CN102228180B - Betelnut buccal tablet and preparation method thereof - Google Patents
Betelnut buccal tablet and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a betelnut buccal tablet and a preparation method thereof. The betelnut buccal tablet comprises betelnut extractives, starfruit powder, Hainan green orange powder, Hainan green okumquat powder, lemon powder or combination of several lemon powders, a sweetener and magnesium stearate. The preparation method comprises the steps of: crushing and screening dry betelnut; softening the powder at high temperature and high pressure and then carrying out microwave-ultrasonic compound extraction with ethanol; condensing the obtained filtrate in a vacuum state and then drying the product through spray to obtain a betelnut extractive; juicing and filtering fresh starfruits, Hainan green oranges, Hainan green okumquats and lemons; drying through spray to obtain starfruit powder, Hainan green orange powder, Hainan green okumquat powder and lemon powder; pelleting and screening the dried betelnut extractive, the starfruit powder, the Hainan green orange powder, the Hainan green okumquat powder and the lemon powder; and then adding proper sweetener, magnesium stearate and the like for intensive mixing and then tabletting to obtain the betelnut buccal tablet. The invention has the health care effects of refreshing oneself, improving heart and stomach, and the like. The betelnut buccal tablet is eaten as food and health products, and is widely applied to all kinds of people, in particular to fatigue populations such as drivers, and the like. The betelnut buccal tablet is convenient to carry and properly sweet and sour in taste.
Description
Technical field
The present invention relates to a kind of Betelnut buccal tablet and preparation method thereof, be specifically related to a kind ofly take the blue or green cumquat of betel nut, lemon, carambola, Hainan Green Orange and Hainan as raw material, add a kind of Betelnut buccal tablet of other food additives preparations.
Background technology
Betel nut is typical tropical economic plants, occupy first of the Chinese four Da Nan medicines, the nutrient and the beneficiating ingredient that contain multiple needed by human body, such as alkaloid, catechin, choline, fat etc., according to theory of traditional Chinese medical science, betel nut is bitter, hot, temperature, puckery, has expelling phlegm and arresting coughing, helps digestion and sober up, wide chest antiemetic, the worm of dispelling, consumer edema, control beriberi, go the effects such as pestilence and prevention miasma disease.On Africa, some countries of Southeast Asia and China Guangdong, Hainan, Taiwan, Hunan and other places, people have the custom of liking chewing the food betel nut.Current, Chinese traditional areca nut food exploitation begins to take shape, and mainly take fructus arecae immaturi and edible areca-nut head product as main, yet the exploitation of betel nut deep processed product and betel nut medicinal product at present basically or blank.At present, the whole world has at least 5% people to eat betel nut, and betel nut is received by people gradually as the fourth-largest preference after cigarette, alcohol, cocaine.Yet scientific research is in recent years found: excessively chew food betel nut health risk, especially can increase the danger of suffering from carcinoma of mouth, chew the food betel nut and can produce strong chemistry and mechanical stimulus to oral mucosa, make mucous membrane lose normal color and luster and smoothness, cause coarsely, wrinkle and slight crack occur.In addition, excessively have a liking for the food betel nut and may cause " liquor-saturated betel nut reactions " such as giddy, palpitaition, perspirations, based on excessively chewing the impact of food betel nut on health, it is imperative to change current traditional betel nut use habit.According in recent years research find the betel nut alcohol extract have expelling parasite, antibacterial, anti-oxidant, remove free radical, antihyaluronidase isoreactivity, therefore, take the betel nut alcohol extract as raw material, explore Betelnut buccal tablet and preparation thereof, improve the exploitation of betel nut deep processed product, the development of Hainan betel nut processing industry is had great significance.
Summary of the invention
The object of the invention is to: a kind of health-care efficacies such as refreshing oneself, improve stomach that has is provided, use easy to carry, the Betelnut buccal tablet of taste sweet and sour taste.
Another purpose of the present invention provides the preparation method of Betelnut buccal tablet.
Realize above-mentioned purpose, technical scheme of the present invention is: a kind of Betelnut buccal tablet is provided, it is made by the raw material of following weight portion: 20 ~ 70 parts of betelnut extracts, 1 ~ 10 part of lemon powder, 1 ~ 10 part in carambola powder, green orange powder 1 ~ 10 powder, 1 ~ 10 part in blue or green cumquat powder, 5 ~ 20 parts of xylitols, 5 ~ 20 parts in sweet mellow wine, 5 ~ 20 parts of lactose, 0.01 ~ 0.5 part of Sucralose, dolomol is an amount of.
The preparation method of Betelnut buccal tablet of the present invention is to be prepared from according to following step:
1) parts by weights is got the betel nut dry product, crushing screening, sieve mesh is the 20-100 order, betel nut behind the sieve is placed in the pressure cooker, added betel nut weight 5-10 water doubly, under 100 ℃ of boiling water and high pressure, preserve 10-20min, then lay down rapidly pressure, open pot cover, then betel nut and water are changed in the container, add the 10-15 40-80% ethanol doubly of betel nut weight, adopt the compound extractive technique of microwave-ultrasonic, at first adopt microwave to extract 3-5 minute, microwave power is 500-900W, then extracts 10-20 minute with ultrasonic washing instrument, ultrasonic frequency is 20-40kHz, microwave-ULTRASONIC COMPLEX extracts twice, filters merging filtrate with flame filter press;
2) will extract gained betel nut filtrate Vacuum Concentration, the Vacuum Concentration temperature is 35-55 ℃, Vacuum Concentration pressure is 60-100mbar, after being concentrated into the 20-30% of filtrate volume, add again the starch of concentrate volume 10-20%, carry out spray-drying after stirring, inlet temperature is 20-160 ℃, outlet temperature is 60-85 ℃, and pressure is 100-150kPa, and wind flow is 0.35-0.65m
3/ min obtains betelnut extract;
3) get fresh carambola, green orange, blue or green cumquat and lemon, clean respectively, peeling and seed, squeeze the juice, the starch that adds respectively squeezeding juice volume 10-20% after the filtration, carry out spray-drying after stirring, inlet temperature is 120-160 ℃, outlet temperature is 60-85 ℃, and pressure is 100-150kPa, and wind flow is 0.35-0.65m
3/ min obtains carambola powder, green orange powder, blue or green cumquat powder and lemon powder;
4) parts by weights get betelnut extract, carambola powder, green orange powder, blue or green cumquat powder and one or several combined hybrid of lemon powder evenly after, granulation, drying; Sieve mesh is the 20-60 order; Bake out temperature is 50-70 ℃, and drying time is 4-8 hour;
5) get by weight dry powder after the granulation, add sweetener and the dolomols such as an amount of xylitol, sweet mellow wine, lactose, Sucralose, the tablet press machine compressing tablet is made sheet and is got final product.
Lemon powder in the described raw material, carambola powder, green orange powder and blue or green cumquat powder are the acid in the prescription, optional one or more mixtures wherein, its weight portion is respectively: 1 ~ 10 part of 1 ~ 10 part in 1 ~ 10 part in carambola powder, 1 ~ 10 part in green orange powder, blue or green cumquat powder and lemon powder.
Advantage of the present invention just is: according to the achievement of China's theory of traditional Chinese medical science, in conjunction with modern means of science and technology, fully extract the active component in the betel nut, add simultaneously unique flavor behind the raw materials such as lemon powder, carambola powder, blue or green cumquat powder and green orange powder, mouthfeel is better.The Betelnut buccal tablet of the present invention preparation can be avoided directly chewing the harm that the food betel nut brings for a long time, has health-care efficacies such as refreshing oneself, improve stomach, use easy to carry, the taste sweet and sour taste.Lozenge of the present invention can be made into the 0.8g/ sheet, contains clothes, each 1-2 sheet, and every 1-2 hour is once, and its effect of fatigable people is more remarkable to working.
The specific embodiment
The invention will be further described below in conjunction with preferred embodiment, but the present invention never is limited to following embodiment.
Embodiment 1
Prescription:
The green orange powder 10g xylitol 10g sweet mellow wine 10g lactose 5g Sucralose 0.01 ~ 0.5g dolomol of betelnut extract 60g is an amount of.
The preparation method is as follows:
1) parts by weights is got the about 200g of betel nut dry product, crushing screening, sieve mesh is 60 orders, betel nut is placed in the pressure cooker after will sieving, and adds the water of 5 times of betel nut weight, preserves 10min under 100 ℃ of boiling water and high pressure, then lay down rapidly pressure, open pot cover, then betel nut and water are changed in the container, add 15 times 60% ethanol of betel nut weight, adopt the compound extractive technique of microwave-ultrasonic, at first carried out microwave abstracting 3 minutes, microwave power is 800W, then carries out ultrasonic wave and extracts 10 minutes, ultrasonic frequency is 40kHz, microwave-ULTRASONIC COMPLEX extracts twice, filters merging filtrate with flame filter press;
2) with betel nut filtrate Vacuum Concentration, the Vacuum Concentration temperature is 40 ℃, Vacuum Concentration pressure is 80mbar, be concentrated into filtrate volume 20% after, add again the starch of concentrate volume 10%, carry out spray-drying after stirring, inlet temperature is 140 ℃, outlet temperature is 60-85 ℃, and pressure is 130kPa, and wind flow is 0.45m
3/ min obtains betelnut extract;
3) get fresh green orange (Hainan Green Orange is preferred), clean, peeling (seed), squeeze the juice, add the starch of squeezeding juice volume 20% after filtering, carry out spray-drying after stirring, inlet temperature is 140 ℃, outlet temperature is 60-85 ℃, and pressure is 130kPa, and wind flow is 0.45 m
3/ min obtains the Hainan Green Orange powder;
4) get by weight betelnut extract and Hainan Green Orange powder and mix after, granulation, drying; Sieve mesh is 40 orders; Bake out temperature is 50 ℃, and drying time is 8 hours;
5) get by weight dry powder after the granulation, add sweetener and the dolomols such as an amount of xylitol, sweet mellow wine, lactose, Sucralose, the tablet press machine compressing tablet is made sheet and is got final product.
Embodiment 2
Prescription
The blue or green cumquat powder of betelnut extract 60g 5g lemon powder 5g xylitol 10g sweet mellow wine 10g lactose 15g Sucralose 0.01 ~ 0.5g dolomol is an amount of.
The preparation method is as follows:
1) parts by weights is got the about 200g of betel nut dry product, crushing screening, sieve mesh is 60 orders, betel nut is placed in the pressure cooker after will sieving, and adds the water of 10 times of betel nut weight, preserves 20min under 100 ℃ of boiling water and high pressure, then lay down rapidly pressure, open pot cover, then betel nut and water are changed in the container, be incorporated as 15 times 80% ethanol of betel nut weight, adopt the compound extractive technique of microwave-ultrasonic, at first carried out microwave abstracting 5 minutes, microwave power is 900W, then carries out ultrasonic wave and extracts 20 minutes, ultrasonic frequency is 40kHz, microwave-ULTRASONIC COMPLEX extracts twice, filters merging filtrate;
2) with betel nut filtrate Vacuum Concentration, the Vacuum Concentration temperature is 45 ℃, Vacuum Concentration pressure is 100mbar, be concentrated into filtrate volume 30% after, add again the starch of concentrate volume 20%, carry out spray-drying after stirring, inlet temperature is 160 ℃, outlet temperature is 60-85 ℃, and pressure is 110kPa, and wind flow is 0.50 m
3/ min obtains betelnut extract;
3) get respectively fresh blue or green cumquat (the blue or green cumquat in Hainan is preferred) and lemon, clean, remove the peel (seed), squeeze the juice, the starch that adds squeezeding juice volume 15% after filtering, carry out spray-drying after stirring, inlet temperature is 160 ℃, outlet temperature is 60-85 ℃, and pressure is 110kPa, and wind flow is 0.50 m
3/ min obtains respectively the blue or green cumquat powder in Hainan and lemon powder;
4) get by weight the blue or green cumquat powder in Hainan, lemon powder and betelnut extract and mix after, granulation, drying; Sieve mesh is 40 orders; Bake out temperature is 60 ℃, and drying time is 6 hours;
5) get by weight dry powder after the granulation, add sweetener and the dolomols such as an amount of xylitol, sweet mellow wine, lactose, Sucralose, the tablet press machine compressing tablet is made sheet and is got final product.
Embodiment 3
Prescription
Betelnut extract 70g carambola powder 10g xylitol 5g sweet mellow wine 5g lactose 5g Sucralose 0.5g dolomol is an amount of.
The preparation method is as follows:
1) parts by weights is got the about 200g of betel nut dry product, crushing screening, sieve mesh is 50 orders, betel nut is placed in the pressure cooker after will sieving, and adds the water of 8 times of betel nut weight, preserves 10min under 100 ℃ of boiling water and high pressure, then lay down rapidly pressure, open pot cover, then betel nut and water are changed in the container, be incorporated as 10 times 40% ethanol of betel nut weight, adopt the compound extractive technique of microwave-ultrasonic, at first carried out microwave abstracting 4 minutes, microwave power is 900W, then carries out ultrasonic wave and extracts 15 minutes, ultrasonic frequency is 40kHz, microwave-ULTRASONIC COMPLEX extracts twice, filters merging filtrate;
2) with betel nut filtrate Vacuum Concentration, the Vacuum Concentration temperature is 45 ℃, Vacuum Concentration pressure is 100mbar, be concentrated into filtrate volume 30% after, add again the starch of concentrate volume 20%, carry out spray-drying after stirring, inlet temperature is 160 ℃, outlet temperature is 85 ℃, and pressure is 110kPa, and wind flow is 0.50 m
3/ min obtains betelnut extract;
3) get fresh carambola, clean, remove the peel (seed), squeeze the juice, add the starch of squeezeding juice volume 15% after filtering, carry out spray-drying after stirring, inlet temperature is 160 ℃, and outlet temperature is 85 ℃, and pressure is 110kPa, and wind flow is 0.50 m
3/ min obtains the carambola powder;
4) get by weight carambola powder and betelnut extract and mix after, granulation, drying; Sieve mesh is 40 orders; Bake out temperature is 60 ℃, and drying time is 8 hours;
5) get by weight dry powder after the granulation, add sweetener and the dolomols such as an amount of xylitol, sweet mellow wine, lactose, Sucralose, the tablet press machine compressing tablet is made sheet and is got final product.
Embodiment 4
Prescription
Betelnut extract 40g carambola powder 10g lemon powder 10g xylitol 10g sweet mellow wine 10g lactose 15g Sucralose 0.01 ~ 0.5g dolomol is an amount of.
The preparation method is as follows:
1) parts by weights is got the about 200g of betel nut dry product, crushing screening, sieve mesh is 40 orders, betel nut is placed in the pressure cooker after will sieving, and adds the water of 6 times of betel nut weight, preserves 10min under 100 ℃ of boiling water and high pressure, then lay down rapidly pressure, open pot cover, then betel nut and water are changed in the container, be incorporated as 10 times 50% ethanol of betel nut weight, adopt the compound extractive technique of microwave-ultrasonic, at first carried out microwave abstracting 5 minutes, microwave power is 900W, then carries out ultrasonic wave and extracts 20 minutes, ultrasonic frequency is 40kHz, microwave-ULTRASONIC COMPLEX extracts twice, filters merging filtrate;
2) with betel nut filtrate Vacuum Concentration, the Vacuum Concentration temperature is 45 ℃, Vacuum Concentration pressure is 100mbar, be concentrated into filtrate volume 30% after, add again the starch of concentrate volume 20%, carry out spray-drying after stirring, inlet temperature is 160 ℃, outlet temperature is 60-85 ℃, and pressure is 110kPa, and wind flow is 0.50 m
3/ min obtains betelnut extract;
3) get respectively fresh carambola and lemon, clean, remove the peel (seed), squeeze the juice, add the starch of squeezeding juice volume 15% after filtering, carry out spray-drying after stirring, inlet temperature is 160 ℃, and outlet temperature is 60-85 ℃, pressure is 110kPa, and wind flow is 0.50 m
3/ min obtains respectively carambola powder and lemon powder;
4) get by weight carambola powder, lemon powder and betelnut extract and mix after, granulation, drying; Sieve mesh is 40 orders; Bake out temperature is 60 ℃, and drying time is 6 hours;
5) get by weight dry powder after the granulation, add sweetener and the dolomols such as an amount of xylitol, sweet mellow wine, lactose, Sucralose, the tablet press machine compressing tablet is made sheet and is got final product.
The experiment of betel nut alcohol extract mouse anti-reflecting fatigue is as follows:
1 method
1.1 the preparation of sample is extracted betel nut with ethanol, cross polyamide column chromatography after the extract rotary evaporation is concentrated, reclaims 75% ethanol elution part, then rotary evaporation is concentrated into without ethanol and steams, and-4 ℃ of preservations are put in bottling, and are for subsequent use.
1.2 96 of animal used as test cleaning level male mice in kunming, body weight 18～22g is provided by Hunan Hygienic ﹠ Epidemic Prevention Station.
1.3 animal grouping experiment animal at room temperature (25 ± 2 ℃) is fed 12h illumination, 12h dark cycle.Raise basal feed and select to meet 96 of the male mice in kunming of requirement of experiment after one week, be divided at random four groups by body weight, be control group and betel nut alcohol extract low (5 ㎎/㎏), in (10 ㎎/㎏), high (20 ㎎/㎏) three dosage groups, every group 24, every animal gavage amount is pressed the 0.2ml/10g gavage, gavage is 15 days continuously, the isopyknic distilled water of control group gavage.
1.4 instrument and reagent Rotary Evaporators, glass chromatography column, absolute ethyl alcohol, polyamide, blood urea nitrogen testing cassete, muscle glycogen/hepatic glycogen testing cassete, blood lactic acid testing cassete.
1.5 experimental technique
1.5.1 the betel nut alcohol extract on the mouse swimming time affect the betel nut alcohol extract 1h that last gives the mouse various dose after, get 8 mouse for every group, the load sheet lead of 5% body weight of every mouse tail root is put into the swimming trunk of 25 ℃ of water temperatures, depth of water 35cm.Record swimming time with stopwatch, to begin can't finish when the mouse submerged can not float and be placed on the plane righting reflex be that power exhausts sign in swimming certainly.
After 1.5.2 the mensuration last of blood lactic acid gives the betel nut alcohol extract 30min of mouse various dose, get 8 mouse for every group, the swimming trunk went swimming 30min posterior orbit blood sampling that mouse is placed 30 ℃ of water temperatures, depth of water 35cm, according to Nanjing build up bio-engineering research kit method carry out sample pre-treatments and detect BLA.Take NAD+ as hydrogen acceptor, lactic dehydrogenase (LDH) catalysis lactic dehydrogenase produces pyruvic acid, makes NAD+ change into NADH.Wherein PMS passs hydrogen and makes NBT be reduced to purple colour generation thing, the absorbance of colour generation thing when 530nm and lactic acid content linear.
1.5.3 serum urea nitrogen determination last to sample 30 min after, get 8 mouse for every group, be not swimming with a load attached to the body 90 min in 30 ℃ ± 1 the water in temperature, pluck the eyeball blood sampling behind the rest 1h, centrifuging and taking serum press kit specification mensuration mice serum urea nitrogen.The level of serum urea nitrogen reflection blood urine element.Under the condition of strong acid, the urea in the sample and DAM and thiosemicarbazides be warm altogether, generates red complex, and its colored intensity is directly proportional with urea content.Compare through the urea titer with same processing, can obtain the urea nitrogen content in the sample.
1.5.4 the mensuration last of hepatic glycogen and muscle glycogen to sample 30 min after, get 8 mouse for every group, be not swimming with a load attached to the body 90 min in 30 ℃ ± 1 ℃ the water in temperature, recover to put to death behind the 1h, get liver and gastrocnemius and after the physiological saline rinsing, blot with filter paper, carry out the content of sample pre-treatments and mensuration hepatic glycogen and muscle glycogen according to kit method.Glycogen can dewater under the effect of the concentrated sulfuric acid and generate the alditol derivative, and the latter forms blue compound with the anthrone effect again, with the standard glucose solution colorimetric assay of processing with method.Glycogen is highly stable in concentrated base, keeps glycogen so first tissue was put into the concentrated base heating before colour developing to destroy other compositions.
2 results
2.1 the betel nut alcohol extract sees Table 1 to the impact of mouse swimming time:
Table 1 betel nut alcohol extract is on the impact (X ± SD, n=8) of mouse swimming time
As can be seen from Table 1, the betel nut alcohol extract of feeding is very large to the swimming endurance time effects of mouse, low dose group is obviously long than the swimming time of blank group, but the swimming endurance of middle dosage group and high dose group has but descended, and significantly is lower than the swimming time of blank group.Possible cause is exactly when gavage the mouse human body damaged to some extent and causes mouse out of condition, thereby has affected the swimming endurance time of mouse.
2.2 the betel nut alcohol extract sees Table 2 to the impact of Mouse Blood lactic acid and serum urea nitrogen content:
The impact (X ± SD, n=8) of the index of correlation in the table 2 betel nut alcohol extract mouse blood
As can be seen from Table 2, the blood Lactate significant difference of control group and each dosage group, and the Serum lactic acid content between each dosage group is without significant difference.The serum urea nitrogen level of basic, normal, high dosage group mouse and control group significant difference (P＜0.05): there were significant differences for the serum urea nitrogen level of low dose group and middle and high dosage group, but between middle dosage group and the high dose group without significant difference.
2.3 the betel nut alcohol extract sees Table 3 to the impact of Mouse Liver glycogen and muscle glycogen content:
Table 3 betel nut alcohol extract is on the hepatic glycogen that recovers mouse after 1 hour and the impact (X ± SD, n=8) of muscle glycogen content
As seen from Table 3, all without significant difference (P〉0.05), the hepatic glycogen content of high dose group is compared with low, middle dosage group with control group and is had significant difference (P＜0.05) between the hepatic glycogen content of blank group and low, middle dosage group.By the content of muscle glycogen relatively, the impact that the betel nut alcohol extract is identical with hepatic glycogen on the effect existence of muscle glycogen.Be between the muscle glycogen content of blank group and low, middle dosage group all without significant difference (P〉0.05), the hepatic glycogen content of high dose group is compared with other three groups and is had significant difference (P＜0.05).
3 conclusions
Along with the increase of betel nut alcohol extract dosage, significantly improve the content of the muscle glycogen of mouse and hepatic glycogen and reduced the level of blood lactic acid and serum urea nitrogen, can infer that thus the betel nut alcohol extract has improved the speed that organism fatigue recovers to a certain extent.
Lemon acid is sweet, property flat, enters liver, stomach warp; Preventing phlegm from forming and stopping coughing is arranged, promote the production of body fluid, the effect of invigorating the spleen.Be rich in vitamin C, carbohydrate, calcium, phosphorus, iron, vitamin B1, vitamin B2, nicotinic acid, quininic acid, citric acid, malic acid, aurantiamarin, aurantiin, coumarin, a large amount potassium element and low amount sodium element etc.Have diuresis, promote digestion and blood circulation, alleviate headache, and it gives out light fragrance and can make the people in high spirits, the effects such as refrigerant health, calmness or makeup energy, elimination fatigue.
Sweet (sweet) acid of carambola flavor, property is slightly cold, is rich in protein, fat, carbohydrate, organic acid, and a large amount of volatile ingredients and multivitamin and mineral matter.Carambola can reduce body to the absorption of fat, and the effect that reduces blood fat, cholesterol is arranged, and the angiocardiopathies such as hypertension, artery sclerosis are had prevention effect, also can protect liver simultaneously, reduces blood sugar.Contain a large amount of oxalic acid, citric acid, malic acid etc. in the carambola fruit juice, can promote appetite, help digest, treat stomach trouble, jaundice, grass dysentery, dermopathic effect.
Green orange flavor is sweet, warm in nature, contain abundant pectin, protein, calcium, phosphorus, iron and vitamin B1, B2, C wait until multivitamin, be rich in addition organic acid and flavonoids, volatile oil, hesperidine etc., have the effects such as defensive ability/resistance ability of enhance metabolism, delay senility phenomenon and enhancing health.
The blue or green cumquat flavor in Hainan is sweet, warm in nature, contain the many kinds of substances such as protein, cellulose, calcium, phosphorus, iron, Alphalin, B, C and B carrotene, treatment eye illness, cough, asthma, hypertension are arranged, prevent the special efficacy such as artery sclerosis and have special acid fragrant, aromatic flavour.
Above disclosed only is preferred embodiment of the present invention, certainly can not limit with this interest field of the present invention, and the equivalent variations of therefore doing according to claim of the present invention still belongs to the scope that the present invention is contained.
Claims (1)
1. Betelnut buccal tablet, be characterised in that: it is made by the raw material of following weight portion: 20 ~ 70 parts of betelnut extracts, 1 ~ 10 part of lemon powder, 1 ~ 10 part in carambola powder, 1 ~ 10 part in green orange powder, 1 ~ 10 part in blue or green cumquat powder, 5 ~ 20 parts of xylitols, 5 ~ 20 parts in sweet mellow wine, 5 ~ 20 parts of lactose, 0.01 ~ 0.5 part of Sucralose, and dolomol is an amount of; This Betelnut buccal tablet is to be prepared from according to following step:
1) gets by weight the betel nut dry product, crushing screening, sieve mesh is the 20-100 order, betel nut behind the sieve is placed in the pressure cooker, added betel nut weight 5-10 water doubly, under 100 ℃ of boiling water and high pressure, preserve 10-20min, then lay down rapidly pressure, open pot cover, then betel nut and water are changed in the container, add the 10-15 40-80% ethanol doubly of betel nut weight, adopt the compound extractive technique of microwave-ultrasonic, at first adopt microwave to extract 3-5 minute, microwave power is 500-900W, then extracts 10-20 minute with ultrasonic washing instrument, ultrasonic frequency is 20-40kHz, merging filtrate is filtered in the compound extraction twice of microwave-ultrasonic with flame filter press;
2) will extract gained betel nut filtrate Vacuum Concentration, the Vacuum Concentration temperature is 35-55 ℃, Vacuum Concentration pressure is 60-100mbar, after being concentrated into the 20-30% of filtrate volume, add again the starch of concentrate volume 10-20%, carry out spray-drying after stirring, inlet temperature is 160 ℃, outlet temperature is 60-85 ℃, and pressure is 100-150kPa, and wind flow is 0.35-0.65m
3/ min obtains betelnut extract;
3) get fresh carambola, green orange, blue or green cumquat and lemon, clean respectively, peeling and seed, squeeze the juice, the starch that adds respectively squeezeding juice volume 10-20% after the filtration, carry out spray-drying after stirring, inlet temperature is 160 ℃, outlet temperature is 60-85 ℃, and pressure is 100-150kPa, and wind flow is 0.35-0.65m
3/ min obtains carambola powder, green orange powder, blue or green cumquat powder and lemon powder;
4) get by weight betelnut extract, carambola powder, green orange powder, blue or green cumquat powder and lemon powder and mix after, granulation, drying; Sieve mesh is the 20-60 order; Bake out temperature is 50-70 ℃, and drying time is 4-8 hour;
5) get by weight dry powder after the granulation, add an amount of xylitol, sweet mellow wine, lactose, sucralose sweetener and dolomol, the tablet press machine compressing tablet is made sheet and is got final product.
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| CN105815707A (en) * | 2016-04-05 | 2016-08-03 | 海南南派实业有限公司 | Green kumquat powder as well as preparation method and purpose thereof |
| CN106307224A (en) * | 2016-08-27 | 2017-01-11 | 湖南皇爷食品有限公司 | Betel nut buccal tablets and making method thereof |
| CN106343417A (en) * | 2016-08-30 | 2017-01-25 | 湖南皇爷食品有限公司 | Efficient softening method for betel nut |
| CN106418098A (en) * | 2016-09-30 | 2017-02-22 | 许启太 | Betel nut-coconut solid material and preparation method thereof |
| CN106805164A (en) * | 2017-02-07 | 2017-06-09 | 海口椰语堂餐饮文化有限公司 | A kind of preparation method of old salt cumquat lemon powder |
| CN107125755A (en) * | 2017-07-06 | 2017-09-05 | 湖南品来品趣美食有限公司 | A kind of refreshing betel nut and preparation method thereof |
| CN113068810A (en) * | 2021-05-07 | 2021-07-06 | 钟明远 | Improved betel nut processing method |
| CN113439842A (en) * | 2021-05-18 | 2021-09-28 | 吴明 | Areca catechu buccal tablet and preparation method thereof |
| CN115381129A (en) * | 2022-08-23 | 2022-11-25 | 深圳市吉迩科技有限公司 | Buccal tobacco product containing betel nut extract and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1317008C (en) * | 2004-05-20 | 2007-05-23 | 林如海 | Plant extract preparation for preventing and controlling constipation of middle and old age people, and its preparation method |
| CN1824110A (en) * | 2005-12-15 | 2006-08-30 | 北京阜康仁生物制药科技有限公司 | Western bovine bezoar mind clearing medicinal preparation and its new preparation method |
| CN101069732A (en) * | 2006-05-09 | 2007-11-14 | 江西诚志信丰药业有限责任公司 | Chinese compounded preparation for spleen-tonifying, sluggish-eliminating, removing infantile malnutrition and preparing method |
| CN101292732A (en) * | 2007-04-23 | 2008-10-29 | 宁小静 | Food containing betel nut |
| CN101721673A (en) * | 2010-01-05 | 2010-06-09 | 林秀连 | Preparation for soothing liver, regulating Qi, reducing phlegm and relieving sore throat and preparation method thereof |
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