CN102007948B - Efficient and non-toxic broad-spectrum insectofungicide as well as preparation method and use method thereof - Google Patents
Efficient and non-toxic broad-spectrum insectofungicide as well as preparation method and use method thereof Download PDFInfo
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- CN102007948B CN102007948B CN2010105637376A CN201010563737A CN102007948B CN 102007948 B CN102007948 B CN 102007948B CN 2010105637376 A CN2010105637376 A CN 2010105637376A CN 201010563737 A CN201010563737 A CN 201010563737A CN 102007948 B CN102007948 B CN 102007948B
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- 231100000252 nontoxic Toxicity 0.000 title claims abstract description 31
- 230000003000 nontoxic effect Effects 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 229930013930 alkaloid Natural products 0.000 claims abstract description 25
- 235000015398 thunder god vine Nutrition 0.000 claims abstract description 25
- RNQBLQALVMHBKH-HHGOQMMWSA-N (2r,3s)-3-[(2r,3s)-5,7-dihydroxy-2-(4-hydroxyphenyl)-4-oxo-2,3-dihydrochromen-3-yl]-5,7-dihydroxy-2-(4-hydroxyphenyl)-2,3-dihydrochromen-4-one Chemical compound C1=CC(O)=CC=C1[C@H]1[C@H]([C@@H]2C(C3=C(O)C=C(O)C=C3O[C@H]2C=2C=CC(O)=CC=2)=O)C(=O)C2=C(O)C=C(O)C=C2O1 RNQBLQALVMHBKH-HHGOQMMWSA-N 0.000 claims abstract description 21
- QOPUSVUZHPIYER-QKOWHPQASA-N neochamaejasmin B Natural products COc1ccc(cc1)[C@H]2Oc3cc(O)cc(O)c3C(=O)[C@H]2[C@@H]4[C@H](Oc5cc(O)cc(O)c5C4=O)c6ccc(O)cc6 QOPUSVUZHPIYER-QKOWHPQASA-N 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims abstract description 18
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229960002715 nicotine Drugs 0.000 claims abstract description 18
- DFBIRQPKNDILPW-CIVMWXNOSA-N Triptolide Chemical compound O=C1OCC([C@@H]2C3)=C1CC[C@]2(C)[C@]12O[C@H]1[C@@H]1O[C@]1(C(C)C)[C@@H](O)[C@]21[C@H]3O1 DFBIRQPKNDILPW-CIVMWXNOSA-N 0.000 claims abstract description 16
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 16
- YKUJZZHGTWVWHA-UHFFFAOYSA-N triptolide Natural products COC12CC3OC3(C(C)C)C(O)C14OC4CC5C6=C(CCC25C)C(=O)OC6 YKUJZZHGTWVWHA-UHFFFAOYSA-N 0.000 claims abstract description 16
- YKPUWZUDDOIDPM-SOFGYWHQSA-N capsaicin Chemical compound COC1=CC(CNC(=O)CCCC\C=C\C(C)C)=CC=C1O YKPUWZUDDOIDPM-SOFGYWHQSA-N 0.000 claims abstract description 14
- 229960002504 capsaicin Drugs 0.000 claims abstract description 14
- 235000002566 Capsicum Nutrition 0.000 claims abstract description 10
- 229920001144 Hydroxy alpha sanshool Polymers 0.000 claims abstract description 7
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- PSKIOIDCXFHNJA-UHFFFAOYSA-N Sanshool Natural products CC=CC=CC=CCCC=CC=CC(=O)NC(C)C PSKIOIDCXFHNJA-UHFFFAOYSA-N 0.000 claims abstract description 7
- SBXYHCVXUCYYJT-UEOYEZOQSA-N alpha-Sanshool Chemical compound C\C=C\C=C\C=C/CC\C=C\C(=O)NCC(C)C SBXYHCVXUCYYJT-UEOYEZOQSA-N 0.000 claims abstract description 7
- 241001558929 Sclerotium <basidiomycota> Species 0.000 claims abstract description 6
- 239000003513 alkali Substances 0.000 claims description 55
- 239000000284 extract Substances 0.000 claims description 50
- 230000000749 insecticidal effect Effects 0.000 claims description 35
- 239000000575 pesticide Substances 0.000 claims description 34
- 230000000844 anti-bacterial effect Effects 0.000 claims description 29
- 239000003899 bactericide agent Substances 0.000 claims description 28
- 241000196324 Embryophyta Species 0.000 claims description 25
- FCPVYOBCFFNJFS-LQDWTQKMSA-M benzylpenicillin sodium Chemical compound [Na+].N([C@H]1[C@H]2SC([C@@H](N2C1=O)C([O-])=O)(C)C)C(=O)CC1=CC=CC=C1 FCPVYOBCFFNJFS-LQDWTQKMSA-M 0.000 claims description 17
- 239000000843 powder Substances 0.000 claims description 17
- 241001263603 Stellera Species 0.000 claims description 16
- 235000017663 capsaicin Nutrition 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- 150000003797 alkaloid derivatives Chemical class 0.000 claims description 13
- 239000003960 organic solvent Substances 0.000 claims description 13
- 239000011344 liquid material Substances 0.000 claims description 12
- 239000002002 slurry Substances 0.000 claims description 12
- 241000545405 Tripterygium Species 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 7
- 241000722363 Piper Species 0.000 claims description 6
- RNQBLQALVMHBKH-RPQLRNILSA-N (2S,3R)-3-[(2R,3R)-5,7-dihydroxy-2-(4-hydroxyphenyl)-4-oxo-2,3-dihydrochromen-3-yl]-5,7-dihydroxy-2-(4-hydroxyphenyl)-2,3-dihydrochromen-4-one Chemical compound Oc1ccc(cc1)[C@H]1Oc2cc(O)cc(O)c2C(=O)[C@@H]1[C@@H]1[C@@H](Oc2cc(O)cc(O)c2C1=O)c1ccc(O)cc1 RNQBLQALVMHBKH-RPQLRNILSA-N 0.000 claims description 5
- 238000010411 cooking Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 108091005804 Peptidases Proteins 0.000 claims description 3
- 239000004365 Protease Substances 0.000 claims description 3
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 230000000975 bioactive effect Effects 0.000 claims description 3
- 241000238631 Hexapoda Species 0.000 abstract description 13
- 241000607479 Yersinia pestis Species 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 8
- 244000061176 Nicotiana tabacum Species 0.000 abstract description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 5
- 240000008574 Capsicum frutescens Species 0.000 abstract description 3
- 239000001390 capsicum minimum Substances 0.000 abstract description 3
- 201000010099 disease Diseases 0.000 abstract description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 3
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 235000013311 vegetables Nutrition 0.000 abstract description 2
- 241000830536 Tripterygium wilfordii Species 0.000 abstract 4
- RSZDAYHEZSRVHS-UHFFFAOYSA-N suberosin Chemical compound O1C(=O)C=CC2=C1C=C(OC)C(CC=C(C)C)=C2 RSZDAYHEZSRVHS-UHFFFAOYSA-N 0.000 abstract 4
- JGSARLDLIJGVTE-MBNYWOFBSA-N Penicillin G Chemical compound N([C@H]1[C@H]2SC([C@@H](N2C1=O)C(O)=O)(C)C)C(=O)CC1=CC=CC=C1 JGSARLDLIJGVTE-MBNYWOFBSA-N 0.000 abstract 1
- 244000203593 Piper nigrum Species 0.000 abstract 1
- 241001263604 Stellera chamaejasme Species 0.000 abstract 1
- 229920002678 cellulose Polymers 0.000 abstract 1
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- 244000144972 livestock Species 0.000 abstract 1
- 229940056360 penicillin g Drugs 0.000 abstract 1
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- 239000002917 insecticide Substances 0.000 description 12
- 239000003905 agrochemical Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 5
- OIGWAXDAPKFNCQ-UHFFFAOYSA-N 4-isopropylbenzyl alcohol Chemical compound CC(C)C1=CC=C(CO)C=C1 OIGWAXDAPKFNCQ-UHFFFAOYSA-N 0.000 description 4
- 241001124076 Aphididae Species 0.000 description 4
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
- 239000004480 active ingredient Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
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- 240000008042 Zea mays Species 0.000 description 2
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 2
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- 230000003115 biocidal effect Effects 0.000 description 2
- 235000005822 corn Nutrition 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
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- 229940113087 geraniol Drugs 0.000 description 2
- 239000008141 laxative Substances 0.000 description 2
- 230000002475 laxative effect Effects 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 230000010534 mechanism of action Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XMGQYMWWDOXHJM-JTQLQIEISA-N (+)-α-limonene Chemical compound CC(=C)[C@@H]1CCC(C)=CC1 XMGQYMWWDOXHJM-JTQLQIEISA-N 0.000 description 1
- 206010002091 Anaesthesia Diseases 0.000 description 1
- 241001530056 Athelia rolfsii Species 0.000 description 1
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- 208000003643 Callosities Diseases 0.000 description 1
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- 206010020649 Hyperkeratosis Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241001477931 Mythimna unipuncta Species 0.000 description 1
- 241000244206 Nematoda Species 0.000 description 1
- 241000228150 Penicillium chrysogenum Species 0.000 description 1
- 241000222341 Polyporaceae Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
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- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
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- 230000002950 deficient Effects 0.000 description 1
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- 229930004069 diterpene Natural products 0.000 description 1
- 150000004141 diterpene derivatives Chemical class 0.000 description 1
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- 229940087305 limonene Drugs 0.000 description 1
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- 235000015097 nutrients Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- WSHJJCPTKWSMRR-RXMQYKEDSA-N penam Chemical compound S1CCN2C(=O)C[C@H]21 WSHJJCPTKWSMRR-RXMQYKEDSA-N 0.000 description 1
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- 239000000341 volatile oil Substances 0.000 description 1
Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides an efficient and non-toxic broad-spectrum insectofungicide as well as a preparation method and a use method thereof. The insectofungicide comprises the following components in parts by weight: 100 parts of water, 15-23 parts of alkaloids from tripterygium wilfordii, 1-5 parts of triptolide, 5-10 parts of omphalin, 3-8 parts of chamaejasmine, 8-20 parts of nicotine, 4-8 parts of capsaicine, 1-2 parts of suberosin and 1-3 parts of benzylpenicillin sodium, wherein the alkaloids from tripterygium wilfordii are extracted from roots, stems and leaves of tripterygium wilfordii; the triptolide is extracted from the root of tripterygium wilfordii; the omphalin is extracted from omphalialapidescens sclerotium; the chamaejasmine is extracted from stellera chamaejasme L.; the tobacco stalk cellulose is extracted from the branches and leaves of the tobaccos; the capsaicine is extracted from the capsicum fruits; and the suberosin contains sanshool and sanshoamide and is extracted from the pepper fruits. The insectofungicide is non-toxic and harmless to human and livestock, does not pollute the environment and the crops and has no toxic residues. The product has the effect of controlling the diseases and insect pests of the crops, fruit trees and vegetables.
Description
Technical field
The present invention relates to agricultural chemical insecticide and preparation method thereof and using method.
Background technology
China's agricultural chemicals output increases year by year in recent years, and whole pesticide industry developing steps are accelerated, and particularly global agricultural chemicals industry shifting to China, has also been impelled the rapid growth of Chinese agricultural chemicals industry gradually.China's pesticide industry in 2005 is total to enforcement sale and takes in 62,500,000,000 yuan, has increased by about 30% on a year-on-year basis; Total profit is 3,300,000,000 yuan, has increased by about 73% on a year-on-year basis.The every annual sales amount of China's pesticide market is between 240-260 hundred million about 3,000,000,000 dollars.The field of international trade also is that outlet is greater than import.China's agricultural chemicals output occupy 25% of the world, but also there is very large gap in China's pesticide technology level compared with developed countries, and with low content of technology, the output value accounts for less the world's 25% output value and only has 70% of world's sales volume.
The kind of existing agricultural chemical insecticide is a lot, and wherein natural insecticide is that the material that adopts the organism fuel to exist is made the pesticide that raw material is produced.This agricultural chemicals is fast decoupled in environmental and biological materials easily, can not cause environmental pollution.Therefore be the main direction of Development in Green Pesticides from now on by efficient, the low toxic pesticide of natural materials production.Show that according to the study a lot of natural fronds contain the material of energy desinsection.Plant insecticide take natural-plant-essence as active ingredient, in crop pests control, have environmentally friendly, toxicity generally lower, be difficult for making the advantages such as insect develops immunity to drugs.And also there is following long-term unsolved technical barrier in existing plant insecticide:
1, existing insecticide is that plurality of raw materials and organic solvent are added in the mixing kettle, heats stirred for several hour, adds the finish product again and obtains cream preparation, has cost height, contaminated environment, harmful defective.
2, existing insecticide active ingredient content is indefinite, affects result of use.
3, the active component of existing insecticide easily decomposes.
4, the performance of the drug effect of existing insecticide is slow, and the effect duration is short.
5, existing insecticide formulation is comparatively single, and active ingredient only possesses insecticidal effect to a small amount of insect, makes medicament not have general applicability.
Summary of the invention
The invention provides a kind of high efficiency nontoxic pesticide universal insecticidal bactericide and preparation method thereof and using method, solve prescription complexity, poor effect, technical problem that production cost is high.
The technical solution adopted for the present invention to solve the technical problems is:
This high efficiency nontoxic pesticide universal insecticidal bactericide, in weight portion, contain following composition in the proportioning:
100 parts in water;
15～23 parts of thunder godvine alkaloids, described triptolide are the extracts of tripterygium root, stem, leaf;
1～5 part of triptolide, described triptolide are the extracts of tripterygium root;
5～10 parts of Omphalins, described Omphalin are the extracts of Omphalia lapidescens sclerotium;
3～8 parts of chamaejasmines, described chamaejasmine are the extracts of Chinese Stellera Root plant;
8～20 parts in nicotine, described offal element are the extracts of tobacco branches and leaves;
4～8 parts of capsaicines, described capsaicine are the extracts of pepper fruit;
1～2 portion of xanthoxlin contains sanshool and sanshoamide in the described xanthoxlin, be the extract of Pericarpium Zanthoxyli fruit;
1～3 part of Benzylpenicillin sodium salt.
Described thunder godvine alkaloid by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form.
Described chamaejasmine is to be 15～17 liquid material or slurry or powder with the Baume degrees that the root of Chinese Stellera Root or stem or leaf or thrin or three's dual-purpose organic solvent or cooking process extract, and described chamaejasmine is new stellerin A, neochamaejasmine B or the chamaejasmine dry powder that extracts with Chinese Stellera Root.
Described xanthoxlin is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract.
Described offal element is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract.
The preparation method of this high efficiency nontoxic pesticide universal insecticidal bactericide, fetch water 100 parts, 1～3 part of 15～23 parts of thunder godvine alkaloid, 1～5 part of triptolide, 5～10 parts of Omphalins, 3～8 parts of chamaejasmines, 8～20 parts in nicotine, 4～8 parts of capsaicines, 1～2 part of xanthoxlin, Benzylpenicillin sodium salt are mixed with 100 parts in water.
The using method of this high efficiency nontoxic pesticide universal insecticidal bactericide, the high efficiency nontoxic pesticide universal insecticidal bactericide water for preparing is interpreted into 200～400 times of aqueous solution, be sprayed directly on plant surface, perhaps under the pH of plant value is 4～7 situation, be injected in plant stem with injection tool.
This high efficiency nontoxic pesticide universal insecticidal bactericide, in weight portion, contain following composition in the proportioning:
100 parts in water;
15～23 parts of thunder godvine alkaloids, described triptolide are the extracts of tripterygium root, stem, leaf;
1～5 part of triptolide, described triptolide are the extracts of tripterygium root;
3～8 parts of chamaejasmines, described chamaejasmine are the extracts of Chinese Stellera Root plant;
8～20 parts in nicotine, described offal element are the extracts of tobacco branches and leaves;
4～8 parts of capsaicines, described capsaicine are the extracts of pepper fruit;
1～2 portion of xanthoxlin contains sanshool and sanshoamide in the described xanthoxlin, be the extract of Pericarpium Zanthoxyli fruit;
1～3 part of Benzylpenicillin sodium salt.
Described thunder godvine alkaloid by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form.
This high efficiency nontoxic pesticide universal insecticidal bactericide, in weight portion, contain following composition in the proportioning:
100 parts in water;
5～10 parts of Omphalins, described Omphalin are the extracts of Omphalia lapidescens sclerotium;
3～8 parts of chamaejasmines, described chamaejasmine are the extracts of Chinese Stellera Root plant;
8～20 parts in nicotine, described offal element are the extracts of tobacco branches and leaves;
4～8 parts of capsaicines, described capsaicine are the extracts of pepper fruit;
1～2 portion of xanthoxlin contains sanshool and sanshoamide in the described xanthoxlin, be the extract of Pericarpium Zanthoxyli fruit;
1～3 part of Benzylpenicillin sodium salt.
Beneficial effect of the present invention is as follows:
The thunder godvine alkaloid has broad-spectrum, efficient, the characteristics such as the mode of action is various to insect, and the mechanism of action is unique, site of action is complicated, and field control effect is good.The alkaloidal chemical composition sesquiterpenoids of thunder godvine alkaloid is the major physiological active substance in the thunder godvine, the rattan alkaloid to the mechanism of action tripterygium total alkaloid of insect cause that the poisoning armyworm is slow in action, stops to take food, then anesthesia, rear recovery (or dead), recovery examination worm can again take food, anaesthetize, recover (or dead).Thunder godvine contains more than 20 plants alkaloid, of the present inventionly decides alkali, throws away alkali, Shanxi alkali, spring alkali and increase alkali and have better insecticidal activity than related alkaloids.
Triptolide is one and has multiple bioactive diterpenoid-lactone, derives from the root of Chinese herb triperygium wilfordii, has disinsection efficiency, is used with the thunder godvine alkaloid, can strengthen insecticidal effect.
Omphalin is the main component of the sclerotium stone-like omphalia of fungi plant medicine Polyporaceae plant Omphalia lapidescens, is a kind of protease, has and drives multiple worm, antiprotozoal effect.
Chamaejasmine contains diterpene, volatile oil material, has the insecticidal action of broad-spectrum.
The offal element contains the active ingredients such as nicotine, nicotine, has the Pesticidal and sterilizing effect, especially aphid is had obvious effect.
Xanthoxlin contains citrene (Limonene), cumic alcohol (Cumic alcohol), geraniol (Geraniol).In addition and contain the multiple compounds such as phytosterol and unsaturated organic acid, played insecticidal action.
The capsaicine capsaicine is that the main capsicum in the capsicum is first, contains capsaicine, can be used for desinsection, plays the effect of quick-acting Vermins-expelling vermins-proofs.
Benzylpenicillin sodium salt is a kind of of antibiotic, refer to from containing penam in the molecule of obtaining through refining the Penicillium notatum culture fluid, can destroying a class antibiotic of the cell wall of bacterium and bactericidal action the breeding period of bacterial cell, not only sterilized but also can desinsection, be used with other several plant source insect killing substances, can make that medicament has fast, the effect of synergy.
The present invention adopts above several plant extracts and Benzylpenicillin sodium salt with insecticidal action to be used, and the agricultural chemical insecticide of production is nontoxic to people, animal, free from environmental pollution and crops, and avirulence is residual.Product has the effect of control crops, fruit tree, vegetable disease insect pest, and the Various Diseases insect pests such as star caterpillar, aphid are had preventive and therapeutic action, can reach the target of medicine Zhiduo County worm.Control efficiency is good, efficacy of a drug longer duration, and use can reduce medication number of times, labor savings.Product be the plant insecticide bactericide also be plant nutrient agent, be again the stabilizing agent of volume increase, can promote the sound growth of crops and precocious, improve quality and increase output, to the best results of star caterpillar, aphid.
High efficiency nontoxic pesticide universal insecticidal bactericide can spray also and can inject, and with the situation hemostasis value preserving of injection tool in plant trees pH value 4-7, can directly act on inside plants, reaches faster, better insecticidal effect.
This high efficiency nontoxic pesticide universal insecticidal bactericide is done insecticidal test at Huludao Liaoning Province Lianshan District Si Erbao town agrotechnical station.Result of the test is as follows:
1, knit 3 mu of ground corns with 1:300 medicament proportioning doubly, the corn of result's laxative does not just have banded sclerotial blight and insect, do not go and buy Chinese medicine a lot of sick worms just arranged.Until August 12, the relevant personnel removed to see root leaf or green, the seed fringe is large without insect pest, and that does not beat is whole dried-up.
2, with 1:300 medicament doubly muskmelon root nematode and aphid are done experiment, observed once in two days, observed result is insect pest minimizings that come off, all disappearances in five days.Two booths contrasts is beaten one of high efficiency nontoxic pesticide insecticidal bactericide for one and is not sprayed this medicament.The canopy of laxative is 2893 yuan of more incomes than the same period, and that does not go and buy Chinese medicine is all dried-up in mid-July.
3, this medicament in Anhui Province the one minute station-service 1:300 in state-run Wan He farm to cook the wheat result of the test as follows:
12 mu are sprayed 6 times with high efficiency nontoxic pesticide universal insecticidal bactericide, and per mu yield 4180 jin, a traditional unit of weight (net weight) is without insect pest; Do not use 3150 jin, a traditional unit of weight of the per mu yields of this medicament, two are increased production 670 jin, a traditional unit of weight on year-on-year basis, 55.83 jin, a traditional unit of weight of mu increments.
1:300 doubly spray 4 times 10 mu without insect pest, 4060 jin, a traditional unit of weight, without beat this medicament 4 times 10 mu 3520 jin, a traditional unit of weight.Two are increased production 550 jin, a traditional unit of weight on year-on-year basis, 55 jin, a traditional unit of weight of mu volume increase.
Embodiment
Embodiment one, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water;
15 parts of thunder godvine alkaloids, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
1 part of triptolide;
10 parts of Omphalins;
8 parts of chamaejasmines;
13 parts in nicotine;
4 parts of capsaicines;
2 parts of xanthoxlins;
2 parts of Benzylpenicillin sodium salts.
Embodiment two, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water;
20 parts of thunder godvine alkaloids, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
3 parts of triptolides;
7 parts of Omphalins;
5 parts of chamaejasmines;
16 parts in nicotine;
6 parts of capsaicines;
1 part of xanthoxlin;
1 part of Benzylpenicillin sodium salt.
Embodiment three, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water;
23 parts of thunder godvine alkaloids, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
5 parts of triptolides;
5 parts of Omphalins;
3 parts of chamaejasmines;
8 parts in nicotine;
8 parts of capsaicines;
1 part of xanthoxlin;
3 parts of Benzylpenicillin sodium salts.
Embodiment four, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water,
15 parts of thunder godvine alkaloids, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
2 parts of triptolides;
3 parts of chamaejasmines;
20 parts in nicotine;
4 parts of capsaicines;
1 part of xanthoxlin;
1 part of Benzylpenicillin sodium salt.
Embodiment five, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water;
23 parts of thunder godvine alkaloids, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
5 parts of triptolides;
8 parts of chamaejasmines;
8 parts in nicotine;
8 parts of capsaicines;
1 part of xanthoxlin;
1 part of Benzylpenicillin sodium salt.
Embodiment six, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water;
10 parts of Omphalins;
8 parts of chamaejasmines;
20 parts in nicotine;
8 parts of capsaicines;
2 parts of xanthoxlins;
3 parts of Benzylpenicillin sodium salts.
Embodiment seven, and this high efficiency nontoxic pesticide universal insecticidal bactericide in weight portion, contains following composition in the proportioning:
100 parts in water;
5 parts of Omphalins;
5 parts of chamaejasmines;
15 parts in nicotine;
4 parts of capsaicines;
2 parts of xanthoxlins;
2 parts of Benzylpenicillin sodium salts.
Thunder godvine alkaloid in above-described embodiment by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form.
Chamaejasmine in above-described embodiment is to be 15～17 liquid material or slurry or powder with the Baume degrees that the root of Chinese Stellera Root or stem or leaf or thrin or three's dual-purpose organic solvent or cooking process extract, and described chamaejasmine is new stellerin A, neochamaejasmine B or the chamaejasmine dry powder that extracts with Chinese Stellera Root.
Xanthoxlin in above-described embodiment is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract.
Offal element in above-described embodiment is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract.
The using method of the high efficiency nontoxic pesticide universal insecticidal bactericide in above-described embodiment, the high efficiency nontoxic pesticide universal insecticidal bactericide water for preparing is interpreted into 200～400 times of aqueous solution, be sprayed directly on plant surface, perhaps under the pH of plant value is 4～7 situation, be injected in plant stem with injection tool.
Claims (5)
1. high efficiency nontoxic pesticide universal insecticidal bactericide is characterized in that: in weight portion, contain following composition in the proportioning:
100 parts in water;
15～23 parts of thunder godvine alkaloids; Described thunder godvine alkaloid is the extract of tripterygium root, stem, leaf, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
1～5 part of triptolide; Described triptolide is the extract of tripterygium root, is one and has multiple bioactive diterpenoid-lactone;
5～10 parts of Omphalins; Described Omphalin is the extract of Omphalia lapidescens sclerotium, is a kind of protease;
3～8 parts of chamaejasmines; Described chamaejasmine is the extract of Chinese Stellera Root plant, be that Baume degrees that dual-purpose organic solvent or cooking process with the root of Chinese Stellera Root or stem or leaf or thrin or three extract is 15～17 liquid material or slurry or powder, described chamaejasmine is new stellerin A, neochamaejasmine B or the chamaejasmine dry powder that extracts with Chinese Stellera Root;
8～20 parts in nicotine;
4～8 parts of capsaicines, described capsaicine is the extract of pepper fruit, contains capsaicine;
1～2 portion of xanthoxlin contains sanshool and sanshoamide in the described xanthoxlin, be the extract of Pericarpium Zanthoxyli fruit, is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract;
1～3 part of Benzylpenicillin sodium salt.
2. the preparation method of a high efficiency nontoxic pesticide universal insecticidal bactericide as claimed in claim 1, it is characterized in that: fetch water 100 parts, 1～3 part of 15～23 parts of thunder godvine alkaloid, 1～5 part of triptolide, 5～10 parts of Omphalins, 3～8 parts of chamaejasmines, 8～20 parts in nicotine, 4～8 parts of capsaicines, 1～2 part of xanthoxlin, Benzylpenicillin sodium salt are mixed with 100 parts in water.
3. the using method of a high efficiency nontoxic pesticide universal insecticidal bactericide as claimed in claim 1, it is characterized in that: the high efficiency nontoxic pesticide universal insecticidal bactericide water for preparing is interpreted into 200～400 times of aqueous solution, be sprayed directly on plant surface, perhaps under the pH of plant value is 4～7 situation, be injected in plant stem with injection tool.
4. high efficiency nontoxic pesticide universal insecticidal bactericide is characterized in that: in weight portion, contain following composition in the proportioning:
100 parts in water;
15～23 parts of thunder godvine alkaloids, described thunder godvine alkaloid are the extracts of tripterygium root, stem, leaf, by decide alkali, throw away alkali, Shanxi alkali, spring alkali and increase five kinds in alkali and form;
1～5 part of triptolide, described triptolide is the extract of tripterygium root, is one and has multiple bioactive diterpenoid-lactone;
3～8 parts of chamaejasmines, described chamaejasmine is the extract of Chinese Stellera Root plant, be that Baume degrees that dual-purpose organic solvent or cooking process with the root of Chinese Stellera Root or stem or leaf or thrin or three extract is 15～17 liquid material or slurry or powder, described chamaejasmine is new stellerin A, neochamaejasmine B or the chamaejasmine dry powder that extracts with Chinese Stellera Root;
8～20 parts in nicotine;
4～8 parts of capsaicines, described capsaicine is the extract of pepper fruit, contains capsaicine;
1～2 portion of xanthoxlin contains sanshool and sanshoamide in the described xanthoxlin, be the extract of Pericarpium Zanthoxyli fruit, is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract;
1～3 part of Benzylpenicillin sodium salt.
5. high efficiency nontoxic pesticide universal insecticidal bactericide is characterized in that: in weight portion, contain following composition in the proportioning:
100 parts in water;
5～10 parts of Omphalins, described Omphalin is the extract of Omphalia lapidescens sclerotium, is a kind of protease;
3～8 parts of chamaejasmines, described chamaejasmine is the extract of Chinese Stellera Root plant, be that Baume degrees that dual-purpose organic solvent or cooking process with the root of Chinese Stellera Root or stem or leaf or thrin or three extract is 15～17 liquid material or slurry or powder, described chamaejasmine is new stellerin A, neochamaejasmine B or the chamaejasmine dry powder that extracts with Chinese Stellera Root;
8～20 parts in nicotine;
4～8 parts of capsaicines, described capsaicine is the extract of pepper fruit, contains capsaicine;
1～2 portion of xanthoxlin contains sanshool and sanshoamide in the described xanthoxlin, be the extract of Pericarpium Zanthoxyli fruit, is to be 15～17 liquid material or slurry or powder with the Baume degrees that organic solvent or water-boiling method extract;
1～3 part of Benzylpenicillin sodium salt.
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| CN2010105637376A CN102007948B (en) | 2010-11-29 | 2010-11-29 | Efficient and non-toxic broad-spectrum insectofungicide as well as preparation method and use method thereof |
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| CN2010105637376A CN102007948B (en) | 2010-11-29 | 2010-11-29 | Efficient and non-toxic broad-spectrum insectofungicide as well as preparation method and use method thereof |
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| CN102696702A (en) * | 2012-05-11 | 2012-10-03 | 丁文贵 | Non-poisonous pesticide and preparation method thereof |
| CN103168803B (en) * | 2013-03-28 | 2014-04-02 | 陈士进 | Plant source bacteriostasis and detoxification deodorant and preparation method and application of plant source bacteriostasis and detoxification deodorant |
| CN105028516A (en) * | 2015-08-29 | 2015-11-11 | 固镇县传红家庭农场 | Medicament capable of preventing and treating Chinese cabbage downy mildew |
| CN105272605A (en) * | 2015-10-26 | 2016-01-27 | 广西农垦国有立新农场 | Fertilizer and preparation method thereof |
| CN105284963B (en) * | 2015-10-30 | 2018-06-05 | 大新县生产力促进中心 | Cock skin fruit tree special plant fungicide and its production method |
| CN106165703A (en) * | 2016-07-13 | 2016-11-30 | 重庆全合农业发展有限公司 | A kind of compositions killing blood orange fruit piercing moth |
| CN106883060A (en) * | 2016-12-28 | 2017-06-23 | 赵永明 | A kind of pesticide-germicide growth promoting composition for promoting crop growth |
| CN110150330A (en) * | 2017-12-29 | 2019-08-23 | 云南宏绿辣素有限公司 | A kind of compound botanical source bactericide and preparation method thereof |
| CN110357726A (en) * | 2019-08-14 | 2019-10-22 | 陈爱红 | High effect nontoxic Pesticidal and sterilizing nutrient solution aqua and preparation method thereof and application method |
| CN112979614B (en) * | 2021-02-09 | 2022-09-13 | 西北大学 | Nicotine-phthalic acid composite crystal, preparation method and application thereof |
| CN114766276A (en) * | 2022-05-25 | 2022-07-22 | 李忠文 | Citrus planting method |
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