CN101861886B - Preparation method of green herbal insecticide - Google Patents
Preparation method of green herbal insecticide Download PDFInfo
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- CN101861886B CN101861886B CN2010102114649A CN201010211464A CN101861886B CN 101861886 B CN101861886 B CN 101861886B CN 2010102114649 A CN2010102114649 A CN 2010102114649A CN 201010211464 A CN201010211464 A CN 201010211464A CN 101861886 B CN101861886 B CN 101861886B
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- insecticide
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- green herbal
- root
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- 239000002917 insecticide Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 19
- 238000003958 fumigation Methods 0.000 claims abstract description 16
- 241000244987 Daiswa polyphylla Species 0.000 claims abstract description 14
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims abstract description 9
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960000846 camphor Drugs 0.000 claims abstract description 9
- 229930008380 camphor Natural products 0.000 claims abstract description 9
- 241000238631 Hexapoda Species 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 16
- 235000015398 thunder god vine Nutrition 0.000 claims description 12
- 235000006226 Areca catechu Nutrition 0.000 claims description 8
- 244000080767 Areca catechu Species 0.000 claims description 8
- 241000601164 Clematis orientalis Species 0.000 claims description 8
- 241000258920 Chilopoda Species 0.000 claims description 6
- 241000338702 Cupido minimus Species 0.000 claims description 5
- 241001474977 Palla Species 0.000 claims description 4
- 241000271897 Viperidae Species 0.000 claims description 4
- 238000000034 method Methods 0.000 claims 2
- 241000196324 Embryophyta Species 0.000 abstract description 7
- 241000607479 Yersinia pestis Species 0.000 abstract description 4
- 230000002147 killing effect Effects 0.000 abstract description 4
- 235000013399 edible fruits Nutrition 0.000 abstract description 3
- 125000003118 aryl group Chemical group 0.000 abstract description 2
- 230000000749 insecticidal effect Effects 0.000 abstract description 2
- 210000001835 viscera Anatomy 0.000 abstract description 2
- 241000545405 Tripterygium Species 0.000 abstract 2
- 229930182470 glycoside Natural products 0.000 abstract 2
- 150000002338 glycosides Chemical class 0.000 abstract 2
- 241000202755 Areca Species 0.000 abstract 1
- 241000218158 Clematis Species 0.000 abstract 1
- 244000044425 Quisqualis indica Species 0.000 abstract 1
- 241001671204 Stemona Species 0.000 abstract 1
- 231100000225 lethality Toxicity 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 229940126672 traditional medicines Drugs 0.000 abstract 1
- 235000013311 vegetables Nutrition 0.000 description 8
- 239000000575 pesticide Substances 0.000 description 5
- 231100000614 poison Toxicity 0.000 description 4
- 239000003814 drug Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 230000007096 poisonous effect Effects 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 241000270295 Serpentes Species 0.000 description 2
- 210000003128 head Anatomy 0.000 description 2
- 210000000214 mouth Anatomy 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 241001124076 Aphididae Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000270322 Lepidosauria Species 0.000 description 1
- 241001454293 Tetranychus urticae Species 0.000 description 1
- 241001238452 Tortrix Species 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 210000000805 cytoplasm Anatomy 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- OEBRKCOSUFCWJD-UHFFFAOYSA-N dichlorvos Chemical compound COP(=O)(OC)OC=C(Cl)Cl OEBRKCOSUFCWJD-UHFFFAOYSA-N 0.000 description 1
- 229950001327 dichlorvos Drugs 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000016507 interphase Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 231100000518 lethal Toxicity 0.000 description 1
- 230000001665 lethal effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 230000010412 perfusion Effects 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000001846 repelling effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- GOLXNESZZPUPJE-UHFFFAOYSA-N spiromesifen Chemical compound CC1=CC(C)=CC(C)=C1C(C(O1)=O)=C(OC(=O)CC(C)(C)C)C11CCCC1 GOLXNESZZPUPJE-UHFFFAOYSA-N 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- JLYXXMFPNIAWKQ-UHFFFAOYSA-N γ Benzene hexachloride Chemical compound ClC1C(Cl)C(Cl)C(Cl)C(Cl)C1Cl JLYXXMFPNIAWKQ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a preparation method of a green herbal insecticide, comprising the following steps: (1) cutting three raw materials of paris polyphylla root tubers, camphor and areca inflorescence into slices according to the weight ratio of 1:0.8-1.2:6.0-7.0, and then soaking the slices into industrial alcohol to obtain a soak solution; (2) pulverizing four raw materials of tripterygium glycoside, clematis root, large stemona root collars and fruit of Rangoon creeper, and then fumigating the pulverized raw materials based on the weight ratio of 1:0.8-1.2:0.8-1.2:1.5-2.5 at the temperature of 150-250 DEG C by hot steam to obtain a fumigation solution, wherein the weight ratio of the tripterygium glycoside to the paris polyphylla root tubers in step (1) is 1.5-2.5:1; and (3) mixing the soak solution with the fumigation solution to obtain the green herbal insecticide. The components of the green herbal insecticide are extracted from natural Chinese traditional medicines or plants, thus the green herbal insecticide has no harm to human body and environment, has aromatic odor and insecticidal lethality, can repel pests and go deep into the internal organs of the pests to kill the pests, and has great killing action on various insects.
Description
Technical field
The present invention relates to a kind of synthetic nuisanceless green method for producing insecticide of multiple herbaceous plant that has.
Technical background
Show generally the residual of chemical pesticide arranged according to the current result the who in the world investigation of crops and by product is checked, the hexachlorcyclohexane of using in the past and 1059,1605, dichlorvos etc. are all checked out the residue of antimony agent and organophosphorous pesticide.Therefore residual toxicity commonly used was left over long difficult decomposition of phase in the past, and the easy like this poisoning that causes sprinkling personnel and eater, countries in the world have ten hundreds of users and eater to poison and death every year, simultaneously, when producing and use, environment and water resource are caused serious pollution, and cause generation even the canceration of eater's various diseases.Countries in the world are dropped into the scientific research that huge fund is carried out non-poisonous pesticides one after another, and make and forbid that the vegetables of spraying insecticide come into the market, this country has also set up nuisanceless green Vegetable Base and special green vegetables selling market in each big city specially, and urge relevant department to carry out special monitoring, prevent that the vegetables of spraying insecticide from coming into the market to sell.Along with people's living standard improves constantly, when people pay close attention to health problem, also at vegetables and the fruit of pursuing the protoplasm original flavor, pursue the protection of environment.Therefore, a kind of energy is long-term, and is efficient, and practical green non-pollution draft insecticide synthetic has realistic meaning.
In order to address the above problem, patent of invention that Wang Wanjun discloses a kind of " Pullution-free insecticide prepared from Chinese herbacteous plant ", application number is 00121313.X.This invention is mainly formulated in proportion by multiple middle herbaceous plant, its preparation method is through screening, pulverize, mix, HTHP boils by swallow, concentrated, filtering processing is prepared from, manufacture craft is simple, the raw material abundance is easy to get, various insects there are good inhibition and killing action, particularly to the green vegetables worm, cotton mountain range worm, aphid, two spotted spider mite all can reach and suppress and killing action, total effective rate reaches 95%, this invention is synthetic by natural plants, do not contain any poisonous chemical analysis, after the sprinkling, plant, fruit tree, vegetables do not have residual toxin, to the people, the Environmental Water resource is harmless, the chemical pesticide of alternative existing use is a kind of novel nuisanceless, the environment-friendly insecticide.
Summary of the invention
The object of the present invention is to provide a kind of green, non-harmful draft method for producing insecticide.
A kind of preparation method of green herbal insecticide comprises the following steps:
(1) with Paris polyphylla piece root, camphor, three kinds of raw material sections of flower betel nut, 1: 0.8~1.2: 6.0~7.0 places industrial alcohol to soak by weight, obtain soak;
(2) thunder godvine herb, root of Chinese clematis herb, fertile white section rhizome, four kinds of raw materials of history gentleman are pulverized, carried out 150~250 ℃ of vapours by weight 1: 0.8~1.2: 0.8~1.2: 1.5~2.5 and fumigate, obtain fumigation liquid; Wherein the weight ratio of Paris polyphylla piece root is 1.5~2.5: 1 in thunder godvine herb and the step (1);
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide.
Preferably, in the described preparation method of green herbal insecticide:
(1) with Paris polyphylla piece root, camphor, three kinds of raw material sections of flower betel nut, places industrial alcohol to soak by weight 1: 1: 6.4, obtain soak;
(2) thunder godvine herb, root of Chinese clematis herb, fertile white section rhizome, four kinds of raw materials of history gentleman are pulverized, by weight 1: 1: 1: 2 carry out 150~250 ℃ of vapours fumigated, and obtains fumigation liquid; Wherein the weight ratio of Paris polyphylla piece root is 2: 1 in thunder godvine herb and the step (1);
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide.
Green herbal insecticide of the present invention can be regulated insecticide concentration by insect size, quantity, pesticide resistance etc. in actual applications, and this all belongs to those skilled in the art's common practise.A 100Kg insecticide finished product raw material consumption of recommending is: Paris polyphylla piece root 250g, camphor 250g, flower betel nut 1600g, thunder godvine herb 500g, root of Chinese clematis herb 500g, fertile white the rhizome 500g of section, history gentleman 1000g.
Every composition among the present invention all refines from natural traditional Chinese medicine or plant, to human body and environmentally friendly.This green herbal insecticide has dense aromatic odor and desinsection lethal, each composition interphase interaction, complement each other, not only can kill and pest repelling with its smell, can also go deep into the insect internal organ it is caused death, all kinds of reptiles, insect, moth, tortrix moth, borer are had great killing action.
Embodiment:
The invention will be further described below in conjunction with embodiment, but protection scope of the present invention is not limited to this.
1 one kinds of preparation method of green herbal insecticide of embodiment comprise the steps:
(1) with 250g Paris polyphylla piece root, 250g camphor, three kinds of raw material sections of 1600g flower betel nut, places the 5000ml industrial alcohol to soak, obtain soak;
(2) 500g thunder godvine herb, 500g root of Chinese clematis herb, the fertile white section of 500g rhizome, four kinds of raw materials of 1000g history gentleman are pulverized, carried out 150~250 ℃ of vapours and fumigate, obtain fumigation liquid;
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide.
2 one kinds of preparation method of green herbal insecticide of embodiment comprise the steps:
(1) with 250g Paris polyphylla piece root, 260g camphor, three kinds of raw material sections of 1700g flower betel nut, places the 5000ml industrial alcohol to soak, obtain soak;
(2) 500g thunder godvine herb, 510g root of Chinese clematis herb, the fertile white section of 490g rhizome, four kinds of raw materials of 1200g history gentleman are pulverized, carried out 150~250 ℃ of vapours and fumigate, obtain fumigation liquid;
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide.
3 one kinds of preparation method of green herbal insecticide of embodiment comprise the steps:
(1) with 250g Paris polyphylla piece root, 240g camphor, three kinds of raw material sections of 150g flower betel nut, places the 5000ml industrial alcohol to soak, obtain soak;
(2) 500g thunder godvine herb, 490g root of Chinese clematis herb, the fertile white section of 490g rhizome, four kinds of raw materials of 900g history gentleman are pulverized, carried out 150~250 ℃ of vapours and fumigate, obtain fumigation liquid;
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide.
The experiment of experimental example insecticidal effect
One, the green herbal insecticide of insecticide: embodiment 1 adds water and is mixed with the 100Kg finished product.
Two, experimental subjects: four double pallas pit vipers, centipede, ant, little blue or green worm.
Three, step:
1, with aiming at the pallas pit viper mouth, the oral cavity of spirt snake behind 5 milliliters the syringe perfusion insecticide;
2, directly adopt sprayer to centipede head, ant, little blue or green worm spraying insecticide.
Four, effect:
1, poisonous snake is at once dizzy, rolls about after 10 minutes, is unable to stir any more death in 30-35 minute in 20 minutes;
2, with liquid medicine jet to the centipede head, centipede cuddles up in a heap at once, begins to stand up after 5 minutes and rolls about, straight death in 10 minutes;
3, death in 15 minutes behind the ant spray medicine;
4, the little blue or green worm on the vegetables, death in 2 minutes behind the spray liquid.
Claims (2)
1. a preparation method of green herbal insecticide is characterized in that comprising the following steps:
(1) with Paris polyphylla piece root, camphor, three kinds of raw material sections of flower betel nut, 1: 0.8~1.2: 6.0~7.0 places industrial alcohol to soak by weight, obtain soak;
(2) thunder godvine herb, root of Chinese clematis herb, fertile white section rhizome, four kinds of raw materials of history gentleman are pulverized, carried out 150~250 ℃ of vapours by weight 1: 0.8~1.2: 0.8~1.2: 1.5~2.5 and fumigate, obtain fumigation liquid; Wherein the weight ratio of Paris polyphylla piece root is 1.5~2.5: 1 in thunder godvine herb and the step (1);
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide;
The insect type that the green herbal insecticide that the method makes is suitable for eliminating is pallas pit viper, centipede, ant, little blue or green worm.
2. preparation method of green herbal insecticide according to claim 1 is characterized in that (1) with Paris polyphylla piece root, camphor, three kinds of raw material sections of flower betel nut, placed industrial alcohol to soak by weight 1: 1: 6.4, obtained soak;
(2) thunder godvine herb, root of Chinese clematis herb, fertile white section rhizome, four kinds of raw materials of history gentleman are pulverized, by weight 1: 1: 1: 2 carry out 150~250 ℃ of vapours fumigated, and obtains fumigation liquid; Wherein the weight ratio of Paris polyphylla piece root is 2: 1 in thunder godvine herb and the step (1);
(3) above-mentioned soak is mixed with fumigation liquid, namely get the green herbal insecticide
The insect type that the green herbal insecticide that the method makes is suitable for eliminating is pallas pit viper, centipede, ant, little blue or green worm.
Priority Applications (1)
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CN2010102114649A CN101861886B (en) | 2010-06-25 | 2010-06-25 | Preparation method of green herbal insecticide |
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CN2010102114649A CN101861886B (en) | 2010-06-25 | 2010-06-25 | Preparation method of green herbal insecticide |
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CN101861886A CN101861886A (en) | 2010-10-20 |
CN101861886B true CN101861886B (en) | 2013-01-23 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105532765A (en) * | 2016-02-17 | 2016-05-04 | 广西大学 | Green botanical insecticide and preparation method thereof |
CN106417400A (en) * | 2016-09-23 | 2017-02-22 | 黄飞必 | Forest insecticide and preparation method thereof |
CN111802413A (en) * | 2020-07-14 | 2020-10-23 | 黑龙江省农业科学院耕作栽培研究所 | Plant-derived pesticide and preparation method thereof |
-
2010
- 2010-06-25 CN CN2010102114649A patent/CN101861886B/en not_active Expired - Fee Related
Non-Patent Citations (8)
Title |
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刘小平.菜用苜蓿无公害生产技术.《西北园艺》.2004,(第03期), |
川北地区川明参高产栽培技术;戚容等;《四川农业科技》;20061028(第10期);27-28页 * |
戚容等.川北地区川明参高产栽培技术.《四川农业科技》.2006,(第10期), |
推广种植除虫菊 发展无公害农业;黄巧连;《北京农业》;20070305(第07期);17-18页 * |
无公害农药――除虫菊.《农村天地》.2004,(第07期), |
无公害农药――除虫菊;《农村天地》;20040705(第07期);19页 * |
菜用苜蓿无公害生产技术;刘小平;《西北园艺》;20040310(第03期);30页 * |
黄巧连.推广种植除虫菊 发展无公害农业.《北京农业》.2007,(第07期), |
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