CN104872280A - Cinnamon oil containing grain insecticide - Google Patents
Cinnamon oil containing grain insecticide Download PDFInfo
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- CN104872280A CN104872280A CN201510277123.4A CN201510277123A CN104872280A CN 104872280 A CN104872280 A CN 104872280A CN 201510277123 A CN201510277123 A CN 201510277123A CN 104872280 A CN104872280 A CN 104872280A
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Abstract
The invention belongs to the technical field of grain storage and particularly relates to a cinnamon oil containing grain insecticide which is prepared from the following raw materials in mass percent: 10-14% of cinnamon oil, 2-5% of garlic essential oil, 5-8% of chinaberry oil, 1-4% of turpentine, 1-4% of citionella oil, 2-5% of star anise oil, 1-4% of rue essential oil and the balance of 75% ethyl alcohol in volume concentration. The cinnamon oil containing grain insecticide is prepared from the natural plant essential oil, safe, environment-friendly and pollution-free and can effectively play the effects of sterilization and insect killing.
Description
Technical field
The invention belongs to foodstuff preservation field, be specifically related to a kind of grain insecticide containing cinnamon oil.
Background technology
According to related data introduction, in the annual food storage process of China, the loss that grain causes because of the harm of insect, mite class and mould at storage period is serious, particularly because insect pest mould causes grain loss to reach 5-10%, the Quality Grade of the grain had a strong impact on, to making grain taste electrochromic variable, after edible, bring out a series of disease of people and animals.Mostly Chemical treatment is adopted in the existing food storage process of China, impact is had on Class of food crop, to the pollution all in various degree of people and animals, environment, traditional chemical agent is difficult to the great variety adapting to grain storage system generation, is also difficult to the storage adapting to increases in grain production.
Some prior aries about grain desinsection are as follows at present:
Chinese patent, application number: 201410187459.7; Applicant: Zeng Qingguo; Address: Shuyang County, Xiuqian City of the Jiangsu Province height market town People's Government; Denomination of invention: a kind of wide spectrum, environmental protection grain storage fumigant; Summary: a kind of wide spectrum, environmental protection grain storage fumigant, be made up of following component: ether acyl lopseed element, athomin, Ethyl formate, cinnamon essential oil.The present invention has following advantages effect: good disinsection effect, act on the advantages such as rapid, easy to operate, disposal cost is low; This product is nontoxic to people, livestock, and to object of protection non-corrosiveness, murder by poisoning, it is high volatility that medicament uses, nonflammable, do not explode, Product processing easily, store convenient transportation.
Chinese patent, application number: 201410186680.0; Applicant: Ye Weiqian; Address: No. 30, height market town Gao Xu street, Shuyang County, Xiuqian City of Jiangsu Province; Denomination of invention: a kind of vegetalitas mildewproof insecticide for grains; Summary: a kind of vegetalitas mildewproof insecticide for grains, by component: turpentine oil, China pink oil, rotenone, triptolide, matrine form.The present invention has following advantages effect: this botanical pesticide has free from environmental pollution, safer to people and animals, and insect not easily produces the features such as resistance.Simultaneously faint to mammalian selective toxicity; In the environment without persistent residual; Varied to the mode of action of controlling object, show as poisoning, food refusal, avoid and keep away and suppress population, lure, anaesthetize and Developing restraint growth etc.; Disease and pest not easily produces resistance; Working condition is gentle, expense is low
Chinese patent, application number: 201310391262.0; Applicant: Gansu Chinese of Traditional Chinese Medicine; Address: No. 35, East Road, Dingxi road, Lanzhou City, Gansu Province; Denomination of invention: a kind of composition of sterilization and disinsection and smoke agent, preparation method; Summary: the invention discloses a kind of composition of sterilization and disinsection, smoke agent and preparation method thereof, its component and weight proportion are: the tuber of stemona 1 ~ 42 part, Chinese cassia tree 1 ~ 23 part, 1 ~ 21 part, turmeric, cloves 1 ~ 25 part, through extracting, obtain medicinal extract; Again described medicinal extract and 1 ~ 37 part, potassium chlorate, 1 ~ 37 part, potassium nitrate, wood powder 1 ~ 46 part, ammonium chloride 1 ~ 34 part, talcum powder 1 ~ 49 part, superfine silica gel powder 0.2 ~ 9 part are made smoke agent.Scientific formulation of the present invention, technique are simple, and obtained product has the effect of sterilization and disinsection, are applicable to the control of Chinese medicine, cereal crops, grain depot, trees flowers and greenhouse vegetable disease and pest.
Chinese patent, application number 201010200184.8; Applicant: Zhengzhou University; Address: No. 100, Zhengzhou, Henan Province science main road; Denomination of invention: a kind of tobacco matrix composite biological insecticide and manufacture method thereof; Summary: the invention provides a kind of tobacco matrix composite biological insecticide and manufacture method thereof.At least comprise in this composite biological insecticide to a kind of tobacco plant source insect disinfestation component and at least one microbial source insect disinfestation component, choosing tobacco waste is raw material, makes through insecticidal microorganism fermentation.Operating procedure comprises the preparation of culture medium, the expansion cultivation of bacterial classification, biological insecticides fermentation and extraction etc.; Zymotechnique can adopt liquid fermentation method or solid state fermentation.Tobacco matrix composite biological insecticide of the present invention not only containing insecticidal microorganism and metabolite thereof, and containing tobacco insecticidal constituent (as nicotine etc.), has dual insecticidal effect; The inventive method can make full use of the tobacco waste resource not yet obtaining Appropriate application at present, and resource of saving food, produces good economic benefit, ecological benefits and social benefit.
Summary of the invention
The object of this invention is to provide a kind of grain insecticide containing cinnamon oil, this grain insecticide is that raw material is prepared from natural plant essential oils, safety, environmental protection, pollution-free and effectively can play the effect of sterilization, desinsection.
In order to realize object of the present invention, the present invention adopts following technical scheme: a kind of grain insecticide containing cinnamon oil, is characterized in that, comprise the raw material of following percentage composition:
Cinnamon oil 10%-14%;
Galic essential oil 2%-5%;
Neem oil 5%-8%;
Turpentine oil 1%-4%;
Citronella oil 1%-4%;
Oil of badian 2%-5%;
ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS 1%-4%;
All the other are the ethanol of volumetric concentration 75%.
The preparation method of the above-mentioned grain insecticide containing cinnamon oil, specifically comprises the steps: to take cinnamon oil according to the proportioning of above-mentioned percentage composition; Galic essential oil; Neem oil; Turpentine oil; Citronella oil; Oil of badian and ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS, make it fully mix, and then adds the ethanol that volumetric concentration is 75%, complement to 100%, stir, and essential oil and ethanol fully mixed and can obtain the grain insecticide containing cinnamon oil of the present invention.
Cinnamon oil, is canella Chinese cassia tree [Classification system]
cinnamomum cassia Preslthe volatile oil that obtains through steam distillation of dry branch, leaf, be supernatant liquid that is yellow or yellowish-brown.Cinnamon oil has natural insect-repelling desinsection, fungicidal effect, again can not contaminated food.Cinnamon oil is to common bacteria (Escherichia coli, salmonella, bacillus subtilis, Dipel etc.), saccharomycete (brewer's yeast, Saccharomyces cerevisiae etc.), mould (aspergillus niger, aspergillus oryzae, aspergillus flavus, mould, mould, the Mucor of wood, head mold etc.) all have very strong inhibitory action, cinnamon oil is the strongest to the inhibitory action of mould, has good volatility.In addition cinnamon oil is to the smoked kill as excellent in sitophilus zea-mais, red flour beetle etc. have of grain storage pest and contact efficacy.
Galic essential oil, [Classification system] of garlic
allium sativumit is a kind of medicine of antibiotic and sterilizing, to the effect that multiple coccus and Escherichia coli, typhoid bacillus, shigella dysenteriae, bacillus pertussis and mould, virus, amoeba worm, burning worm etc. have good suppression and kill, in addition, reduce the function of cholesterolemia, triglyceride and lipoprotein in addition, tablet, oral liquid or glucose drip solution Clinical practice can be made, the daily edible resistance against diseases that also can increase human body of garlic essence oral liquid.Galic essential oil is multicomponent mixture, and the sulfide compound be made up of allicin, Allicin and multiple pi-allyl and methyl forms.Galic essential oil has the effect that antibacterium, fungi and white read coccus, also plays certain suppression, smoked kill and action of contace poison to grain storage pest.Active component in galic essential oil has stronger inhibitory action to many plant pathogenic fungis and food miscellaneous bacteria, is usually used in preventing and treating diseases and pests of agronomic crop.
Oil of badian, obtains through steam distillation Illicillm Verum Fruit, [Classification system] of Chinese anise
illicium verumits main component is: anethole, safrole, cineole, anisaldehyde, fenchone, benzoic acid, palmitic acid, terpinol, fanesol, firpene, phellandrene, citrene, carypohyllene, bisabolene, farnesene etc.Oil of badian has antibacterial, antibacterial action preferably, and experiment in vitro shows: alcohol extract is to gram-positive bacteria as staphylococcus aureus, pneumococcus, corynebacterium diphtheriae etc. have bacteriostasis, and its effect is similar to potassium salt of penicillin 20 units/mL; To gram-negative bacteria as hay bacillus, Escherichia coli, comma bacillus and typhoid bacillus, paratyphosum Bacterium, shigella dysenteriae etc. also have bacteriostasis, its effect is similar to streptomycin sulphate 50 units/mL; The bacteriostasis of fungi is greater than to benzoic acid and the salicylic acid of 1%.Oil of badian has better insecticidal activity and Green Tea Extract oxidation, has strong smoked kill and action of contace poison to insect.
Neem oil, is margosa [Classification system]
melia azedarach L., and the oil that seed extract.Neem oil contain one be called nimbin (
azadirachtin) chemical composition, there is potent antimicrobial acivity, there is insecticidal effect simultaneously, can be used as natural insecticide.Plant sprays China tree extract, plant can be made to become and be not very good eating, and stop insect's food-taking, as insect continues to take food, then can suppress laying eggs and decortication ability of insect.Neem oil is harmless nontoxic to people, animal, birds, complete environmental protection.The scope of the anti-system of neem oil is very extensive, comprises aphid, Gypsy dance moth, leaf mining insect, geometer, powder scale insect, thrips and aleyrodid etc.Also can kill importance insect, as potato leaf beetle, corn earworm, leaf flea beetle worm etc., also have effect of control for powdery mildew, dew bacterium disease, anthracnose, rust etc. in addition.
Turpentine oil, be the liquid extracted from the rosin of coniferale plant by distillation or other method, main component is terpenes.Turpentine oil is a kind of natural essential oil, and being the mixture of the multiple terpene hydro carbons based on firpene, having distinctive chemism, is coating, artificial camphor, terpinol, synthetic perfume, medicine, synthetic resin, the aspect industrial chemicals such as organic chemical industry.As paint solvent and synthetic perfume, also make agrochemical medicinal raw material.Except rosin turpentine oil, also have with the extraction turpentine oil of pine stump pine torch organic solvent lixiviate, the destructive distillation turpentine obtained by distillation needle timber and the turpentine oil reclaimed from paper industry.
Citronella oil, [another name] vanilla flavour concentrate, citronellol.[Classification system] of lemongrass
elsholtzia ciliata (Thunb.) Hyland.obtained through steam distillation by the herb of lemongrass, weak yellow liquid, has strong Chinese pepper fragrance, and main component is citronellal, geraniol and citronellol, for extracting citronellal, for synthesis of hydroxy citronellal, geraniol and menthol. also can be used as pesticide, anophelifuge and soap perfume.
ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS utilizes steam distillation, from rue [Classification system]
ruta graveolens L.the secondary metabolite of middle extraction.Because essential oil contains Antimicrobial preservative composition, ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS is scattered capable of purifying air in atmosphere, reduce and pollute, mosquito density can be reduced in garden cultivation, therefore be widely used in afforestation, plants essential oil removing insect has outside higher activity, also has people and animals' nonhazardous, the advantage such as free from environmental pollution, insect not easily develops immunity to drugs, can become desirable biological pesticide.ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS high volatility, antibacterial and anti-virus ability is strong.
Compared with prior art, the invention has the beneficial effects as follows
:
1, the present invention is that raw material is prepared from natural plant essential oils containing the grain insecticide of cinnamon oil, safety, environmental protection, pollution-free, insect not easily produces resistance and used often kind raw material to be had and has obvious smoked kill and action of contace poison to the insect occurred normal in grain storing granary.
2, the reasonable assembly of various raw materials that the present invention is used makes its use, can play the effect of Synergistic, bactericidal action and more strong to the smoked kill effect of storage pest, to the effect needing the grain stored to play good expelling parasite, desinsection and sterilization.
3, preparation cost of the present invention is cheap, and preparation technology is simple, easy to use and safe and efficient, cheap; Nontoxic to people, livestock, to object of protection non-corrosiveness, murder by poisoning.
4, the present invention adopts cinnamon oil to be one of primary raw material, it has natural insect-repelling desinsection, fungicidal effect, again can not contaminated food, to common bacteria (Escherichia coli, salmonella, bacillus subtilis, Dipel etc.), saccharomycete (brewer's yeast, Saccharomyces cerevisiae etc.), mould (aspergillus niger, aspergillus oryzae, aspergillus flavus, mould, mould, the Mucor of wood, head mold etc.) all have very strong inhibitory action, also have good volatility.In addition cinnamon oil is to the smoked kill as excellent in sitophilus zea-mais, red flour beetle etc. have of grain storage pest and contact efficacy.
Detailed description of the invention
One, a kind of preparation of the grain insecticide containing cinnamon oil
Embodiment 1
Containing a grain insecticide for cinnamon oil, it is characterized in that, comprise the raw material of following percentage composition: cinnamon oil 10%; Galic essential oil 2%; Neem oil 5%; Turpentine oil 1%; Citronella oil 1%; Oil of badian 2%; ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS 1%; All the other are the ethanol of volumetric concentration 75%, complement to 100%.
The preparation method of the above-mentioned grain insecticide containing cinnamon oil, specifically comprises the steps: to take cinnamon oil according to the proportioning of above-mentioned percentage composition; Galic essential oil; Neem oil; Turpentine oil; Citronella oil; Oil of badian and ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS, make it fully mix, and then adds the ethanol that volumetric concentration is 75%, complement to 100%, stir, and essential oil and ethanol fully mixed and can obtain the grain insecticide containing cinnamon oil of the present invention.
Embodiment 2
Containing a grain insecticide for cinnamon oil, it is characterized in that, comprise the raw material of following percentage composition: cinnamon oil 11%; Galic essential oil 3%; Neem oil 6%; Turpentine oil 2%; Citronella oil 2%; Oil of badian 3%; ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS 2%; All the other are the ethanol of volumetric concentration 75%, complement to 100%.
The preparation method of the above-mentioned grain insecticide containing cinnamon oil, specifically comprises the steps: to take cinnamon oil according to the proportioning of above-mentioned percentage composition; Galic essential oil; Neem oil; Turpentine oil; Citronella oil; Oil of badian and ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS, make it fully mix, and then adds the ethanol that volumetric concentration is 75%, complement to 100%, stir, and essential oil and ethanol fully mixed and can obtain the grain insecticide containing cinnamon oil of the present invention.
Embodiment 3
Containing a grain insecticide for cinnamon oil, it is characterized in that, comprise the raw material of following percentage composition: cinnamon oil 12%; Galic essential oil 4%; Neem oil 7%; Turpentine oil 3%; Citronella oil 3%; Oil of badian 4%; ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS 3%; All the other are the ethanol of volumetric concentration 75%, complement to 100%.
The preparation method of the above-mentioned grain insecticide containing cinnamon oil, specifically comprises the steps: to take cinnamon oil according to the proportioning of above-mentioned percentage composition; Galic essential oil; Neem oil; Turpentine oil; Citronella oil; Oil of badian and ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS, make it fully mix, and then adds the ethanol that volumetric concentration is 75%, complement to 100%, stir, and essential oil and ethanol fully mixed and can obtain the grain insecticide containing cinnamon oil of the present invention.
Embodiment 4
Containing a grain insecticide for cinnamon oil, it is characterized in that, comprise the raw material of following percentage composition: cinnamon oil 14%; Galic essential oil 5%; Neem oil 8%; Turpentine oil 4%; Citronella oil 4%; Oil of badian 5%; ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS 4%; All the other are the ethanol of volumetric concentration 75%, complement to 100%.
The preparation method of the above-mentioned grain insecticide containing cinnamon oil, specifically comprises the steps: to take cinnamon oil according to the proportioning of above-mentioned percentage composition; Galic essential oil; Neem oil; Turpentine oil; Citronella oil; Oil of badian and ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS, make it fully mix, and then adds the ethanol that volumetric concentration is 75%, complement to 100%, stir, and essential oil and ethanol fully mixed and can obtain the grain insecticide containing cinnamon oil of the present invention.
Two, Application Example
Adopt at Guangxi Zhuang Autonomous Region Nanning City peasant family and just fumigated and the paddy that worm corpse sieves is tested, initial insect density is 0, and worm kind is rice weevil, gelechiid and booklice etc.Test group is: adopt embodiment 1 containing cinnamon oil grain insecticide and grain according to the dosage that the grain of 100 kilograms prepared by every 100 grams of pesticides carry out mix even after surround with paddy, often enclose and put 40 kilograms of grains.Control group is: in the silo placing grain, do not put into the grain insecticide containing cinnamon oil of the present invention.Monthly sampling Detection insect death condition.
Observe the situation of the grain of two silos do not put into the grain insecticide containing cinnamon oil of the present invention and put into the grain insecticide containing cinnamon oil of the present invention.The results are shown in experimental record table 1.
Claims (2)
1., containing a grain insecticide for cinnamon oil, it is characterized in that: the raw material comprising following percentage composition:
Cinnamon oil 10%-14%;
Galic essential oil 2%-5%;
Neem oil 5%-8%;
Turpentine oil 1%-4%;
Citronella oil 1%-4%;
Oil of badian 2%-5%;
ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS 1%-4%;
All the other are the ethanol of volumetric concentration 75%.
2. the grain insecticide containing cinnamon oil as described in claim l, is characterized in that: preparation method comprises the steps: to take cinnamon oil according to the proportioning of above-mentioned percentage composition; Galic essential oil; Neem oil; Turpentine oil; Citronella oil; Oil of badian and ACTIVITY OF THE RUE OIL AND ANALYSIS OF ITS COMPONENTS, make it fully mix, and then adds the ethanol that volumetric concentration is 75%, complement to 100%; Stir, essential oil and ethanol are fully mixed and can obtain the grain insecticide containing cinnamon oil of the present invention.
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Cited By (5)
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|---|---|---|---|---|
| RU2628796C1 (en) * | 2016-12-26 | 2017-08-22 | Мария Павловна Никифорова | Composition to control grain pests at growing and storage |
| CN108040648A (en) * | 2017-12-18 | 2018-05-18 | 绩溪县万禾林业开发有限公司 | A kind of hickory grafting method |
| CN109984191A (en) * | 2017-12-30 | 2019-07-09 | 中国科学院上海有机化学研究所 | A kind of grain fumigating technique |
| CN110384113A (en) * | 2019-07-11 | 2019-10-29 | 广州翼鲲生物科技有限公司 | A kind of prevention and treatment mosquitos and flies insecticide and its preparation method and application |
| CN113767936A (en) * | 2021-08-17 | 2021-12-10 | 仲恺农业工程学院 | Pesticide synergist and pesticide composition for preventing and treating white pelecypyriasis insects |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110384113A (en) * | 2019-07-11 | 2019-10-29 | 广州翼鲲生物科技有限公司 | A kind of prevention and treatment mosquitos and flies insecticide and its preparation method and application |
| CN113767936A (en) * | 2021-08-17 | 2021-12-10 | 仲恺农业工程学院 | Pesticide synergist and pesticide composition for preventing and treating white pelecypyriasis insects |
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Application publication date: 20150902 |