CN104886267A - Rice bran crude oil with high nutritive value and preparation method of rice bran crude oil - Google Patents
Rice bran crude oil with high nutritive value and preparation method of rice bran crude oil Download PDFInfo
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Abstract
The invention discloses rice bran crude oil with a high nutritive value. The rice bran crude oil comprises the raw materials in parts by weight: 200-250 parts of rice bran, 10-13 parts of grape seeds, 13-16 parts of sweet apricot kernels, 20-26 parts of corn kernels, 23-28 parts of coconut meat, 5-8 parts of penoy seeds, 12-15 parts of semen juglandis, 12-16 parts of purple perilla seeds, 15-18 parts of fruits of Chinese wolfberries, 9-12 parts of rosemary, 5-9 parts of thyme, 15-18 parts of oregano, 6-8 parts of myrrh, 2-4 parts of siraitia grosvenorii and 18-20 parts of coix seeds. The invention further discloses a preparation method of the rice bran crude oil with the high nutritive value. The preparation method comprises the steps: rushing, mixing, spraying and wetting the raw materials to obtain a first material; carrying out microwave treatment on the first material to obtain a second material; adjusting the pH value of the second material and adding water and compound enzymes for enzymolysis to obtain a third material; and after deactivating the third material, cooling, filter, lixiviating, centrifugalizing and distilling the third material to obtain the rice bran crude oil with the high nutritive value.
Description
Technical field
The present invention relates to vegetable oil technical field, particularly relate to Rice bran crude oil of a kind of high nutritive value and preparation method thereof.
Background technology
Paddy is the maximum large agricultural product of China's output, within nearly 5 years, rice yield is between 1.75-1.99 hundred million tons, account for more than 1/3 of national total output of grain, account for 31% of world's paddy total output, occupy first place in the world, paddy is that the food problem solving China 1,300,000,000 population has made significant contribution, has its own strategic significance to guarantee China grain security.
One of principal by product that rice bran obtains when being paddy processing polished rice.The general oil content of rice bran is 15-20%, oleic acid in rice bran oil and the ratio of linoleic acid content are roughly 1:1, from the viewpoint of modern nutriology, it, with other cereal grease (as wheat-germ oil, maize germ wet goods), has higher nutritive value; Meanwhile, rice bran oil contains more lipoids, mainly contains vitamin E, oryzanol, sitosterol and other phytosterol, has the function reducing human serum cholesterol, prevention and cure of cardiovascular disease.
But the problems such as material composition shows slightly single, production technology is relatively loaded down with trivial details that rice bran oil commercially available at present exists, limit the utilization and extention of rice bran oil to a certain extent, therefore, other natural component can be added in traditional rice bran oil raw material, with improve Dietotherapy health be worth, simultaneously consider take more safely and efficiently production technology to enhance productivity.
Contain the compositions such as multiple volatility oils, liposoluble constituent and alkaloid in Chinese herbal medicine and spice, these compositions all have certain medicinal effects, add in rice bran oil by these active components, improve the edibility of rice bran oil greatly.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes Rice bran crude oil of a kind of high nutritive value and preparation method thereof, comprehensive nutrition, aromatic flavour, energy enriching yin and nourishing kidney, dehumidifying is fallen dry, has holding time long effect, is applicable to consumer's daily health caring and uses.
The Rice bran crude oil of a kind of high nutritive value that the present invention proposes, its raw material comprises by weight: rice bran 200-250 part, grape pip 10-13 part, dessert almond 13-16 part, iblet 20-26 part, coconut meat 23-28 part, peony seeds 5-8 part, walnut kernel 12-15 part, purple perilla seed 12-16 part, fruit of Chinese wolfberry 15-18 part, rosemary 9-12 part, thyme 5-9 part, wild marjoram 15-18 part, myrrh 6-8 part, Momordica grosvenori 2-4 part, coix seed 18-20 part.
Preferably, the weight ratio of rice bran, grape pip, dessert almond, iblet, coconut meat is 220-230:11-12:14-15:22-24:25-26.
Preferably, the weight ratio of rice bran, peony seeds, walnut kernel, purple perilla seed, the fruit of Chinese wolfberry, rosemary is 220-230:6-7:13-14:13-15:16-17:10-11.
Preferably, the weight ratio of rice bran, rosemary, thyme, wild marjoram, myrrh, Momordica grosvenori is 220-230:10-11:6-8:16-17:6.2-7.8:2.5-3.5.
Preferably, its raw material comprises by weight: rice bran 220-230 part, grape pip 11-12 part, dessert almond 14-15 part, iblet 22-24 part, coconut meat 25-26 part, peony seeds 6-7 part, walnut kernel 13-14 part, purple perilla seed 13-15 part, fruit of Chinese wolfberry 16-17 part, rosemary 10-11 part, thyme 6-8 part, wild marjoram 16-17 part, myrrh 6.2-7.8 part, Momordica grosvenori 2.5-3.5 part, coix seed 18.8-19.6 part.
The preparation method of the Rice bran crude oil of the above-mentioned high nutritive value that the present invention also proposes, comprises the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 30-40 order, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 10-12wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 500-700w, and microwave treatment time is 80-90s;
S3, the pH of the second material is adjusted to acidity, then adds water and complex enzyme, be warming up to 50-52 DEG C, insulation 2-3h obtains 3 material;
S4,3 material is warming up to 125-130 DEG C, insulation 1-2min, cooling, filtration obtains the first mixing material, adds leaching liquor, stir in the first mixing material, be warming up to 38-42 DEG C, lixiviate 8-9h, centrifugally obtains the second mixing material, and then distillation obtains the Rice bran crude oil of high nutritive value.
Preferably, in S3, the pH of the second material is adjusted to 4-4.5.
Preferably, in S3, complex enzyme is made up of acid protease and cellulase.
Preferably, in S3, the weight ratio of the second material, water and complex enzyme is 100:400-500:0.8-1.5.
Preferably, in S4, leaching liquor is 3-4:0.8-1.5 by n-hexane and isopropyl alcohol by volume.
The present invention adopts rice bran, grape pip, dessert almond, iblet, coconut meat, peony seeds, walnut kernel, purple perilla seed to be prepared crude oil, make the present invention based on rice bran oil, further comprises grape-kernel oil, Sweet Almond Oil, iblet oil, coconut meat oily, peony seed oil, Semen Juglandis oil, Purple Perilla Seed Oil, its Sweet Almond Oil is rich in the trace element of protein, unrighted acid, vitamin, inorganic salts, dietary fiber and needed by human body, there is moistening lung, stomach invigorating, the effect that regains one's strength of body, the anti-cancer active matter that its amygdalin is natural especially, peony seed oil unsaturated fatty acid content reaches more than 90%, especially estimable is wherein polyunsaturated fatty acid-leukotrienes (belonging to ω-3 series) content more than 40%, the grease that coconut oil is made up of medium chain fatty acid, the long-chain fat molecule of other foods of Medium chain fatty molecular proportion is little, easily digested, can improve metabolic efficiency, also has natural comprehensive antibacterial ability, walnut oil and Purple Perilla Seed Oil are all rich in alpha-linolenic acid containing abundant, and linoleic acid, as essential fatty acid, is easily absorbed by the body, and can reduce human serum cholesterol, the vegetative nerve function of effective mediator, above-mentioned all material coordinate the ratio greatly reducing saturated fatty acid and unrighted acid in the present invention, are of value to health, and are rich in leukotrienes in raw material, can form DHA in vivo, can be of value to child and grow, and the fruit of Chinese wolfberry, rosemary, thyme, wild marjoram, myrrh, Momordica grosvenori, coix seed is as auxiliary material, crude oil mating reaction prepared by the leaching liquor adopted and the present invention, liposoluble constituent in auxiliary material is extracted, greatly strengthen nutritive value of the present invention, energy enriching yin and nourishing kidney, dehumidifying is fallen dry, wherein rosemary, thyme, Momordica grosvenori and peony seeds cooperatively interact, the present invention is made not only to have the delicate fragrance of rice, also there is the smell of the fragrance of a flower, and from rosemary, thyme, wild marjoram, the liposoluble constituent extracted in myrrh can improve non-oxidizability of the present invention greatly, extend the holding time.
Comprehensive nutrition of the present invention, aromatic flavour, energy enriching yin and nourishing kidney, dehumidifying is fallen dry, has holding time long effect, is applicable to consumer's daily health caring and uses.
Accompanying drawing explanation
Fig. 1 is the process chart of the preparation method of the Rice bran crude oil of a kind of high nutritive value that the present invention proposes.
Detailed description of the invention
As shown in Figure 1, Fig. 1 is the process chart of the preparation method of the Rice bran crude oil of a kind of high nutritive value that the present invention proposes.
With reference to Fig. 1, the preparation method of the Rice bran crude oil of a kind of high nutritive value that the present invention proposes, comprises the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 30-40 order, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 10-12wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 500-700w, and microwave treatment time is 80-90s;
S3, the pH of the second material is adjusted to acidity, then adds water and complex enzyme, be warming up to 50-52 DEG C, insulation 2-3h obtains 3 material;
S4,3 material is warming up to 125-130 DEG C, insulation 1-2min, cooling, filtration obtains the first mixing material, adds leaching liquor, stir in the first mixing material, be warming up to 38-42 DEG C, lixiviate 8-9h, centrifugally obtains the second mixing material, and then distillation obtains the Rice bran crude oil of high nutritive value.
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The Rice bran crude oil of a kind of high nutritive value that the present invention proposes, its raw material comprises by weight: 200 parts, rice bran, grape pip 13 parts, dessert almond 13 parts, iblet 26 parts, coconut meat 23 parts, peony seeds 8 parts, walnut kernel 12 parts, purple perilla seed 16 parts, the fruit of Chinese wolfberry 15 parts, rosemary 12 parts, thyme 5 parts, wild marjoram 18 parts, myrrh 6 parts, Momordica grosvenori 4 parts, coix seed 18 parts.
The preparation method of the Rice bran crude oil of the above-mentioned high nutritive value that the present invention also proposes, comprises the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 30 orders, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 12wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 500w, and microwave treatment time is 90s;
S3, the pH of the second material is adjusted to acidity, then adds water and complex enzyme, be warming up to 50 DEG C, insulation 3h obtains 3 material;
S4,3 material is warming up to 125 DEG C, insulation 2min, cooling, filters and obtains the first mixing material, in the first mixing material, add leaching liquor, stir, be warming up to 38 DEG C, lixiviate 9h, centrifugally obtains the second mixing material, and then distillation obtains the Rice bran crude oil of high nutritive value.
Embodiment 2
The Rice bran crude oil of a kind of high nutritive value that the present invention proposes, its raw material comprises by weight: 250 parts, rice bran, grape pip 10 parts, dessert almond 16 parts, iblet 20 parts, coconut meat 28 parts, peony seeds 5 parts, walnut kernel 15 parts, purple perilla seed 12 parts, the fruit of Chinese wolfberry 18 parts, rosemary 9 parts, thyme 9 parts, wild marjoram 15 parts, myrrh 8 parts, Momordica grosvenori 2 parts, coix seed 20 parts.
The preparation method of the Rice bran crude oil of the above-mentioned high nutritive value that the present invention also proposes, comprises the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 34 orders, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 11wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 650w, and microwave treatment time is 82s;
S3, the pH of the second material is adjusted to 4.5, then the complex enzyme adding water and be made up of acid protease and cellulase, be warming up to 51 DEG C, insulation 2.6h obtains 3 material, and wherein the weight ratio of the second material, water and complex enzyme is 100:500:0.8;
S4,3 material is warming up to 127 DEG C, insulation 1.6min, cooling, filters and obtains the first mixing material, in the first mixing material, add leaching liquor, stir, be warming up to 40 DEG C, lixiviate 8.3h, centrifugally obtain the second mixing material, then distillation obtains the Rice bran crude oil of high nutritive value, and wherein leaching liquor is 5:1 by n-hexane and isopropyl alcohol by volume.
Embodiment 3
The Rice bran crude oil of a kind of high nutritive value that the present invention proposes, its raw material comprises by weight: 230 parts, rice bran, grape pip 11 parts, dessert almond 15 parts, iblet 22 parts, coconut meat 26 parts, peony seeds 6 parts, walnut kernel 14 parts, purple perilla seed 13 parts, the fruit of Chinese wolfberry 17 parts, rosemary 10 parts, thyme 8 parts, wild marjoram 16 parts, myrrh 7.8 parts, Momordica grosvenori 2.5 parts, coix seed 19.6 parts.
The preparation method of the Rice bran crude oil of the above-mentioned high nutritive value that the present invention also proposes, comprises the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 36 orders, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 10.5wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 550w, and microwave treatment time is 88s;
S3, the pH of the second material is adjusted to 4, then the complex enzyme adding water and be made up of acid protease and cellulase, be warming up to 51 DEG C, insulation 2.4h obtains 3 material, and wherein the weight ratio of the second material, water and complex enzyme is 100:400:1.5;
S4,3 material is warming up to 128 DEG C, insulation 1.2min, cooling, filters and obtains the first mixing material, in the first mixing material, add leaching liquor, stir, be warming up to 39 DEG C, lixiviate 8.6h, centrifugally obtain the second mixing material, then distillation obtains the Rice bran crude oil of high nutritive value, and wherein leaching liquor is 2:1 by n-hexane and isopropyl alcohol by volume.
Embodiment 4
The Rice bran crude oil of a kind of high nutritive value that the present invention proposes, its raw material comprises by weight: 220 parts, rice bran, grape pip 12 parts, dessert almond 14 parts, iblet 24 parts, coconut meat 25 parts, peony seeds 7 parts, walnut kernel 13 parts, purple perilla seed 15 parts, the fruit of Chinese wolfberry 16 parts, rosemary 11 parts, thyme 6 parts, wild marjoram 17 parts, myrrh 6.2 parts, Momordica grosvenori 3.5 parts, coix seed 18.8 parts.
The preparation method of the Rice bran crude oil of the above-mentioned high nutritive value that the present invention also proposes, comprises the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 40 orders, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 10wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 700w, and microwave treatment time is 80s;
S3, the pH of the second material is adjusted to acidity, then adds water and complex enzyme, be warming up to 52 DEG C, insulation 2h obtains 3 material;
S4,3 material is warming up to 130 DEG C, insulation 1min, cooling, filters and obtains the first mixing material, in the first mixing material, add leaching liquor, stir, be warming up to 42 DEG C, lixiviate 8h, centrifugally obtains the second mixing material, and then distillation obtains the Rice bran crude oil of high nutritive value.
Detect embodiment of the present invention 1-4, adopt commercially available Rice bran crude oil as a control group, its result is as shown in the table:
| Test item | Embodiment 1-4 mean value | Control group |
| Linoleic acid, % | 52 | 38 |
| Leukotrienes, % | 6.4 | 1.2 |
| Content of vitamin E, mg/100g | 112.96 | 96.9 |
| Oryzanol content, % | 2.62 | 1.44 |
| Holding time, year | 3 | 1.5 |
The above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (10)
1. a Rice bran crude oil for high nutritive value, is characterized in that, its raw material comprises by weight: rice bran 200-250 part, grape pip 10-13 part, dessert almond 13-16 part, iblet 20-26 part, coconut meat 23-28 part, peony seeds 5-8 part, walnut kernel 12-15 part, purple perilla seed 12-16 part, fruit of Chinese wolfberry 15-18 part, rosemary 9-12 part, thyme 5-9 part, wild marjoram 15-18 part, myrrh 6-8 part, Momordica grosvenori 2-4 part, coix seed 18-20 part.
2. the Rice bran crude oil of high nutritive value according to claim 1, it is characterized in that, the weight ratio of rice bran, grape pip, dessert almond, iblet, coconut meat is 220-230:11-12:14-15:22-24:25-26.
3. the Rice bran crude oil of high nutritive value according to claim 1 or 2, it is characterized in that, the weight ratio of rice bran, peony seeds, walnut kernel, purple perilla seed, the fruit of Chinese wolfberry, rosemary is 220-230:6-7:13-14:13-15:16-17:10-11.
4. the Rice bran crude oil of high nutritive value according to any one of claim 1-3, it is characterized in that, the weight ratio of rice bran, rosemary, thyme, wild marjoram, myrrh, Momordica grosvenori is 220-230:10-11:6-8:16-17:6.2-7.8:2.5-3.5.
5. the Rice bran crude oil of high nutritive value according to any one of claim 1-4, it is characterized in that, its raw material comprises by weight: rice bran 220-230 part, grape pip 11-12 part, dessert almond 14-15 part, iblet 22-24 part, coconut meat 25-26 part, peony seeds 6-7 part, walnut kernel 13-14 part, purple perilla seed 13-15 part, fruit of Chinese wolfberry 16-17 part, rosemary 10-11 part, thyme 6-8 part, wild marjoram 16-17 part, myrrh 6.2-7.8 part, Momordica grosvenori 2.5-3.5 part, coix seed 18.8-19.6 part.
6. the preparation method of the Rice bran crude oil of high nutritive value as described in any one of claim 1-5, is characterized in that, comprise the steps:
S1, above-mentioned raw materials is cleared up sorting after, be crushed to 30-40 order, mix and obtain mixed material, with Water spray wet mix material, leaving standstill to mixed material water content is that 10-12wt% obtains the first material;
S2, the first material is carried out microwave treatment obtain the second material, microwave power is 500-700w, and microwave treatment time is 80-90s;
S3, the pH of the second material is adjusted to acidity, then adds water and complex enzyme, be warming up to 50-52 DEG C, insulation 2-3h obtains 3 material;
S4,3 material is warming up to 125-130 DEG C, insulation 1-2min, cooling, filtration obtains the first mixing material, adds leaching liquor, stir in the first mixing material, be warming up to 38-42 DEG C, lixiviate 8-9h, centrifugally obtains the second mixing material, and then distillation obtains the Rice bran crude oil of high nutritive value.
7. the preparation method of the Rice bran crude oil of high nutritive value according to claim 6, is characterized in that, in S3, the pH of the second material is adjusted to 4-4.5.
8. the preparation method of the Rice bran crude oil of high nutritive value according to claim 6 or 7, it is characterized in that, in S3, complex enzyme is made up of acid protease and cellulase.
9. the preparation method of the Rice bran crude oil of high nutritive value according to any one of claim 6-8, it is characterized in that, in S3, the weight ratio of the second material, water and complex enzyme is 100:400-500:0.8-1.5.
10. the preparation method of the Rice bran crude oil of high nutritive value according to any one of claim 6-9, it is characterized in that, in S4, leaching liquor is 3-4:0.8-1.5 by n-hexane and isopropyl alcohol by volume.
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