CN102204629B - Feed additive and preparation method thereof - Google Patents
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Abstract
The invention relates to a feed additive and a preparation method thereof, belonging to the technical field of feeds. The feed additive is characterized by comprising the following substances in percentage by weight: 40 percent to 60 percent of dogwood, astragalus, medlar and licorice extract, 30 percent to 50 percent of honeysuckle flower, cortex eucommiae, okra and mimosa pudica extract, 5 percent to 10 percent of fish meal, 0.5 percent to 1 percent of selenium yeast, 0.1 percent to 0.5 percent of compound vitamins, 0.1 percent to 0.2 percent of compound amino acids and 2 percent to 5 percent of spirulina. The feed additive has the advantages of rich raw material sources, low price, no toxic or side effects, effects of preventing various diseases of laying hens and improving immunity and disease resistance of the laying hens, environment-friendliness, high safety, high laying rate, high laying quality, high survival rate of the laying hens, enrichment of selenium, iodine, zinc and other nutrient elements, and the like.
Description
Technical field
The invention belongs to field of feed, be specially a kind of feed addictive and preparation method thereof.
Background technology
Feed addictive is meant and in the feed processing and making process, adds a certain amount of material.The effect of this feed addictive performance can be to have additional nutrients, improve output and quality, ward off disease and infect etc.In recent years; Along with the continuous development of breeding layer chicken industry, some laying hen specialty raisers' cultural technique has not caught up with the fast-developing level of growing aquaculture, and various nonstandard cultural methods cause laying hen egg yield low; The quality of laying eggs and nutritive value are not high; And laying hen is prone to suffer from various diseases, like fowl plague, bird flu, infectiousness tracheitis etc., causes the survival rate of laying hen to reduce.The specialist of raising chickens that also has is in order significantly to increase harmful substances such as the cutability of fryer, abuse clenbuterol hydrochloride; The raiser who has is sick in order to prevent laying hen; Often be employed in and add protide and the materials such as antibiotics or chemical synthetic drug that contain hormone in the chicken feed; The long-term use of these feed addictives not only can cause the drug resistance of pathogen; Also can the chicken body and the institute lay eggs in the residual harmful medicine, have certain toxic and side effect; The abuse that contains the protide feed addictive of hormone; Its residual hormone also makes egg and egg product exist bigger potential safety hazard; This all will be utilized the human health of egg to bring harm, affects the outlet of China's animal products and the development of breeding layer chicken industry.
Chinese herbal medicine is pure natural source, advantage such as have aboundresources, side effect is little, and no noxious material is residual, and is cheap and easy to get.Therefore; Utilize Chinese medicine or natural plant extracts not only can avoid the residual harm that is brought of harmful substance to substitute hormone, antibiotic or chemical synthetic drug as feed addictive; Also have certain nutrient value and prophylactic treatment effect, become the research focus of current aquaculture at present feed addictive.
Fructus Corni is the pulp of Cornaceae plant Fructus Corni, and all there are distribution and cultivation in ground such as China Zhejiang, Henan, Shanxi, Shaanxi, Sichuan, and the quality of its kind has material impact to medicinal material output and quality.Be accustomed to clinically being used as medicine with the ripening fruits of removing seed; Mainly contain compositions such as carbohydrate (glucose, fructose, sucrose), organic acid (gallic acid, malic acid, tartaric acid), iridoids, tannin class, protein, amino acid, vitamin, flavones, anthraquinone, cumarin, vitamin, trace element in the Fructus Corni, have effects such as liver-kidney tonifying, anti-inflammation, enhance immunity power, reduction blood sugar.
Chinese herbal medicine astragalus is the pulse family herbaceos perennial, and its chemical composition comprises various trace elements such as saponins, polysaccharide, amino acid, folic acid and selenium, zinc, copper etc.Have the enhancing body immunologic function, protect the liver, diuresis, adjusting blood-sugar content, anti-ageing, anti-stress, step-down and antibacterial action more widely.
Matrimony vine is the ripening fruits of matrimony vine of solanaceae plant, is that a kind of nutritive value is abundant, the fruit that effect is splendid.The composition such as multiple constant and trace element that mainly contains amino acid, taurine, organic acid, compound sugar, fat, multivitamin, carrotene and the needed by human body of LBP-X, protein, needed by human; Have enhancing body immunity tonifying kidney and benefiting sperm, nourish the liver to improve visual acuity; Transfer blood fat, hypoglycemic; Anti-ageing, antifatigue, anti-sudden change such as protect the liver at effect.
Radix Glycyrrhizae is the root and the root-like stock of glycyrrhizic legume.Contain bioactivators such as a large amount of glycyrrhizic acids, Radix Glycyrrhizae acid amide and licoflavone in the Radix Glycyrrhizae, have well moisten the lung and relieve the cough, purging intense heat and detonicating, beneficial gas bowl spares, relieving spasm to stop pain is in harmonious proportion the effect of the property of medicine.Licoflavone ability restraint of tyrosinase is active, the removing oxyradical, and its oxidation resistance and vitamin E are approaching.A large amount of researchs show that also Radix Glycyrrhizae can neutralize or remove the noxious material in the skin, and have good antiallergy, anti-inflammatory, antivirus action.
Honeysuckle is the bud of caprifoliaceae plant honeysuckle etc., has heat-clearing, detoxifcation, cool blood, clearing and activating the channels and collaterals effect.Mainly contain flavonoids, compositions such as cyanidenon and glycoside, chlorogenic acid, isochlorogenic acid and saponin(e, chlorogenic acid and isochlorogenic acid are the main antimicrobial component in the honeysuckle.Honeysuckle has very strong antibiotic and antivirus action, and staphylococcus aureus, hemolytic streptococcus, dysentery, typhoid fever, diplococcus meningitidis, Diplococcus pneumopniae, green pus and influenza virus etc. are all had obvious inhibitory action.Honeysuckle also has the function of enhance immunity power, can promote lymphocyte transformation, strengthens leukocytic phagocytic activity.Simultaneously honeysuckle also has clearing heat and detoxicating, wind-heat dissipating, anti-inflammatory, antiendotoxin, step-down, reduction serum cholesterol, increases CF; Improve the human body free radical of anti-the anoxic, enhance memory, the effect that delays senility, enhances metabolism, regulates body function, improves aspects such as immunity.
Mainly contain lignanoids, iridoids, plain type of phenylpropyl alcohol and other terpenoid in the bark of eucommia, also have polysaccharide, flavones, phenols, organic acid, amino acid, vitamin, chlorogenic acid, Tea Polyphenols; Multivitamin, compositions such as abundant mineral matter iron, calcium, potassium, phosphorus, zinc, magnesium, selenium.Have and bring high blood pressure down, keep the blood pressure balance; It is active to increase liver cell, recovers liver function; The establishing-Yang diuresis, be beneficial to defaecation, strengthen enterocinesia; The fatigue that refreshes, kidney tonifying is healthy and strong; The expansion capillary strengthens blood circulation; Enhance metabolism the effect of aspects such as enhancing body immunity.
Okra is a Malvaceae Abelmoschus annual herb plant; Contain multiple efficacies compositions such as flavones, polysaccharide, pectin, trace element, amino acid in the okra; Immunity with antifatigue, enhancing endurance and body; Protect the liver strong kidney, anti-ageing, reduce blood sugar, help digest, relieve inflammation or internal heat make eye bright, the effect of aspect such as stomach-invigorating intestine-moisturizing, be a kind of health-care vegetable of good food medicine dual-purpose.
Sensitive plant is the herb of pulse family Mimosa plant sensitive plant.Mainly be distributed in hillside jungle, wetland, the roadside on ground such as China East China, south China, southwest.The research report mainly contains bioactive ingredients such as flavones, phenolic acid class in the sensitive plant, have effects such as tangible reducing fever and causing diuresis, ataralgesia, the diffusing stasis of blood of detoxifcation, hemostasis convergence.
Along with the progress of science and technology, trace elements of selenium also more and more is much accounted of the effect of human health.The expert call people will pay attention to replenishing organic selenium product as paying attention to enriching the iodine both at home and abroad.Organic selenium element can be widely used in producing selenium-enriched food, and it is anti-ageing to the mankind, promote longevity, and is used for diseases such as anti-curing cancers, myopia, cataract, cardiovascular and cerebrovascular diseases, endemic disease and has all brought into play certain function.At food with in producing, organic selenium product replenishers as trace elements of selenium have been widely used.Rare Elements Preparations such as some developed countries' productions and application of selenium have reached suitable scale at present.The healthy nutritive value of organic selenium product is to be difficult to substitute in the product of the same trade.
The main component of spirulina is vitamins, trace element and amino acid, protein, γ-leukotrienes, beta carotene etc., has anticancer, radioresistance, effects such as reducing blood lipid, reduction cholesterol, raising body's immunity.
Summary of the invention
To the problems referred to above that exist in the prior art; The objective of the invention is to design provide a kind of nuisanceless, low-residual, nutrition with disease-resistant be one; Have clearing heat and detoxicating, anti-inflammation, the multiple disease of prevention laying hen, improve the technical scheme of the feed addictive and preparation method thereof of immunity of layer chicken and resistance against diseases; Feed laying hen through in daily chicken feed, adding this additive; To improve laying rate, the quality of laying eggs and the premunition of laying hen, make the egg that produces contain trace elements of selenium, iodine and zinc to the human body beneficial, human consumption this type egg; Eliminated indirectly because microelement deficiencies such as selenium, iodine and zinc to the harm that human body produces, play the effect of extra-nutrition.
Described a kind of feed addictive; It is characterized in that forming: 40%～60% Fructus Corni, the Radix Astragali, matrimony vine, licorice, 30%～50% honeysuckle, the bark of eucommia, okra, sensitive plant extract, 5%～10% fish meal by the following material of weight content; 0.5%～1% selenium yeast; 0.1%～0.5% B B-complex, 0.1%～0.2% compound amino acid, 2%～5% spirulina.
Described a kind of feed addictive, the content that it is characterized in that said Fructus Corni, the Radix Astragali, matrimony vine, licorice is 45%～55%, preferred 50%～53%; The content of said honeysuckle, the bark of eucommia, okra, sensitive plant extract is 35%～45%, and is preferred, 40%～42%; The content 6%～8% of said fish meal; The content of said selenium yeast is 0.6%～0.8%; The content of said B B-complex is 0.2%～0.4%, and the content of said compound amino acid is 0.15%～0.18%, and the content of said spirulina is 3%～4%.
The preparation method of described a kind of feed addictive is characterized in that:
The preparation method of said Fructus Corni, the Radix Astragali, matrimony vine, licorice may further comprise the steps:
Get the drying and crushing of pollution-free, no agricultural chemicals and heavy-metal residual and 1～3 part of 1～3 part of 2～4 parts of Fructus Cornis, matrimony vine, the Radix Astragali, 2～4 parts in the Radix Glycyrrhizae that passes through 20 mesh sieves; Mix the back and adopt water boiling and extraction 1～2 time; If the medicinal material dry weight is 1 kg; Then the consumption of solvent is 8～12 L, and each extraction time is 1～1.5 hour; Suction filtration discards filter residue, and merging filtrate, the extract that obtains adopt Reduced Pressure Concentration Device at 70 ℃～80 ℃, and vacuum is 0.090 Mpa～0.095 Mpa, and solution to be concentrated feed liquor flow velocity is 200-300 mL min
-1Condition under carry out flash concentration, the concentrate medicinal extract that obtains carries out vacuum drying under 50 ℃～60 ℃, obtain extract dry powder;
Said honeysuckle, the bark of eucommia, okra, sensitive plant preparation method of extract may further comprise the steps:
Get the drying and crushing of pollution-free, no agricultural chemicals and heavy-metal residual and 2～4 parts of 1～3 part of 2～4 parts of honeysuckles, the bark of eucommia, okras, 2～4 parts of the sensitive plants that passes through 20 mesh sieves; Adopting 45%～55% ethanol is that solvent refluxing extracts 2～4 times; If the medicinal material dry weight be 1kg then the consumption of etoh solvent be 8～10 liters, each extraction time is 30～45 minutes; Suction filtration, the extract of merging adopt Reduced Pressure Concentration Device at 70 ℃～80 ℃, and vacuum is 0.090 Mpa～0.095 Mpa, and solution to be concentrated feed liquor flow velocity is 250 mL min
-1～350 mL min
-1Condition under carry out flash concentration, the concentrate medicinal extract that obtains carries out vacuum drying under 50 ℃～60 ℃, obtain extract dry powder.
The preparation method of described a kind of feed addictive is characterized in that among the preparation method of said Fructus Corni, the Radix Astragali, matrimony vine, licorice: medicinal material water decocting time is 1.2～1.3 hours; Solution to be concentrated feed liquor flow velocity is 220～280 mL min
-1, preferred 250～260 mL min
-1
The preparation method of described a kind of feed addictive; It is characterized in that in said honeysuckle, the bark of eucommia, okra, the sensitive plant preparation method of extract: concentration of ethanol is 50%～53%; Reflux extracting time is 35～40 minutes, and solution to be concentrated feed liquor flow velocity is 260～320 mL min
-1, preferred 280～300 mL min
-1
Contain vitamin C and vitamin E in the described B B-complex, described compound amino acid contains lysine, methionine.
Above-mentioned a kind of feed addictive with the component of natural plant extracts as premix in the chicken feed, adds other nutrition compositions again, admixes in feed as required to make.Have following beneficial effect:
1, adopt feed addictive of the present invention to sneak into daily forage feed laying hen again, have clearing heat and detoxicating, antibiotic corrosion-resistant effect; Can not only prevent multiple disease, raising immunity of layer chicken and the resistance against diseases of laying hen; Also have well antibacterial and antisepsis, can suppress the mould in the feed, the growth of bacterium.
2, the natural plant extracts in the feed addictive is the pure natural source; Can avoid adding hormone and antibiotics or chemical synthetic drug additive like this; Can not make the chicken of laying hen or the poisonous and harmful substances such as containing hormone, antibiotic, clenbuterol hydrochloride in the egg of producing after the nursing; Guarantee the edible safety of chicken and egg, also improved the survival rate of the laying rate of laying hen, the quality of laying eggs and laying hen simultaneously.
3, the nutriment that adds makes the egg that produces contain nutritional labeling selenium, iodine, zinc and vitamin and amino acid, has higher nutritive value, the egg color and luster of while output should mouthfeel all than common egg.
4, the Chinese medical extract that adds in the feed addictive of the present invention, have raw material sources abundant, cheap, have no side effect, environmental protection, degree of safety are high, the prophylactic treatment effect is obvious, have the advantage of very strong resistance against diseases.
The percentage composition that relates in the present specification unless otherwise indicated all refers to weight percentage.
The specific embodiment
Combine embodiments of the invention and correlation test at present, the present invention is described further.
Embodiment 1
The percentage by weight of this feed addictive consists of: Fructus Corni, the Radix Astragali, matrimony vine, licorice 40%; Honeysuckle, the bark of eucommia, okra, sensitive plant extract 50%; Fish meal 5%, selenium yeast 1%, B B-complex (containing vitamin C and vitamin E) 0.4%; Compound amino acid (containing lysine, methionine) 0.2%, spirulina 4%.
Embodiment 2
The percentage by weight of this feed addictive consists of: Fructus Corni, the Radix Astragali, matrimony vine, licorice 50%; Honeysuckle, the bark of eucommia, okra, sensitive plant extract 40%; Fish meal 6%, selenium yeast 0.5%, B B-complex (containing vitamin C and vitamin E) 0.5%; Compound amino acid (containing lysine, methionine) 0.1%, spirulina 3%.
Embodiment 3
The percentage by weight of this feed addictive consists of: Fructus Corni, the Radix Astragali, matrimony vine, licorice 57%; Honeysuckle, the bark of eucommia, okra, sensitive plant extract 30%; Fish meal 7%, selenium yeast 0.6%, B B-complex (containing vitamin C and vitamin E) 0.3%; Compound amino acid (containing lysine, methionine) 0.2%, spirulina 5%.
Embodiment 4
The percentage by weight of this feed addictive consists of: Fructus Corni, the Radix Astragali, matrimony vine, licorice 48%; Honeysuckle, the bark of eucommia, okra, sensitive plant extract 40%; Fish meal 8%, selenium yeast 1%, B B-complex (containing vitamin C and vitamin E) 0.5%; Compound amino acid (containing lysine, methionine) 0.2%, spirulina 3%.
Embodiment 5
The percentage by weight of this feed addictive consists of: Fructus Corni, the Radix Astragali, matrimony vine, licorice 60%; Honeysuckle, the bark of eucommia, okra, sensitive plant extract 30%; Fish meal 5%, selenium yeast 0.8%, B B-complex (containing vitamin C and vitamin E) 0.4%; Compound amino acid (containing lysine, methionine) 0.1%, spirulina 4%.
Embodiment 6
The percentage by weight of this feed addictive consists of: Fructus Corni, the Radix Astragali, matrimony vine, licorice 45%; Honeysuckle, the bark of eucommia, okra, sensitive plant extract 45%; Fish meal 7%, selenium yeast 0.6%, B B-complex (containing vitamin C and vitamin E) 0.5%; Compound amino acid (containing lysine, methionine) 0.2%, spirulina 2%.
The preparation method of said Fructus Corni, the Radix Astragali, matrimony vine, licorice: get the drying and crushing of pollution-free, no agricultural chemicals and heavy-metal residual and 2 parts of 2 parts of 3 parts of Fructus Cornis, matrimony vines, the Radixs Astragali, 3 parts in the Radix Glycyrrhizae that passes through 20 mesh sieves; Mix the back and adopt water boiling and extraction 2 times; If the medicinal material dry weight is 1 kg; Then the consumption of solvent is 10 L, and each extraction time is 1 hour.Suction filtration discards filter residue, and merging filtrate, the extract that obtains adopt Reduced Pressure Concentration Device at 80 ℃, and vacuum is 0.095 Mpa, and solution to be concentrated feed liquor flow velocity is 250 mL min
-1Condition under carry out flash concentration, the concentrate medicinal extract that obtains carries out vacuum drying under 60 ℃, obtain extract dry powder.In this preparation method: 2 parts of Fructus Cornis, 1 part of matrimony vine, 1 part of the Radix Astragali, 2 parts in Radix Glycyrrhizae, 4 parts of Fructus Cornis, 3 parts of matrimony vines, 3 parts of the Radixs Astragali, 4 parts in Radix Glycyrrhizae; Medicinal material water decocting time is 1.2 hours, 1.3 hours, 1.5 hours; Solution to be concentrated feed liquor flow velocity is 200 mL min
-1, 220 mL min
-1, 260 mL min
-1, 280 mL min
-1, 300 mL min
-1, the vacuum drying temperature is 50 ℃, 55 ℃, and other method is the same, and the extract yield that makes reaches 30.3%～40.8%.
Said honeysuckle, the bark of eucommia, okra, sensitive plant preparation method of extract: get the drying and crushing of pollution-free, no agricultural chemicals and heavy-metal residual and 3 parts of 1 part of 3 parts of honeysuckles, the bark of eucommia, okras, 3 parts of the sensitive plants that passes through 20 mesh sieves; Adopting 50% ethanol is that solvent refluxing extracts 3 times; If the medicinal material dry weight is 1 kg; Then the consumption of solvent is 8 L, and each extraction time is 40 minutes.Suction filtration, the extract of merging adopt Reduced Pressure Concentration Device at 80 ℃, and vacuum is 0.095 Mpa, and solution to be concentrated feed liquor flow velocity is 300 mL min
-1Condition under carry out flash concentration, the concentrate medicinal extract that obtains carries out vacuum drying under 60 ℃, obtain extract dry powder.In this preparation method: 2 parts of honeysuckles, 1 part of the bark of eucommia, 2 parts of okras, 2 parts of sensitive plants, 4 parts of honeysuckles, 3 parts of the barks of eucommia, 4 parts of okras, 4 parts of sensitive plants; Concentration of ethanol is 45%, 53%, 55%, and during refluxing extraction 30 minutes, 35 minutes, 45 minutes, solution to be concentrated feed liquor flow velocity was 250 mL min
-1, 260 mL min
-1, 280 mL min
-1, 350 mL min
-1, other method is the same, and the extract yield that makes reaches 23.5%～31.8%.
The feed addictive for preparing is added in the basal diet of laying hen according to percentage by weight 10%～20%, feed after stirring, take free drinking-water way.After feeding a period of time, prove; Adopt behind this forage feed the laying hen body and produce the egg environmental protection, do not have antibiotic, chemical substance such as hormone is residual; Environmental protection, degree of safety height; And the resistance against diseases of laying hen is strong, the egg that produces contains nutrient selenium, zinc, iodine, and vitamin and amino acid have the laying rate height, the quality of laying eggs reaches advantages such as laying hen survival rate height well.
Described fish meal is that the fresh fish back that gills is dry, after be ground into the product of powder, a kind of animal protein raw material of high-quality.Selenium yeast is selenium yeast sheet (50 μ g * 50 slice/bottle), B B-complex (containing vitamin C and vitamin E), and compound amino acid (containing lysine, methionine), spirulina are that the unicellular alga protist processes.Said fish meal, selenium yeast, B B-complex, compound amino acid, spirulina all can directly buy from market.
Described Reduced Pressure Concentration Device is an existing equipment for design and assembly voluntarily, vacuum drying, can be by directly buying on the market.
1, the contained technical indicator effectively main and nutritional labeling of feed addictive of the present invention is seen table 1.
The contained content (1kg finished product) that effectively reaches nutritional labeling in the feed addictive of table 1 embodiment 1～embodiment 6
| General flavone content | The content of lysine | The content of methionine | The content of vitamin E |
| 2.25~6.67 g | 0.62~1.78 g | 0.45~0.86 g | 1.66~3.04 g |
| Ascorbic content | Se content | Content of iodine | Zinc content |
| 1.23~2.26 g | 12.56~36.13 mg | 89.5～156 mg | 21.7~56.8 mg |
2, the nutritional labeling of the egg that produces is relatively seen table 2. behind the feed addictive of use embodiment 1
3, the laying rate of the egg that produces is relatively seen table 3 behind the feed addictive of use embodiment 3.
The laying rate of the egg that produces compares (lay eggs every day) behind the feed addictive of table 3 use embodiment 3
| ? | Laying hen quantity | The nursing time | 60 days egg productions | Average every day laying rate |
| Normal diet is fed the egg that produces | 30 | 60 days | 31 | 51.7% |
| Feed the egg that produces behind the feed addictive of adding embodiment 3 | 30 | 60 days | 53 | 88.3% |
4, adopt the feed addictive of embodiment 1 invention to add in the daily feed according to certain ratio and feeds laying hen, laying hen quantity is 50, and the ill and survival rate of laying hen is relatively seen table 4.
Ill and the survival rate comparison of table 4 laying hen
| The amount that adds feed addictive of the present invention | The nursing time | Defensive measure | The incidence of disease | Number becomes to live | Survival rate |
| 10% | 60 days | Do not adopt | The chicken crowd does not have disease and takes place | 48 | 96% |
5, adding behind the feed addictive of the present invention in the feed content of beary metal measures and sees table 5.
The assay result of heavy metal in the feed behind the feed addictive of table 5 adding embodiment 1
| Arsenic mg/100g | Plumbous mg/100g | Mercury mg/100g | Copper mg/100g | Chromium mg/100g |
| Do not detect | 0.04 | Do not detect | 11.53 | 0.56 |
Measuring the used instrument of content of elements is: adopt micro-wave digestion-inductively coupled plasma mass spectrometry to measure the content of heavy metal element.X-Series type icp ms (U.S. power & light company); MARS-5 type microwave dissolver (U.S. CE M company) attaches RTP-300 Plus temperature control; Milli-Q Academic ultra-pure water processor (U.S. Millipore company).Nitric acid is that top grade is pure, and it is pure that other reagent are analysis.Instrument working parameter and micro-wave digestion program are seen table 6 and table 7.
Table 6 ICP-MS running parameter
| Running parameter | Setting value | Running parameter | Setting value |
| Forward power/(W) | 1200 | Sampling depth | 130 |
| Scan pattern | Jump the peak | Cooling gas flow/(L min -1) | 13.02 |
| Scanning times | 100 | Secondary air amount/(L min -1) | 0.70 |
| Residence time/(μ s) | 10000 | Atomization gas flow/(L min -1) | 0.84 |
| The sampling time/(s) | 49 | Sample injection time/(s) | 45 |
| Sample lifting rate/(mLmin -1) | 1.0 | Scavenging period/(s) | 60 |
Table 7 micro-wave digestion program
| Clear up program | Power/W | Heating-up time/min | Controlled pressure/kPa | Temperature/℃ | Duration/min |
| 1 | 1200 | 5 | 340 | 120 | 2 |
| 2 | 1200 | 3 | 689 | 150 | 3 |
| 3 | 1200 | 3 | 1000 | 180 | 6 |
Claims (4)
1. the feed addictive of a laying hen; It is characterized in that processing: 40%～60% Fructus Corni, the Radix Astragali, matrimony vine, licorice, 30%～50% honeysuckle, the bark of eucommia, okra, sensitive plant extract, 5%～10% fish meal by the following material of weight content; 0.5%～1% selenium yeast; 0.1%～0.5% B B-complex, 0.1%～0.2% compound amino acid, 2%～5% spirulina;
The preparation method of said Fructus Corni, the Radix Astragali, matrimony vine, licorice may further comprise the steps:
Get the drying and crushing of pollution-free, no agricultural chemicals and heavy-metal residual and 1～3 part of 1～3 part of 2～4 parts of Fructus Cornis, matrimony vine, the Radix Astragali, 2～4 parts in the Radix Glycyrrhizae that passes through 20 mesh sieves; Mix the back and adopt water boiling and extraction 1～2 time; The consumption of solvent is in medicinal material dry weight 1 kg; Be 8-12L, each extraction time is 1～1.5 hour; Suction filtration discards filter residue, and merging filtrate, the extract that obtains adopt Reduced Pressure Concentration Device at 70 ℃～80 ℃, and vacuum is 0.090 Mpa～0.095 Mpa, and solution to be concentrated feed liquor flow velocity is 200-300 mL min
-1Condition under carry out flash concentration, the concentrate medicinal extract that obtains carries out vacuum drying under 50 ℃～60 ℃, obtain extract dry powder;
Said honeysuckle, the bark of eucommia, okra, sensitive plant preparation method of extract may further comprise the steps:
Get the drying and crushing of pollution-free, no agricultural chemicals and heavy-metal residual and 2～4 parts of 1～3 part of 2～4 parts of honeysuckles, the bark of eucommia, okras, 2～4 parts of the sensitive plants that passes through 20 mesh sieves; Adopting 45%～55% ethanol is that solvent refluxing extracts 2～4 times; The consumption of etoh solvent is in medicinal material dry weight 1 kg; Be 8-10L, each extraction time is 30～45 minutes; Suction filtration, the extract of merging adopt Reduced Pressure Concentration Device at 70 ℃～80 ℃, and vacuum is 0.090 Mpa～0.095 Mpa, and solution to be concentrated feed liquor flow velocity is 250 mL min
-1～350 mL min
-1Condition under carry out flash concentration, the concentrate medicinal extract that obtains carries out vacuum drying under 50 ℃～60 ℃, obtain extract dry powder.
2. the feed addictive of a kind of laying hen as claimed in claim 1, the content that it is characterized in that said Fructus Corni, the Radix Astragali, matrimony vine, licorice is 45%～55%; The content of said honeysuckle, the bark of eucommia, okra, sensitive plant extract is 35%～45%; The content 6%～8% of said fish meal; The content of said selenium yeast is 0.6%～0.8%; The content of said B B-complex is 0.2%～0.4%, and the content of said compound amino acid is 0.15%～0.18%, and the content of said spirulina is 3%～4%.
3. the feed addictive of a kind of laying hen as claimed in claim 1, it is characterized in that among the preparation method of said Fructus Corni, the Radix Astragali, matrimony vine, licorice: medicinal material water decocting time is 1.2～1.3 hours; Solution to be concentrated feed liquor flow velocity is 220～280 mL min
-1
4. the feed addictive of a kind of laying hen as claimed in claim 1; It is characterized in that in said honeysuckle, the bark of eucommia, okra, the sensitive plant preparation method of extract: concentration of ethanol is 50%～53%; Reflux extracting time is 35～40 minutes, and solution to be concentrated feed liquor flow velocity is 260～320 mL min
-1
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| CN102524600B (en) * | 2012-02-22 | 2013-02-13 | 长沙学院 | Meat quality improver for grass carps and preparation method for meat quality improver |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1465273A (en) * | 2002-08-14 | 2004-01-07 | 天津市德馨斋路记烧鸡食品有限公司 | Fodder for producing high-selenium egg and selenium enriched chicken |
| CN101181018A (en) * | 2007-12-13 | 2008-05-21 | 济南和美华饲料有限公司 | Hen feedstuff for producing healthy egg |
| CN101543262A (en) * | 2009-04-20 | 2009-09-30 | 邹振可 | Chinese medicinal herb additive for egg chickens and application |
-
2011
- 2011-05-19 CN CN2011101297524A patent/CN102204629B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1465273A (en) * | 2002-08-14 | 2004-01-07 | 天津市德馨斋路记烧鸡食品有限公司 | Fodder for producing high-selenium egg and selenium enriched chicken |
| CN101181018A (en) * | 2007-12-13 | 2008-05-21 | 济南和美华饲料有限公司 | Hen feedstuff for producing healthy egg |
| CN101543262A (en) * | 2009-04-20 | 2009-09-30 | 邹振可 | Chinese medicinal herb additive for egg chickens and application |
Non-Patent Citations (1)
| Title |
|---|
| 葛洪伟 等.中药复方制剂对绿壳蛋鸡生产性能的影响.《中国家禽》.2009,第31卷(第4期), * |
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