CN101946811A - Microencapsulated botanical insect-resist agent - Google Patents
Microencapsulated botanical insect-resist agent Download PDFInfo
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- CN101946811A CN101946811A CN2010102628587A CN201010262858A CN101946811A CN 101946811 A CN101946811 A CN 101946811A CN 2010102628587 A CN2010102628587 A CN 2010102628587A CN 201010262858 A CN201010262858 A CN 201010262858A CN 101946811 A CN101946811 A CN 101946811A
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Abstract
A microencapsulated botanical insect-resist agent comprises 50-70 parts of microcapsule core materials, 5-10 parts of microcapsule adhesives and 20-30 parts of microcapsule wall materials by weight, wherein the core material is one or more of fennel essential oil, folium artemisiae argyi essential oil, cinnamon essential oil and clove essential oil; the adhesive is one or more of gelatine, peach gum, glycerol and ethyl acrylate; and the wall material is one or more of porous starch, cyclodextrin and diatomite. When used for grain storage, the insect-resist agent can achieve the sustained release and efficient insect-resist effects on sitophilus zeamais and tribolium confusum. The insect-resist agent achieves sustained release through one-time use and can lengthen the storage time, reduce the insect-resist working capacity and lower the grain storage cost.
Description
Technical field
The invention belongs to insect-proof agent, particularly a kind of microencapsulation plant resource insect-proof agent.
Background technology
The storage of grain, the very important point are insect protected, and the method and the medicament of insect protected are a lot.The method and the medicament of most insect protected use, the use complicated operation that has, and the needs that have regularly use, and bring very big workload like this, and make carrying cost and strengthen.
Summary of the invention
Technical problem to be solved by this invention is: a kind of microencapsulation plant resource insect-proof agent is provided.Disposable use can continue very long memory time, reduces the insect protected workload, reduces the grain carrying cost.
Technical scheme of the present invention is:
A kind of microencapsulation plant resource insect-proof agent is characterized in that:
By weight:
1) core of microcapsules accounts for 50-70 part
2) binder of microcapsules accounts for 5-10 part
3) the wall material of microcapsules accounts for 20-30 part
Wherein:
Core is: one or more among fennel essential oil, tarragon essential oil, cinnamon essential oil and the clove oil;
Binder is: one or more among gelatin, peach gum, glycerine and the ETHYL CYANOACRYLATE;
The wall material is: one or more in porous-starch, cyclodextrin and the diatomite.
Described microencapsulation plant resource insect-proof agent is characterized in that:
Core is fennel essential oil, tarragon essential oil and cinnamon essential oil 60-70 part
Binder is: glycerine or ETHYL CYANOACRYLATE 8-10 part
The wall material is: porous-starch or diatomite 25-30 part
The tablet of microcapsules through being processed to form, and adopt the nonwoven pouch to pack.
The preparation method of described microencapsulation plant resource insect-proof agent, it is characterized in that: raw material is prepared burden in proportion, and follow these steps to finish: core is dissolved in the 1.0mL atoleine, make the essential oil dilution, add third triketone and the ETHYL CYANOACRYLATE for preparing then respectively, add porous-starch and the diatomite for preparing again, place and stir 15～20min under the electric mixer, its speed of agitator 600～1050r/min fully enters in porous-starch and the diatomite essential oil, makes it to carry out microencapsulation.
Pour the material of microencapsulation in granulator granulation, then granulated materials is put into the tablet press machine compressing tablet, the tablet that presses is put into pouch 60mm * 40mm that nonwoven is made, and every bag of 2-4 sheet seals with the sealing machine thermoplastic, makes microencapsulation plant resource insect-proof agent.
Effect of the present invention is:
Adopt this microencapsulation biological insect-proof agent to carry out foodstuff preservation, can reach the effect of slow release, efficient insect protected corn weevil and confused flour beetle.Disposable use reaches slow release, can continue very long memory time, reduces the insect protected workload, reduces the grain carrying cost.
Embodiment
The invention provides a kind of method for preparing microencapsulation plant resource insect-proof agent, core: fennel essential oil, tarragon essential oil, cinnamon essential oil and one or more plants essential oils of clove oil; Binder: gelatin, peach gum, third triketone and ETHYL CYANOACRYLATE; Wall material: porous-starch, cyclodextrin and diatomite.Fennel essential oil, tarragon essential oil, cinnamon essential oil and four kinds of essential oils of clove oil all have significant vermins-proof effect to corn weevil and confused flour beetle.Four kinds of essential oils are diluted with atoleine obtain dilution, add gelatin, peach gum, third triketone and ETHYL CYANOACRYLATE then, add porous-starch, cyclodextrin and diatomite again, stir with agitator, essential oil is fully entered in the wall material, carry out microencapsulation, put into the pouch that nonwoven is made, seal with the sealing machine thermoplastic, make the microencapsulation biological insect-proof agent.
A kind of microencapsulation plant resource insect-proof agent is grouped into by following one-tenth: by weight
1. core accounts for 50-70 part
2. binder accounts for 5-10 part
3. the wall material accounts for 20-30 part
Wherein: core is one or more among fennel essential oil, tarragon essential oil, cinnamon essential oil and the clove oil; Binder is one or more among gelatin, peach gum, glycerine and the ETHYL CYANOACRYLATE; The wall material is one or more in porous-starch, cyclodextrin and the diatomite.
Best composition is:
Example one:
Core is 60 kilograms of fennel essential oil, tarragon essential oil and cinnamon essential oils
Binder is 8 kilograms of glycerine or ETHYL CYANOACRYLATE
The wall material is 25 kilograms in porous-starch or a diatomite
Example two:
Core is 70 kilograms of fennel essential oil, tarragon essential oil and cinnamon essential oils
Binder is 10 kilograms of glycerine or ETHYL CYANOACRYLATE
The wall material is 30 kilograms in porous-starch or a diatomite
Example three:
Core is 65 kilograms of fennel essential oil, tarragon essential oil and cinnamon essential oils
Binder is 9 kilograms of glycerine or ETHYL CYANOACRYLATE
The wall material is 28 kilograms in porous-starch or a diatomite
Example four:
Core is 50 kilograms of fennel essential oil, tarragon essential oil and cinnamon essential oils
Binder is 5 kilograms of glycerine or ETHYL CYANOACRYLATE
The wall material is 20 kilograms in porous-starch or a diatomite
Production method: above raw material is prepared burden in proportion, and follow these steps to finish: core is dissolved in the 1.0mL atoleine, make the essential oil dilution, add third triketone and the ETHYL CYANOACRYLATE for preparing then respectively, add porous-starch and the diatomite for preparing again, place and stir 15～20min, its speed of agitator 600～1050r/min under the electric mixer, essential oil is fully entered in porous-starch and the diatomite, make it to carry out microencapsulation.Pour material in granulator granulation, then granulated materials is put into the tablet press machine compressing tablet, the tablet that presses is put into the pouch that nonwoven makes, and (60mm * 40mm), every bag of 2-4 sheet seals with the sealing machine thermoplastic, makes the microencapsulation biological insect-proof agent.Its profile is a tablet, and adopts the nonwoven pouch to pack.
Claims (4)
1. microencapsulation plant resource insect-proof agent is characterized in that:
By weight:
1) core of microcapsules accounts for 50-70 part
2) binder of microcapsules accounts for 5-10 part
3) the wall material of microcapsules accounts for 20-30 part
Wherein:
Core is: one or more among fennel essential oil, tarragon essential oil, cinnamon essential oil and the clove oil;
Binder is: one or more among gelatin, peach gum, glycerine and the ETHYL CYANOACRYLATE;
The wall material is: one or more in porous-starch, cyclodextrin and the diatomite.
2. microencapsulation plant resource insect-proof agent according to claim 1 is characterized in that:
Core is fennel essential oil, tarragon essential oil and cinnamon essential oil 60-70 part
Binder is: glycerine or ETHYL CYANOACRYLATE 8-10 part
The wall material is: porous-starch or diatomite 25-30 part
The tablet of microcapsules through being processed to form, and adopt the nonwoven pouch to pack.
3. the preparation method of microencapsulation plant resource insect-proof agent according to claim 1 and 2, it is characterized in that: raw material is prepared burden in proportion, and follow these steps to finish: core is dissolved in the 1.0mL atoleine, make the essential oil dilution, add third triketone and the ETHYL CYANOACRYLATE for preparing then respectively, add porous-starch and the diatomite for preparing again, place and stir 15～20min under the electric mixer, its speed of agitator 600～1050r/min, essential oil is fully entered in porous-starch and the diatomite, make it to carry out microencapsulation.
4. the preparation method of microencapsulation plant resource insect-proof agent according to claim 3; it is characterized in that: pour the material of microencapsulation in granulator granulation; then granulated materials is put into the tablet press machine compressing tablet; the tablet that presses is put into pouch 60mm * 40mm that nonwoven is made; every bag of 2-4 sheet; seal with the sealing machine thermoplastic, make microencapsulation plant resource insect-proof agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010262858 CN101946811B (en) | 2010-08-26 | 2010-08-26 | Microencapsulated botanical insect-resist agent |
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| CN 201010262858 CN101946811B (en) | 2010-08-26 | 2010-08-26 | Microencapsulated botanical insect-resist agent |
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| CN101946811A true CN101946811A (en) | 2011-01-19 |
| CN101946811B CN101946811B (en) | 2013-07-31 |
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Cited By (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102084863A (en) * | 2011-03-01 | 2011-06-08 | 刘鹏 | Slow-release preparation of slow-release thiadiazine substances |
| CN102165952A (en) * | 2011-03-01 | 2011-08-31 | 刘鹏 | Sustained-release benzothiazole ammonium salt |
| CN102388958A (en) * | 2011-10-11 | 2012-03-28 | 华南农业大学 | Method for controlling grain pest by using essential oil |
| CN102492551A (en) * | 2011-12-21 | 2012-06-13 | 佰香汇生物科技（厦门）有限公司 | Preparation method for novel long-acting solid aromatic agent |
| CN102492557A (en) * | 2011-11-24 | 2012-06-13 | 西华大学 | Preparation method for olive oil-embedded powder by using porous starch |
| CN103229830A (en) * | 2013-04-03 | 2013-08-07 | 广东工业大学 | Gas-phase sustained-release mildew-resistant antistaling agent, and preparation method and application thereof |
| CN103329697A (en) * | 2013-06-06 | 2013-10-02 | 青川县食用菌科研开发中心 | Konjak planting method |
| CN104207076A (en) * | 2014-09-17 | 2014-12-17 | 天津春发生物科技集团有限公司 | Method for preparing essential oil microcapsules |
| CN104872280A (en) * | 2015-05-27 | 2015-09-02 | 闭炳春 | Cinnamon oil containing grain insecticide |
| CN104872215A (en) * | 2015-05-27 | 2015-09-02 | 闭炳春 | Micro-encapsulated plant essential oil mosquito repellent containing cinnamon oil |
| CN105028512A (en) * | 2015-06-17 | 2015-11-11 | 湖州道场污水处理有限公司 | Preparation method for cinnamonandlavender-containing environment-friendly pesticide |
| CN105076129A (en) * | 2014-04-22 | 2015-11-25 | 广东华润涂料有限公司 | Insecticide microcapsules and preparation method thereof |
| CN105532754A (en) * | 2016-02-03 | 2016-05-04 | 中南林业科技大学 | Natural plant composition extract for controlling grain worms and mildew |
| CN106172748A (en) * | 2016-07-28 | 2016-12-07 | 和县金城米业有限责任公司 | A kind of food storage insect protected medicament and preparation method thereof |
| CN106212455A (en) * | 2016-07-28 | 2016-12-14 | 和县金城米业有限责任公司 | A kind of food storage prevents medicament of going mouldy and preparation method thereof |
| CN106879640A (en) * | 2017-03-24 | 2017-06-23 | 李军 | The vegetable insecticide microcapsules and its preparation technology of a kind of clove oil synergy |
| CN107375628A (en) * | 2017-06-28 | 2017-11-24 | 安徽省黄淮兽药有限公司 | A kind of micro-capsule loads plant source fish insect killing agent |
| CN107950606A (en) * | 2017-12-06 | 2018-04-24 | 河南科技学院 | A kind of sitophilus zea-mais repellant based on P-Cymene and preparation method thereof |
| CN108219940A (en) * | 2017-12-27 | 2018-06-29 | 安徽香博士芳香技术研究院有限公司 | A kind of sterilization microcapsule fragrance |
| CN108978190A (en) * | 2018-06-25 | 2018-12-11 | 太极石股份有限公司 | A kind of antibiosis anti-acarien far infrared health care cellulose fibre and its preparation method and application |
| CN109455384A (en) * | 2018-12-12 | 2019-03-12 | 天津科技大学 | A kind of rice mould-proof disinsectization preservation device and application method |
| CN111870544A (en) * | 2020-08-11 | 2020-11-03 | 青岛美今生物科技有限公司 | Formula and preparation method of sustained-release fragrance-lasting shampoo |
| CN112931539A (en) * | 2021-03-12 | 2021-06-11 | 中南粮油食品科学研究院有限公司 | Rice composite insect-resist agent and preparation method and application thereof |
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Cited By (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102084863A (en) * | 2011-03-01 | 2011-06-08 | 刘鹏 | Slow-release preparation of slow-release thiadiazine substances |
| CN102165952A (en) * | 2011-03-01 | 2011-08-31 | 刘鹏 | Sustained-release benzothiazole ammonium salt |
| CN102388958A (en) * | 2011-10-11 | 2012-03-28 | 华南农业大学 | Method for controlling grain pest by using essential oil |
| CN102492557A (en) * | 2011-11-24 | 2012-06-13 | 西华大学 | Preparation method for olive oil-embedded powder by using porous starch |
| CN102492551A (en) * | 2011-12-21 | 2012-06-13 | 佰香汇生物科技（厦门）有限公司 | Preparation method for novel long-acting solid aromatic agent |
| CN103229830A (en) * | 2013-04-03 | 2013-08-07 | 广东工业大学 | Gas-phase sustained-release mildew-resistant antistaling agent, and preparation method and application thereof |
| CN103329697A (en) * | 2013-06-06 | 2013-10-02 | 青川县食用菌科研开发中心 | Konjak planting method |
| CN103329697B (en) * | 2013-06-06 | 2014-12-17 | 青川县食用菌科研开发中心 | Konjak planting method |
| CN105076129A (en) * | 2014-04-22 | 2015-11-25 | 广东华润涂料有限公司 | Insecticide microcapsules and preparation method thereof |
| CN104207076A (en) * | 2014-09-17 | 2014-12-17 | 天津春发生物科技集团有限公司 | Method for preparing essential oil microcapsules |
| CN104872280A (en) * | 2015-05-27 | 2015-09-02 | 闭炳春 | Cinnamon oil containing grain insecticide |
| CN104872215A (en) * | 2015-05-27 | 2015-09-02 | 闭炳春 | Micro-encapsulated plant essential oil mosquito repellent containing cinnamon oil |
| CN104872215B (en) * | 2015-05-27 | 2017-11-03 | 闭炳春 | Microencapsulation plants essential oil culicifuge containing cinnamon oil |
| CN105028512A (en) * | 2015-06-17 | 2015-11-11 | 湖州道场污水处理有限公司 | Preparation method for cinnamonandlavender-containing environment-friendly pesticide |
| CN105532754B (en) * | 2016-02-03 | 2018-08-07 | 中南林业科技大学 | A kind of infested natural plants combined extracts to go mouldy of prevention grain |
| CN105532754A (en) * | 2016-02-03 | 2016-05-04 | 中南林业科技大学 | Natural plant composition extract for controlling grain worms and mildew |
| CN106172748A (en) * | 2016-07-28 | 2016-12-07 | 和县金城米业有限责任公司 | A kind of food storage insect protected medicament and preparation method thereof |
| CN106212455A (en) * | 2016-07-28 | 2016-12-14 | 和县金城米业有限责任公司 | A kind of food storage prevents medicament of going mouldy and preparation method thereof |
| CN106879640A (en) * | 2017-03-24 | 2017-06-23 | 李军 | The vegetable insecticide microcapsules and its preparation technology of a kind of clove oil synergy |
| CN107375628A (en) * | 2017-06-28 | 2017-11-24 | 安徽省黄淮兽药有限公司 | A kind of micro-capsule loads plant source fish insect killing agent |
| CN107375628B (en) * | 2017-06-28 | 2020-06-16 | 安徽省凯强生物科技有限公司 | Microcapsule-loaded plant source fishing pesticide |
| CN107950606A (en) * | 2017-12-06 | 2018-04-24 | 河南科技学院 | A kind of sitophilus zea-mais repellant based on P-Cymene and preparation method thereof |
| CN107950606B (en) * | 2017-12-06 | 2020-10-16 | 河南科技学院 | Corn elephant repellent based on folium artemisiae argyi essential oil and preparation method thereof |
| CN108219940A (en) * | 2017-12-27 | 2018-06-29 | 安徽香博士芳香技术研究院有限公司 | A kind of sterilization microcapsule fragrance |
| CN108978190A (en) * | 2018-06-25 | 2018-12-11 | 太极石股份有限公司 | A kind of antibiosis anti-acarien far infrared health care cellulose fibre and its preparation method and application |
| CN109455384A (en) * | 2018-12-12 | 2019-03-12 | 天津科技大学 | A kind of rice mould-proof disinsectization preservation device and application method |
| CN111870544A (en) * | 2020-08-11 | 2020-11-03 | 青岛美今生物科技有限公司 | Formula and preparation method of sustained-release fragrance-lasting shampoo |
| CN112931539A (en) * | 2021-03-12 | 2021-06-11 | 中南粮油食品科学研究院有限公司 | Rice composite insect-resist agent and preparation method and application thereof |
| CN112931539B (en) * | 2021-03-12 | 2022-03-04 | 中南粮油食品科学研究院有限公司 | Rice composite insect-resist agent and preparation method and application thereof |
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| CN101946811B (en) | 2013-07-31 |
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