Summary of the invention
The purpose of this invention is to provide a kind of plant insecticide, its kill pests is rapid, and insecticidal spectrum is wide, and insecticidal effect is remarkable, has overcome existing plant insecticide desinsection speed slowly and the shortcoming of insecticidal effect difference.
The present invention also aims to, preparation method, using method and the purposes of this plant insecticide is provided.
First kind of technical scheme of the present invention is, a kind of plant insecticide, its raw materials of effective components percentage by weight consists of: Lappula echinata 7%~9%, Fructus meliae toosendan 26%~29%, the fruit of Rangoon creeper 13%~16%, hairyvein agrimony 26%~29%, levisticum 11%~16% pivot holds 3%~5%, alum 3%~6%, more than the percentage by weight sum of each component be 100%.Pivot holds, and is also referred to as Armstrong.
Second kind of technical scheme of the present invention is that a kind of preparation method of plant insecticide as mentioned above may further comprise the steps:
Step 1, take by weighing following component as raw materials of effective components: Lappula echinata 7%~9% according to percentage by weight, Fructus meliae toosendan 26%~29%, the fruit of Rangoon creeper 13%~16%, hairyvein agrimony 26%~29%, levisticum 11%~16% pivot holds 3%~5%, alum 3%~6%, more than the percentage by weight sum of each component be 100%;
Step 2, Lappula echinata, Fructus meliae toosendan, the fruit of Rangoon creeper, hairyvein agrimony, levisticum He pivot that step 1 is taken by weighing hold component pulverize after, mix with the alum that step 1 takes by weighing, make ball shape solid pharmaceutical preparation according to conventional method.
A kind of preparation method of plant insecticide as mentioned above may further comprise the steps:
Step 1, take by weighing following component as raw materials of effective components: Lappula echinata 7%~9% according to percentage by weight, Fructus meliae toosendan 26%~29%, the fruit of Rangoon creeper 13%~16%, hairyvein agrimony 26%~29%, levisticum 11%~16% pivot holds 3%~5%, alum 3%~6%, more than the percentage by weight sum of each component be 100%;
Step 2, Lappula echinata, Fructus meliae toosendan, the fruit of Rangoon creeper, hairyvein agrimony, levisticum He pivot that step 1 is taken by weighing hold the component pulverizing, soak, decoct, and cooling, filter and remove residue adds the alum component that step 1 takes by weighing in filtrate, be stirred to evenly, promptly gets liquid preparation.
Wherein, in the step 2, soak time is 4~6 hours, and decocting time is 1.5~3 hours.
A kind of preparation method of plant insecticide as mentioned above may further comprise the steps:
Step 1, take by weighing following component as raw materials of effective components: Lappula echinata 7%~9% according to percentage by weight, Fructus meliae toosendan 26%~29%, the fruit of Rangoon creeper 13%~16%, hairyvein agrimony 26%~29%, levisticum 11%~16% pivot holds 3%~5%, alum 3%~6%, more than the percentage by weight sum of each component be 100%;
Step 2, Lappula echinata, Fructus meliae toosendan, the fruit of Rangoon creeper, hairyvein agrimony, levisticum He pivot that step 1 is taken by weighing hold the component pulverizing, soak, decoct, and cooling, filter and remove residue adds the alum component that step 1 takes by weighing in filtrate, be stirred to evenly;
Step 3, the mixed liquor that step 2 is obtained concentrate the back and make the chip solid thing according to conventional method, and at the surface coverage starch layer of gained chip solid thing, oven dry at its surface-coated castor oil, promptly gets the chip solid preparation again.
Wherein, in the step 2, soak time is 4~6 hours, and decocting time is 1.5~3 hours.
Another kind of technical scheme of the present invention is the using method of above-mentioned plant insecticide: at seeding time, together sow with the ball shape solid pharmaceutical preparation seed dressing of this plant insecticide and with plant seed; Or at root system of plant both sides trench digging, the ball shape solid pharmaceutical preparation of this plant insecticide is sowed in ditch, cover with soil.
The using method of above-mentioned plant insecticide: the liquid preparation of this plant insecticide is injected in the trees dimension pipe, or is injected in the trees dimension pipe after the liquid preparation dilution with this plant insecticide.
The using method of above-mentioned plant insecticide: evenly be sprayed on the stem leaves of plants after the chip solid preparation dilution with this plant insecticide.
The application of above-mentioned plant insecticide in the control agriculture and forestry injurious insect.
The application of above-mentioned plant insecticide in control of maize snout moth's larva, apple aphid, cabbage caterpillar prodenia litura, diamond-back moth, black cutworm insect.
The beneficial effect of a kind of plant insecticide of the present invention is:
1, kill pests is rapid, insecticidal spectrum is wide, effect is remarkable.
2 and environmental friendliness.People, animal and small animal are not had any infringement, and wherein contained organic element helps the growth of plant.
Preparation method's step of this plant insecticide of the present invention is simple, and the task equipment of use is few, realize easily, and the demand of different situations when its various formulations that make have made things convenient for practical application, and can suppress the oxidative degradation of plant insecticide active ingredient.
New desinsection approach has been opened up in injection in the demand of different situations when using method of the present invention has satisfied practical application, especially the Qiao Mu Victoria pipe, has enlarged the utilization of pesticides scope.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment.
The mechanism of action of plant insecticide of the present invention is:
1, highlights the effect of infiltration insect epidermis and intersegmental membrane: the present situation that has broken through plant insecticide insecticidal active ingredient infiltration insect epidermis and intersegmental membrane difficulty.Levisticum has the enhancing photosensitization, and alum has the effect of solidifying protein, and the two plays a role simultaneously insect epidermis and intersegmental membrane are festered rapidly, lays a good foundation for other insecticidal active ingredient among the present invention enters in the pest body fast.The invention solves plant insecticide and cause a desinsection difficult problem slowly because of medicine infiltration difficulty.
2, the synergy of insecticidal active ingredient: Lappula echinata paralysis polypide, Fructus meliae toosendan destroys the neuromuscular junction anatomical structure, and the fruit of Rangoon creeper promotes the neuronal cell necrosis, and the three share has the paralysis of enhancing polypide, destroys the effect of insect nervous function rapidly; The Fructus meliae toosendan and the fruit of Rangoon creeper all have the effect that suppresses the insect breathing, and the two share and has quickened the insect respiration inhibition; Hairyvein agrimony and Lappula echinata all have the insect of inhibition cellular metabolism effect, the biogenic energy source of blocking-up insect, and the two share and can quicken each organ function depletion of insect; Levisticum and Fructus meliae toosendan all can promote visceral hemorrhage, and the two share and can quicken the structural damage of insect internal organ; For prevent indivedual insects hide tag may, add pivot Xu , pivot in the prescription of the present invention and hold to have and cause the insect gastrointestinal dysfunction and bring into play the effect that stomach kills, this effect can be used as the additional measure of kill pests.
3, improved insect extracellular fluid osmotic pressure: contained sodium, potassium, calcium, magnesium plasma improved the osmotic pressure of insect extracellular fluid in the prescription of the present invention, and cell is in this outer pendular ring border cell dehydration takes place easily, quickens meronecrosis, promotes insect death.
Embodiment 1
A kind of plant insecticide, its raw materials of effective components percentage by weight consists of: Lappula echinata 7%, Fructus meliae toosendan 26%, the fruit of Rangoon creeper 13%, hairyvein agrimony 29%, levisticum 14% , pivot holds 5%, alum 6%.
The preparation method of above-mentioned this plant insecticide may further comprise the steps:
Step 1, take by weighing following component as raw materials of effective components according to percentage by weight: Lappula echinata 7%, Fructus meliae toosendan 26%, the fruit of Rangoon creeper 13%, hairyvein agrimony 29%, levisticum 14% , pivot holds 5%, alum 6%.
Step 2, Lappula echinata, Fructus meliae toosendan, the fruit of Rangoon creeper, hairyvein agrimony, levisticum He pivot that step 1 is taken by weighing hold component pulverize after, cross 300 mesh sieves, mix with the alum that step 1 takes by weighing, make ball shape solid pharmaceutical preparation according to conventional method, and guarantee that active constituent content accounts for 50%~70% of said preparation gross mass in the gained ball shape solid pharmaceutical preparation.
For the active ingredient that guarantees this plant insecticide is difficult for oxidized decomposition when preserving, the ball shape solid pharmaceutical preparation that makes is packed with black plastic, be convenient to preserve.
Above-mentioned this utilization of pesticides method is: at seeding time, together sow with the ball shape solid pharmaceutical preparation seed dressing of this plant insecticide and with plant seed; Or at root system of plant both sides trench digging, the ball shape solid pharmaceutical preparation of this plant insecticide is sowed in ditch, cover with soil.
Embodiment 2
A kind of plant insecticide, its raw materials of effective components percentage by weight consists of: Lappula echinata 8%, Fructus meliae toosendan 29%, the fruit of Rangoon creeper 13%, hairyvein agrimony 28%, levisticum 11% , pivot holds 5%, alum 6%.
The preparation method of above-mentioned this plant insecticide may further comprise the steps:
Step 1, take by weighing following component as raw materials of effective components according to percentage by weight: Lappula echinata 8%, Fructus meliae toosendan 29%, the fruit of Rangoon creeper 13%, hairyvein agrimony 28%, levisticum 11% , pivot holds 5%, alum 6%.
Step 2, Lappula echinata, Fructus meliae toosendan, the fruit of Rangoon creeper, hairyvein agrimony, levisticum He pivot that step 1 is taken by weighing hold the component pulverizing, soak, decoct, cooling, filter and remove residue adds the alum component that step 1 takes by weighing in filtrate, be stirred to evenly, promptly get liquid preparation, and guarantee that active constituent content accounts for 50%~70% of said preparation gross mass in the gained liquid preparation.Wherein, soak time is 6 hours, and decocting time is 2 hours.
For the active ingredient that guarantees this plant insecticide is difficult for oxidized decomposition when preserving, the liquid preparation can that makes in dark glass bottle or brown soft bag, is convenient to preserve.
Above-mentioned this utilization of pesticides method is: the liquid preparation of this plant insecticide is injected in the trees dimension pipe, or is injected in the trees dimension pipe after the liquid preparation dilution with this plant insecticide.
Embodiment 3
A kind of plant insecticide, its raw materials of effective components percentage by weight consists of: Lappula echinata 9%, Fructus meliae toosendan 27%, the fruit of Rangoon creeper 16%, hairyvein agrimony 26%, levisticum 16% , pivot holds 3%, alum 3%.
The preparation method of above-mentioned this plant insecticide may further comprise the steps:
Step 1, take by weighing following component as raw materials of effective components according to percentage by weight: Lappula echinata 9%, Fructus meliae toosendan 27%, the fruit of Rangoon creeper 16%, hairyvein agrimony 26%, levisticum 16% , pivot holds 3%, alum 3%.
Step 2, Lappula echinata, Fructus meliae toosendan, the fruit of Rangoon creeper, hairyvein agrimony, levisticum He pivot that step 1 is taken by weighing hold the component pulverizing, soak, decoct, and cooling, filter and remove residue adds the alum component that step 1 takes by weighing in filtrate, be stirred to evenly; Wherein, soak time is 4 hours, and decocting time is 3 hours.
Step 3, the mixed liquor that step 2 is obtained concentrate the back and make the chip solid thing according to conventional method, surface coverage starch layer at gained chip solid thing, oven dry, again at its surface-coated castor oil, promptly get the chip solid preparation, and guarantee that active constituent content accounts for 50%~70% of said preparation gross mass in the gained chip solid preparation.
For the active ingredient that guarantees this plant insecticide is difficult for oxidized decomposition when preserving, the chip solid preparation that makes is packed with black plastic, be convenient to preserve.
Above-mentioned this utilization of pesticides method is: evenly be sprayed on the stem leaves of plants after the chip solid preparation dilution with this plant insecticide.
Test one, kill the laboratory test of corn borer:
In the farmland of maize planting, pounce on and grasp 26 corn borers, and be equally divided into first experimental group and second experimental group at random.Get the chip solid preparation of plant insecticide of the present invention, add entry and be configured to the test soup that concentration is 0.01g/ml, get 10 milliliters of above-mentioned test soups, all drip two test soups on every corn borer in first experimental group; Simultaneously kuh-seng Methomyl (plant insecticide that market is buied) is formulated as 10 milliliters of the test soups of 1% concentration, second group every corn borer health is dripped the test soup of two these kuh-seng Methomyls.Find the first experimental group corn borer after 3~5 minutes through observing, promptly begin distortion, struggle that indivedual corn borers began death in 45 minutes, all dead after 90 minutes.And all corn borers of second experimental group are still being creeped after 90 minutes.Result of the test confirms that the present invention kills the corn borer effect and is better than existing plant insecticide kuh-seng Methomyl.
Test two: kill the test of apple aphid:
Plants such as wooly aphis main host plants apple, Malus spectabilis, Chinese pear-leaved crabapple.Harm apple and other fruit tree spray, leaf liquid, tender shoots, often accumulate in apple tree scar, crack and near surface root and draw the nutrition of resin consumption tree body, cause that tree vigo(u)r is weak, photosynthesis goes to pot, leaf abscission, fruit be caducous because of depauperation, can cause when serious that the whole post of plant is withered, total crop failure, until ruining the garden.The thick continuous floccule of apple aphid body surface lining one deck, multiform becomes continuous cotton-shaped projection during gathering, forms a kind of protection barrier, and the killing insects by touching agent is little to its control efficiency.The way that the orchard worker usually adopts alcolhol burner to burn is killed the apple aphid worm, but therefore apple tree also is subjected to grievous injury simultaneously.
Select 6 place's wooly aphis habitats as point of observation and be divided into two groups, every observation group is 3 place's points of observation.First group with liquid preparation of the present invention (concentration is 0.5%) injection its habitat carries out Shu Gan Victoria pipe near the trunk side in, observes wooly aphis habitat white floccule situation of change, and its quantity begins to reduce after two hours, thoroughly disappearance after eight hours.Second group of plant insecticide 5% pyrethrin missible oil that adopts market sale, the same 3 place's wooly aphis worm habitats of selecting, same concentrations with 0.5%, kill apple aphid same method test, observe after eight hours and find: do not have obviously minimizing before the white floccule of lining and the medication.Result of the test confirms that the present invention kills wooly aphis worm effect and is better than the plant insecticide Dalmatian chrysanthemum.
Test three, kill the agricultural experiment of cabbage caterpillar:
The larva of imported cabbageworm is called cabbage caterpillar, and China is widely distributed.Select five groups of viewing test groups at random in the farmland of plantation green vegetables, radish, each experimental group is selected the point of observation of 1 meter=1 square metre of 31 meter * at random, is divided into control group, one group of observation at random and observes two groups, and every group has five points of observation.The dark greyish green borer population of counting five points of observation of control group respectively is as the experimental control number.
The chip solid preparation of getting plant insecticide of the present invention is some, adds entry and is configured to the test soup that concentration is 0.01g/ml.Get market sale product concentration and be 100 milliliters of 1% emulsion oil of Angulatin.The method that adopts randomized, double-blind subsequently evenly is sprayed at the soup of plant insecticide of the present invention and emulsion oil of Angulatin liquid respectively and observes one group of each point of observation with two groups of observations, and the spray liquid of each point of observation is 20 milliliters.One group of difference statistical observation and two groups of insecticidal effects of observation after eight hours.The difference of two groups of cabbage caterpillars survival number and control group is a significant figure, as following table:
|
Control group |
Observe one group |
Observe two groups |
First point of observation |
18 |
16 |
15 |
Second point of observation |
15 |
14 |
12 |
The 3rd point of observation |
17 |
15 |
13 |
The 4th point of observation |
16 |
14 |
10 |
The 5th point of observation |
16 |
15 |
13 |
Add up to |
82 |
74 |
63 |
This tests as calculated mean, standard deviation, and t assay such as following table:
|
Observed number |
Significant figure |
Invalid number |
Efficient % |
Observe one group |
82 |
74 |
8 |
90.24±0.8367 |
Observe two groups |
82 |
64 |
18 |
78.05±1.4832 |
The t check: p<0.01, the two has significant difference.
The test back confirms: observing one group of spray liquid is plant insecticide of the present invention, observes two groups of spray liquids and is existing commercially available emulsion oil of Angulatin liquid.
Conclusion: the cabbage caterpillar effect that plant insecticide of the present invention is killed is better than plant insecticide emulsion oil of Angulatin liquid.
Test four, kill the agricultural experiment of prodenia litura:
Prodenia litura is the worldwide insect of the very assorted gluttony of a kind of feeding habits, and it is general to distribute in China, and all there is generation various places, the harm various vegetables.Each determines totally five groups of one group of viewing test groups in the farmland of plantation capsicum, eggplant, tomato, spinach, five kinds of vegetables of potato, and concrete test method and criterion are all with test three.Kill Spodoptera litura larvae significant figure such as following table for two groups.
|
Control group |
Observe one group |
Observe two groups |
First point of observation |
18 |
17 |
15 |
Second point of observation |
20 |
18 |
17 |
The 3rd point of observation |
17 |
15 |
14 |
The 4th point of observation |
19 |
17 |
13 |
The 5th point of observation |
18 |
16 |
14 |
Add up to |
92 |
83 |
73 |
This tests as calculated mean, standard deviation, and t assay such as following table:
|
Control group |
Significant figure |
Invalid number |
Efficient % |
Observe one group |
92 |
83 |
9 |
90.22±1.1402 |
Observe two groups |
92 |
73 |
19 |
79.35±1.5166 |
The t check: p<0.02, the two has significant difference.
Through examining, observing one group of soup that sprays is that concentration is 1% plant insecticide soup of the present invention, and observing two groups is that commercially available product concentration is 1% Celangulin liquid.
Conclusion: the present invention and Celangulin liquid are killed the two insecticidal effect of prodenia litura there were significant differences, and the present invention kills the efficient Celangulin liquid that is better than of prodenia litura.
Test five, kill the agricultural experiment of diamond-back moth:
Diamond-back moth is the important pests of China brassicaceous vegetable, and all there are distribution in each province, autonomous region, and over past ten years, diamond-back moth has produced pesticide resistance in various degree in the use of chemical pesticide.Select five groups of test sites at random in the farmland of plantation Chinese cabbage, test method and criterion are all with test three.Test data is added up as following table:
|
Control group |
Observe one group |
Observe two groups |
First point of observation |
21 |
15 |
18 |
Second point of observation |
23 |
17 |
21 |
The 3rd point of observation |
19 |
13 |
16 |
The 4th point of observation |
20 |
16 |
17 |
The 5th point of observation |
18 |
12 |
16 |
Add up to |
101 |
73 |
88 |
This tests as calculated mean, standard deviation, and t assay such as following table:
|
Control group |
Significant figure |
Invalid number |
Efficient % |
Observe one group |
101 |
73 |
28 |
72.28±2.7019 |
Observe two groups |
101 |
88 |
13 |
87.13±1.6432 |
The t check: p<0.05, the two has significant difference.
Observing one group of spray liquid is that concentration is 1% commercially available nimbin matrine insecticide, and observing two groups of spray liquids is that concentration is 1% plant insecticide soup of the present invention.
Conclusion: the present invention and nimbin matrine insecticide are killed little tea moth the two are had significant difference, and insecticidal effect of the present invention is better than nimbin matrine insecticide.
The laboratory test of test six, repellent black cutworm
It is standby to catch 60 of black cutworms in the big field of plantation tomato, cucumber, fresh kidney beans, respectively spreads 4 kilograms of shallow soils on 2 glass plates of 1 meter=1 square metre of 1 meter *, identifies A observation group and B observation group respectively.Get commercially available plant insecticide 5% Dalmatian chrysanthemum missible oil and be formulated as 50 milliliters of 2% concentration for 20 milliliters, spray in the soil of A observation group; Soup after the plant insecticide liquid preparation dilution of the present invention of B observation group sprinkling same concentrations same dose.After stirring with soil, the medicine that A, B two observation groups are sprayed is tiled in the test edition.Respectively place 30 black cutworms in two test sites.Place fresh Chinese cabbage, fresh kidney beans vegetable seedling subsequently thereon.Observed 24 hours, and counted the black cutworm number of test site separately, compare with number before the test, the difference of the two is effective repellent number, its result such as following table:
|
Observed number |
Significant figure |
Invalid number |
Effective ratio |
A observation group |
30 |
7 |
13 |
23.33 |
B observation group |
30 |
22 |
8 |
73.33 |
Test data demonstration anthelminthic effect B group is organized apparently higher than A.Repellent black cutworm effect of the present invention is better than the plant insecticide Dalmatian chrysanthemum.
To sum up, the determining of prescription of the present invention and composition proportion content carries out under scientific theory instructs, and the rapid and effect of kill pests effect significantly is two important feature of plant insecticide of the present invention.
Plant insecticide of the present invention can be applied in the control agriculture and forestry injurious insect, especially insects such as control of maize snout moth's larva, apple aphid, cabbage caterpillar prodenia litura, diamond-back moth, black cutworm.