts of emulsifier.
2. a kind of novel linseed oil microcapsules according to claim 1, which is characterized in that the vitamin is by vitamin
E, one or more of vitamin B, vitamin A, vitamin C form.
3. a kind of novel linseed oil microcapsules according to claim 1, which is characterized in that the wall material is by dextrin, shallow lake
Powder, gelatin composition, the dextrin, starch, gelatin mass fraction be 5-20 parts of dextrin, 6-10 parts of starch, 1-5 parts of gelatin.
4. a kind of novel linseed oil microcapsules according to claim 1, which is characterized in that the antioxidant is more by tea
One or more of phenol, beta carotene, carnosol composition.
5. a kind of novel linseed oil microcapsules according to claim 1, which is characterized in that the emulsifier is by Sucrose Fatty Acid Ester
One of fat ester, beeswax, lecithin are a variety of.
6. a kind of preparation method of novel linseed oil microcapsules according to claim 1, which is characterized in that preparation step
It is as follows:
(1) wall material of formula ratio, antioxidant are successively poured into blender, the water of 90-100 mass fraction is added, is heated to
It 40 DEG C~70 DEG C of temperature, keeps the temperature and 20~60min of high-speed stirred is allowed to be completely dissolved, mixture A is made；
(2) by the linseed oil of formula ratio, olive oil, mulberries powder, Bilberry fruit P.E, vitamin, soybean lecithin, emulsifier, mixed
It closes uniformly, is heated to 45-75 DEG C, heat preservation is persistently stirred 20-50 minutes, and mixture B is made；
(3) mixture B is poured slowly into mixture A and obtains mixture C, using cutter to mixture C high speed shear, cut
Cutting speed degree is 15000rpm~21000rpm, and shear time is 20-40 minutes, obtains lotion；
(4) second homogenate, homogenization pressure 40-75Mpa are carried out to lotion obtained by step (3) using homogenizer, homogenizing time is
30- 60min；
(5) lotion obtained by step (4) is spray-dried, 175-185 DEG C of spray drying EAT, leaving air temp 65-75
DEG C, obtain linseed oil microcapsule granule.
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| CN112471484A (en) * | 2020-11-28 | 2021-03-12 | 福建师范大学 | Litsea cubeba powder oil and preparation method thereof |
| CN113785983A (en) * | 2021-09-16 | 2021-12-14 | 吉林大学 | High-oxidation-stability macadamia nut oil microcapsule and preparation method thereof |
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