CN104872215B - Microencapsulation plants essential oil culicifuge containing cinnamon oil - Google Patents

Microencapsulation plants essential oil culicifuge containing cinnamon oil Download PDF

Info

Publication number
CN104872215B
CN104872215B CN201510277804.0A CN201510277804A CN104872215B CN 104872215 B CN104872215 B CN 104872215B CN 201510277804 A CN201510277804 A CN 201510277804A CN 104872215 B CN104872215 B CN 104872215B
Authority
CN
China
Prior art keywords
parts
oil
essential oil
microencapsulation
culicifuge
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510277804.0A
Other languages
Chinese (zh)
Other versions
CN104872215A (en
Inventor
贺均林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201510277804.0A priority Critical patent/CN104872215B/en
Publication of CN104872215A publication Critical patent/CN104872215A/en
Application granted granted Critical
Publication of CN104872215B publication Critical patent/CN104872215B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fats And Perfumes (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention belongs to daily chemical product field, and in particular to a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil;It is prepared from the following raw materials in parts by weight:The core of microcapsules:37 parts of cinnamon oil;15 20 parts of wormwood essential oil;10 15 parts of shiu oil;Silver grey 47 parts of chrysanthemum essential oil;6 10 parts of lemon grass (Cymbopogon citratus) essential oil;7 12 parts of Rosemary Oil;25 parts of neem oil;Additives:Sorbester p17,46 parts;The wall material of microcapsules:13 18 parts of Arabic gum, 12 17 parts of gelatin.Microencapsulation plants essential oil culicifuge of the invention containing cinnamon oil is prepared from cinnamon oil, wormwood essential oil, fragrant camphor tree essential oil etc. for raw material, without conventional chemical insecticide, safe and environment-friendly, pollution-free and used raw material has good dispersion effect to mosquito, skin is not stimulated, dispelling fatigue, the quiet effect calmed the nerves can be also played to human body.

Description

Microencapsulation plants essential oil culicifuge containing cinnamon oil
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of microencapsulation plants essential oil culicifuge.
Background technology
Summer arrives, and the life given people as the mosquito of one of " four pests " brings very big harm.Drone sound is hesitated Wander in one's ear, disturb one's sleep, and then have influence on new darg, studying and living.If unfortunate by mosquito bite, it will ache Itch hard to bear, be on tenterhooks.More serious the problem of is that mosquito can propagate malaria, filariasis, Japanese Type-B encephalitis and dengue fever etc. Disease.
With the development of society, the continuous improvement of human living standard, people also exist to the consciousness of health and self-protection It is continuously increased, various mosquito repellent products arise at the historic moment in succession.At present, the product of in the market mosquito repellent class is a lot, is concentrated mainly on disc type Mosquito-repellent incense, the piece that kindles mosquito repellent incense, mosquito-killing spraying agent, floral water, mosquito-dispelling cream, dimethyl carbate, heating mosquito-repellent incense liquid etc..People are the most commonly used in summer Mosquito repellent articles for use be mosquito-repellent incense, do not know that this can damage to human body but.In fact, the effective ingredient of most of mosquito-repellent incenses is pyrethrin Insecticide, and organic filler, fusion agent, dyestuff and other additives etc., therefore containing many to people in the cigarette of mosquito incense burning The harmful material of body, it is possible to induce the diseases such as asthma.According to measuring and calculating, particulate and burn l00 roots or so perfume (or spice) that a roll of mosquito-repellent incense of point is released The amount of cigarette is roughly the same, the ultrafine dust discharged, can enter and be deposited in lung, may trigger asthma in a short time, for a long time Cancer may then be triggered.Next to that the carcinogen that mosquito-repellent incense base material imperfect combustion is produced, and some can stimulate and exhale The compound in road is inhaled, these materials can make the nervous system of people be poisoned.Mosquito-repellent incense, the piece that kindles mosquito repellent incense, mosquito-killing spraying agent, floral water, drive These mosquito repellent product majorities such as mosquito frost, dimethyl carbate, heating mosquito-repellent incense liquid are to reach repelling effect by agricultural chemicals or chemical analysis, only It is to play mosquito-repelling function with the harmless composition of Nantural non-toxic to have minority.Therefore, a good, nontoxic, harmless, safety-type mosquito repellent Product is particularly important in summer.It can not only play good effectiveness, and more importantly the health hazards to human body is seldom, very To being free from side effects, there is no any pollution simultaneously for environment.
Plants essential oil refers to a kind of volatile flavour for refining and extracting from the flower of plant, leaf, stem, root or fruit Matter, domestic and international researcher has found that effect of catching up with, and tool are driven, refuse to keep away and smoked to various plants and its essential oil to mosquito with certain Have and safety educated to people, be not likely to produce the resistance to the action of a drug, it is degradable under natural environment the characteristics of.Much it is made up for this of plants essential oil Scent mosquito repellent product the sixth of the twelve Earthly Branches is widely used in household bedroom, the occasion such as office, hospital, outdoor.But existing banana mosquito repellent Product, the problems such as generally existing component is more, cost high and mosquito repellent efficiency is low, fragrance is dull flat weary.Along with some with higher The most fragrance of folk prescription essential oil of mosquito repellent efficiency is strong, stimulate, and makes us using discomfort, existing essential oil mosquito repellent class product formula does not conform to Reason, repelling effect, which is difficult to, to be continued, and essential oil product is as liquid form product, and its extremely strong volatility is also to using bringing Inconvenience, therefore also it is difficult to the requirement that meets consumers in general.
The content of the invention
It is an object of the invention to there is problem and shortage there is provided one kind for above-mentioned with cinnamon oil, wormwood essential oil, fragrant camphor tree Essential oil etc. is that raw material is prepared from, repelling effect significantly, safety non-toxic, without it is strong, fragrance is stimulated, with comfortable, pleased The microencapsulation plants essential oil culicifuge of happy unique perfume.
In order to realize the purpose of the present invention, the present invention is adopted the following technical scheme that:
A kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, is prepared from the following raw materials in parts by weight:
The core of microcapsules:3-7 parts of cinnamon oil;15-20 parts of wormwood essential oil;10-15 parts of shiu oil;Silver grey chrysanthemum essential oil 4-7 Part;6-10 parts of lemon grass (Cymbopogon citratus) essential oil;7-12 parts of Rosemary Oil;2-5 parts of neem oil;
Additives:Sorbester p17,4-6 parts;
The wall material of microcapsules:13-18 parts of Arabic gum;12-17 parts of gelatin.
Above-mentioned a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, it is characterised in that described contains Chinese cassia tree The preparation method step of the microencapsulation plants essential oil culicifuge of oil is as follows:
(1)The sorbester p17 of parts by weight is taken, the water that temperature is 35-45 DEG C is added, it is the molten of 4%-6% to be configured to mass fraction Liquid A;
(2)The Arabic gum of parts by weight is taken, according to volume ratio Arabic gum:Water is 1:2 ratio adds water, and stirring is equal It is even, the core of the microcapsules of parts by weight is then added, and add step(1)In obtained solution A, stir, mixed Close emulsion B;
(3)The gelatin of parts by weight is taken, appropriate water is added, solution is formed, in the case where solution temperature is 50-60 DEG C, added Step(2)In obtained mixed emulsion B, stir, obtain emulsion C, the pH value that emulsion C is then adjusted with acetum is Less than 5.0, emulsion C is placed on magnetic stirring apparatus stirred 25-35 minutes afterwards, then stand half an hour at 15-20 DEG C, It is allowed to carry out microencapsulation;
(4)The material of microencapsulation is dried at 40-50 DEG C, is then placed in comminutor and granulates, you can obtain containing meat The microencapsulation plants essential oil culicifuge of oil of bay.
The microencapsulation plants essential oil culicifuge containing cinnamon oil that the present invention is prepared uses non-woven fabrics pouch when in use Son(50mm*30mm)Install, the amount of being put into of culicifuge is 1/3rd of sack capacity, and sack then is placed on into room In corner.
In the present invention, described cinnamon oil for canella Chinese cassia tree Cinnamomum cassia Presl drying branch, The volatile oil that leaf is obtained through vapor distillation.Cinnamon oil is widely used in medicine, food and light industry industry.It is classified as in history tree Top grade, it is believed that have mends fire supporing yang, let the fire back to its origin, eliminating cold to stop pain, invigorate blood circulation etc. is acted on.The traditional Chinese medical science is as controlling waist and knee crymodynia, kidney deficiency Breathe heavily, dizziness due to yang deficiency, hot eyes pharyngalgia, trusted subordinate's crymodynia, cold of insufficiency type vomiting and diarrhea, cold hernia, run quickly globefish, Amenorrhea, emmenagogue is used.Modern study shows Show, Chinese cassia tree has a variety of effects such as antibacterial, antitumor, antiulcer, antipyretic, analgesia spasmolysis, establishing-Yang, desinsection, and cinnamon oil is to common Bacterium(Escherichia coli, salmonella, bacillus subtilis, Dipel etc.), saccharomycete(Brewer's yeast, Saccharomyces cerevisiae Deng), mould(Aspergillus niger, aspergillus oryzae, aspergillus flavus, mould, trichoderma, Mucor, head mold etc.)It is respectively provided with very strong inhibitory action, Chinese cassia tree Oil there is natural insect-repelling desinsection, killing fungus, again will not contaminated food, to mosquito drive effect significantly.
Described wormwood essential oil is from wormwood(Scientific name:Artemisia argyi H. Lév. & Vaniot)Leaf, The extract of stem, extrusion and solvent extraction method refine the volatile flavor of extraction.Folium artemisiae argyi has antibacterial and antiviral work With;Relieving asthma, antibechic and phlegm-dispelling functions;Hemostasis and blood coagulation resisting function;Calm and anti-allergic effects;Protect liver choleretic effect etc..Wormwood With a kind of special fragrance, this special fragrance has effects that mosquito dispersing, so, ancients often hang wormwood, one in front of the door For avoiding evil spirits, two are used to driving mosquito away.Wormwood has special fragrance taste, makes fragrance pillow, also it is sleeping help to sleep recover from fatigue Effect.Wormwood leaf extractive, then dilution is watered shower, can be except small red pimple long with it.Additionally can be with mosquito repellent fly, sterilizing Sterilization, prevention disease.Wormwood or a kind of food plant, wormwood can make " folium artemisiae argyi tea ", " folium artemisiae argyi soup ", " folium artemisiae argyi congee ", argy wormwood steamed bun The recipes such as steamed bun, to strengthen resistivity of the human body to disease.Wormwood essential oil has rationale blood, and warm meridians, dispellieg cold and dampness is relieved pain, resisted Bacterium, anti-inflammatory encourages glandula digestive, and relieving cough and reducing sputum promotees circulation, and tonifying Qi lifts effect of immunity.
Shiu oil is by camphor tree(Classification system Cinnamomum camphora (L.) Presl.)Obtained by interior extraction, virtue Camphor tree is the evergreenness arbor for belonging to Lauraceae, and shiu oil has analgesic, anti-depression, antibacterial, anti-spasm, sharp heart, flatulence of dispelling, profit Urinate, bring down a fever, raise blood pressure, desinsection, laxative, make that skin is warm, encourage, urge sweat, expelling parasite, control wound, repelling mosquitoes and preventing insects mosquito, sterilization It is antipruritic, except foot odour, anti-tinea pedis, purify air effect;Available for antibacterial and viral infection resisting, deodorant, anti-caries agent, calmness Effect, insecticide, acaricide;Improve Fat quality, stabilization can be played to foam, using tea as the aromatic beverage of matrix, mould proof Agent, animal repellant, in daily chemical products bad smell screening agent.
Silver grey chrysanthemum is evergreen perennial herb, Classification system Santolina chamaecyparissus L., and silver grey chrysanthemum is Conventional fragrant plant with mosquito repellent function.Silver grey chrysanthemum essential oil main component is artemone, vulgarone, β-phellandrene, turmeric Alkene, laurene, sabinene, nopinene etc., total percentage composition account for 83.44%, and the silver grey chrysanthemum essential oil of low concentration can be produced to mosquito children Lethal effect, the repelling effect of silver grey chrysanthemum essential oil very well, and lemon grass (Cymbopogon citratus) essential oil when being used in mixed way repelling effect it is stronger.
Described lemon grass (Cymbopogon citratus) essential oil is to extract from lemon grass (Cymbopogon citratus)(Scientific name: Cymbopogon citratus (DC.) Stapf) A kind of essential oil, have extraordinary anti-depression, antibacterial, sterilize, ventosity of dispelling, deodorization, help digest, diuresis, killing fungus, urge Breast, kill insect, prevention disease, excitation, mend body the effects such as;Excitation, recovery, generation energy, have very much for used-up state Help, improve spirit, set out again;It is powerful, micro- sweet tea, with lemonene taste.It makes body recapture the effect of vigor, can mitigate The malaise symptoms of some time differences, allow clearheaded, dispelling fatigue.Effective expelling parasite, makes flea, insect with animal remote, and Deodorization functions can allow animal to keep good odour.
Rosemary, Classification system(Rosmarinus officinalis)Labiatae shrub, rosemary is also Mozzie buster, is Perennial xylophyta, distributes cool peppermint fragrance throughout the year, has repelling effect, and have air purification effect.From rosemary Antioxidant and Rosemary Oil with excellent anti-oxidation characteristics can be extracted in flower and leaf.Rosemary Oil(Classification system Rosmarinus officinalis)It is a kind of colourless to faint yellow volatile liquid.Rosemary is very helpful to respiratory system, The respiratory diseases such as flu, bronchitis, can use Rosemary Oil, and Rosemary Oil has sterilization, desinsection, anti-inflammatory etc. Effect, very well, Rosemary Oil is used for spices, air freshener, drives the daily-use chemical industry such as ant agent and sterilization, desinsection repelling effect Industry.
Neem oil is margosa(neem tree, Azadirachta indica)Benevolence extract, it has desinsection And deterrent effect, it can be used as insecticide.Neem oil contains a kind of chemical composition for being referred to as nimbin (Azadirachtin), With potent antimicrobial acivity, while having insecticidal effect, neem oil is a kind of fabulous product, can be used as desinsection Agent can also be used using outer as pest repellant and growth regulator.The scope of the anti-system of neem oil is quite varied, includes aphid, Ji Pu Sai dances moth, leaf mining insect, geometer, powder scale insect, thrips and aleyrodid etc..Also importance insect, such as potato can be killed Chrysomelid worm, corn earworm, leaf flea beetle worm etc., also have effect of control for powdery mildew, dew bacterium disease, anthracnose, rust etc. in addition.It is bitter Chinaberry oil is a kind of agent that improves of immune system, is directly applied to the problem of being effective against Tou Lice on scalp, can also utilize it To carry out the health maintenance of animal, neem oil directly can be applied on skin in many cases in the outer used time.
The beneficial effect comprise that:
1st, the present invention is prepared in the microencapsulation plants essential oil culicifuge containing cinnamon oil, and the cinnamon oil of addition is to common bacteria (Escherichia coli, salmonella, bacillus subtilis, Dipel etc.), saccharomycete(Brewer's yeast, Saccharomyces cerevisiae etc.), it is mould Bacterium(Aspergillus niger, aspergillus oryzae, aspergillus flavus, mould, trichoderma, Mucor, head mold etc.)Very strong inhibitory action is respectively provided with, cinnamon oil has Effect of natural insect-repelling desinsection, killing fungus, again will not contaminated food, the effect of driveing to mosquito is notable, adds cinnamon oil so that The mosquito-repelling function of the microencapsulation plants essential oil culicifuge containing cinnamon oil prepared is strengthened.
2nd, the microencapsulation plants essential oil culicifuge of the invention containing cinnamon oil is with cinnamon oil, wormwood essential oil, fragrant camphor tree essential oil Deng what is be prepared from for raw material, without conventional chemical insecticide, safe and environment-friendly, pollution-free and used raw material is to mosquito There is good dispersion effect, skin is not stimulated, dispelling fatigue, the quiet effect calmed the nerves can be also played to human body.
3rd, the various raw materials used in the present invention, which are rationally assembled, uses it, can play a part of Synergistic, and effectively Solve the problem of single plant essential oil has inefficiency and single fragrance, repelling effect is good, and essential oil is carried out micro- Encapsulated, overcomes strong, the strong volatility of essential oil fragrance, stimulation, makes us using uncomfortable defect, what the present invention was prepared contains There is the microencapsulation plants essential oil culicifuge of cinnamon oil, it is natural with comfortable, pleasure unique perfume without strong, stimulation fragrance Dissipate perfume, repelling effect duration is long, effect is good, using, carry all very convenient, human body is had no side effect.
Embodiment
Embodiment 1:
A kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, is prepared from the following raw materials in parts by weight:
The core of microcapsules:3 parts of cinnamon oil;15 parts of wormwood essential oil;10 parts of shiu oil;Silver grey 4 parts of chrysanthemum essential oil;Lemon grass (Cymbopogon citratus) essence 6 parts of oil;7 parts of Rosemary Oil;2 parts of neem oil;
Additives:Sorbester p17,4 parts;
The wall material of microcapsules:13 parts of Arabic gum, 12 parts of gelatin.
Above-mentioned a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, it is characterised in that described contains Chinese cassia tree The preparation method step of the microencapsulation plants essential oil culicifuge of oil is as follows:
(1)The sorbester p17 of parts by weight is taken, the water that temperature is 35 DEG C is added, the solution that mass fraction is 4%-6% is configured to A;
(2)The Arabic gum of parts by weight is taken, according to volume ratio Arabic gum:Water is 1:2 ratio adds water, and stirring is equal It is even, the core of the microcapsules of parts by weight is then added, and add step(1)In obtained solution A, stir, mixed Close emulsion B;
(3)The gelatin of parts by weight is taken, appropriate water is added, solution is formed, in the case where solution temperature is 50 DEG C, step is added (2)In obtained mixed emulsion B, stir, obtain emulsion C, the pH value that emulsion C is then adjusted with acetum is 5.0 Hereinafter, emulsion C is placed on magnetic stirring apparatus afterwards and stirred 35 minutes, then stood half an hour at 15 DEG C, be allowed to carry out Microencapsulation;
(4)The material of microencapsulation is dried at 40 DEG C, is then placed in comminutor and granulates, you can obtain containing cinnamon oil Microencapsulation plants essential oil culicifuge.
Embodiment 2:
A kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, is prepared from the following raw materials in parts by weight:
The core of microcapsules:5 parts of cinnamon oil;17 parts of wormwood essential oil;12 parts of shiu oil;Silver grey 5 parts of chrysanthemum essential oil;Lemon grass (Cymbopogon citratus) essence 7 parts of oil;9 parts of Rosemary Oil;3 parts of neem oil;
Additives:Sorbester p17,5 parts;
The wall material of microcapsules:15 parts of Arabic gum, 13 parts of gelatin.
Above-mentioned a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, it is characterised in that described contains Chinese cassia tree The preparation method step of the microencapsulation plants essential oil culicifuge of oil is as follows:
(1)The sorbester p17 of parts by weight is taken, the water that temperature is 38 DEG C is added, the solution that mass fraction is 4%-6% is configured to A;
(2)The Arabic gum of parts by weight is taken, according to volume ratio Arabic gum:Water is 1:2 ratio adds water, and stirring is equal It is even, the core of the microcapsules of parts by weight is then added, and add step(1)In obtained solution A, stir, mixed Close emulsion B;
(3)The gelatin of parts by weight is taken, appropriate water is added, solution is formed, in the case where solution temperature is 53 DEG C, step is added (2)In obtained mixed emulsion B, stir, obtain emulsion C, the pH value that emulsion C is then adjusted with acetum is 5.0 Hereinafter, emulsion C is placed on magnetic stirring apparatus afterwards and stirred 31 minutes, then stood half an hour at 18 DEG C, be allowed to carry out Microencapsulation;
(4)The material of microencapsulation is dried at 44 DEG C, is then placed in comminutor and granulates, you can obtain containing cinnamon oil Microencapsulation plants essential oil culicifuge.
Embodiment 3:
A kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, is prepared from the following raw materials in parts by weight:
The core of microcapsules:6 parts of cinnamon oil;19 parts of wormwood essential oil;13 parts of shiu oil;Silver grey 6 parts of chrysanthemum essential oil;Lemon grass (Cymbopogon citratus) essence 8 parts of oil;11 parts of Rosemary Oil;4 parts of neem oil;
Additives:Sorbester p17,5 parts;
The wall material of microcapsules:17 parts of Arabic gum, 15 parts of gelatin.
Above-mentioned a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, it is characterised in that described contains Chinese cassia tree The preparation method step of the microencapsulation plants essential oil culicifuge of oil is as follows:
(1)The sorbester p17 of parts by weight is taken, the water that temperature is 42 DEG C is added, the solution that mass fraction is 4%-6% is configured to A;
(2)The Arabic gum of parts by weight is taken, according to volume ratio Arabic gum:Water is 1:2 ratio adds water, and stirring is equal It is even, the core of the microcapsules of parts by weight is then added, and add step(1)In obtained solution A, stir, mixed Close emulsion B;
(3)The gelatin of parts by weight is taken, appropriate water is added, solution is formed, in the case where solution temperature is 56 DEG C, step is added (2)In obtained mixed emulsion B, stir, obtain emulsion C, the pH value that emulsion C is then adjusted with acetum is 5.0 Hereinafter, emulsion C is placed on magnetic stirring apparatus afterwards and stirred 28 minutes, then stood half an hour at 20 DEG C, be allowed to carry out Microencapsulation;
(4)The material of microencapsulation is dried at 47 DEG C, is then placed in comminutor and granulates, you can obtain containing cinnamon oil Microencapsulation plants essential oil culicifuge.
Embodiment 4:
A kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, is prepared from the following raw materials in parts by weight:
The core of microcapsules:7 parts of cinnamon oil;20 parts of wormwood essential oil;15 parts of shiu oil;Silver grey 7 parts of chrysanthemum essential oil;Lemon grass (Cymbopogon citratus) essence 10 parts of oil;12 parts of Rosemary Oil;5 parts of neem oil;
Additives:Sorbester p17,6 parts;
The wall material of microcapsules:18 parts of Arabic gum, 17 parts of gelatin.
Above-mentioned a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, it is characterised in that described contains Chinese cassia tree The preparation method step of the microencapsulation plants essential oil culicifuge of oil is as follows:
(1)The sorbester p17 of parts by weight is taken, the water that temperature is 45 DEG C is added, the solution that mass fraction is 4%-6% is configured to A;
(2)The Arabic gum of parts by weight is taken, according to volume ratio Arabic gum:Water is 1:2 ratio adds water, and stirring is equal It is even, the core of the microcapsules of parts by weight is then added, and add step(1)In obtained solution A, stir, mixed Close emulsion B;
(3)The gelatin of parts by weight is taken, appropriate water is added, solution is formed, in the case where solution temperature is 60 DEG C, step is added (2)In obtained mixed emulsion B, stir, obtain emulsion C, the pH value that emulsion C is then adjusted with acetum is 5.0 Hereinafter, afterwards by emulsion C be placed on magnetic stirring apparatus stir 25 minutes, then stand half an hour at 15-20 DEG C, be allowed into Row microencapsulation;
(4)The material of microencapsulation is dried at 50 DEG C, is then placed in comminutor and granulates, you can obtain containing cinnamon oil Microencapsulation plants essential oil culicifuge.
Application effect
Specific method of testing:
(1) tester:Closed transparent vessel (specification is 50cm*50cm*50cm);
(2) test object:There is the mosquito 100 of normal life vigor;
Test process:Place l00 mosquito in closed transparent vessel 100cm*50cm*50cm, the inside.It is held by hand equipped with this Invent the non-woven fabrics pouch of the microencapsulation plants essential oil culicifuge containing cinnamon oil prepared(50mm*30mm), mosquito repellent The amount of being put into of agent is 1/3rd of sack capacity, is then reached into container, mosquito does not bite completely within one and a half hours, and And avoid;Mosquito flies in container surrounding near corners after 2 and a half hours;Mosquito is accumulated in surrounding corner after 4 hours;5 The mosquito overwhelming majority just falls the bottom farthest from pouch after hour;Still there are 5 mosquitoes in space flight.
Repelling effect reaches 95%.

Claims (1)

1. a kind of microencapsulation plants essential oil culicifuge containing cinnamon oil, it is characterised in that be by the raw material of following parts by weight It is made:
The core of microcapsules:3-7 parts of cinnamon oil;15-20 parts of wormwood essential oil;10-15 parts of shiu oil;Silver grey chrysanthemum essential oil 4-7 parts;6-10 parts of lemon grass (Cymbopogon citratus) essential oil;7-12 parts of Rosemary Oil;2-5 parts of neem oil;
Additives:Sorbester p17,4-6 parts;
The wall material of microcapsules:13-18 parts of Arabic gum;12-17 parts of gelatin;
The preparation method step of described microencapsulation plants essential oil culicifuge is as follows:
(1)The sorbester p17 of parts by weight is taken, the water that temperature is 35-45 DEG C is added, it is the molten of 4%-6% to be configured to mass fraction Liquid A;
(2)The Arabic gum of parts by weight is taken, according to volume ratio Arabic gum:Water is 1:2 ratio adds water, and stirring is equal It is even, the core of the microcapsules of parts by weight is then added, and add step(1)In obtained solution A, stir, mixed Close emulsion B;
(3)The gelatin of parts by weight is taken, appropriate water is added, solution is formed, in the case where solution temperature is 50-60 DEG C, step is added (2)In obtained mixed emulsion B, stir, obtain emulsion C, emulsion C pH values are then adjusted with acetum For less than 5.0, emulsion C is placed on magnetic stirring apparatus stirs 25-35 minute afterwards, then the standing at 15-20 DEG C Half an hour, it is allowed to carry out microencapsulation;
(4)The material of microencapsulation is dried at 40-50 DEG C, is then placed in comminutor and granulates, you can obtain microencapsulation plant Essential mosquito repellent.
CN201510277804.0A 2015-05-27 2015-05-27 Microencapsulation plants essential oil culicifuge containing cinnamon oil Expired - Fee Related CN104872215B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510277804.0A CN104872215B (en) 2015-05-27 2015-05-27 Microencapsulation plants essential oil culicifuge containing cinnamon oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510277804.0A CN104872215B (en) 2015-05-27 2015-05-27 Microencapsulation plants essential oil culicifuge containing cinnamon oil

Publications (2)

Publication Number Publication Date
CN104872215A CN104872215A (en) 2015-09-02
CN104872215B true CN104872215B (en) 2017-11-03

Family

ID=53940117

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510277804.0A Expired - Fee Related CN104872215B (en) 2015-05-27 2015-05-27 Microencapsulation plants essential oil culicifuge containing cinnamon oil

Country Status (1)

Country Link
CN (1) CN104872215B (en)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105614641B (en) * 2015-09-06 2019-12-03 上海应用技术学院 A kind of cinnamon essential oil microcapsule and preparation method thereof assembled automatically layer by layer
CN106511125A (en) * 2015-09-09 2017-03-22 佩兰生物科技(上海)股份有限公司 Eupatorium fortunei turcz compound solid-state essential oil and uses thereof, eupatorium fortunei turcz compound solid-state essential oil capsule preparation method
CN105248460B (en) * 2015-10-09 2018-02-06 广州潮徽生物科技有限公司 A kind of composite antibacterial composition containing microcapsules and preparation method and application
CN105463604A (en) * 2015-12-25 2016-04-06 江苏金太阳纺织科技股份有限公司 Preparation method of regenerated cellulose fiber containing cinnamon oil microcapsule
CN105442331A (en) * 2015-12-25 2016-03-30 江苏金太阳纺织科技股份有限公司 Antibacterial mite-proofing finishing agent and preparation method thereof
CN106035326A (en) * 2016-06-06 2016-10-26 南通伟德动力电池研究所(普通合伙) Preparation method of fragrance microcapsule spraying agent for dispelling houseflies
CN106120354A (en) * 2016-06-23 2016-11-16 无锡市金五星针纺有限公司 It is a kind of that natural plant is mosquito-proof drives fly microcapsule dressing agent and its preparation method and application
CN106012555A (en) * 2016-06-23 2016-10-12 无锡市金五星针纺有限公司 Mosquito preventing and fly repelling microcapsule finishing agent as well as preparation method and application thereof
CN106420410A (en) * 2016-09-28 2017-02-22 济南大学 Preparing method of fresh and scent type natural botanical mosquito repellant liquor
CN107375628B (en) * 2017-06-28 2020-06-16 安徽省凯强生物科技有限公司 Microcapsule-loaded plant source fishing pesticide
CN107853298A (en) * 2017-09-01 2018-03-30 南通香佳纺织科技有限公司 A kind of Catnip oil microcapsule toy finishing agent and preparation method thereof
CN107675512A (en) * 2017-09-15 2018-02-09 南通香佳纺织科技有限公司 A kind of microcapsules children down toy finishing agent and preparation method thereof
CN107747227A (en) * 2017-09-15 2018-03-02 南通香佳纺织科技有限公司 A kind of microcapsules diabetes socks finishing agent and preparation method thereof
CN108690730A (en) * 2018-05-25 2018-10-23 广州番禺职业技术学院 A kind of candle and preparation method thereof with mosquito-prevention mosquito-repellent
CN110638700B (en) * 2018-06-27 2022-07-01 山东大学 Mosquito repellent liquid extracted from pure plants and preparation method thereof
ES2769604A1 (en) * 2018-12-26 2020-06-26 Zobele Espana Sa Combustion volatile substances diffusion device (Machine-translation by Google Translate, not legally binding)
CN110583708B (en) * 2019-09-05 2022-01-18 天津市城西广源电力工程有限公司 Mosquito-repelling microcapsule and preparation method thereof
CN110522678A (en) * 2019-10-18 2019-12-03 周梦斯 A kind of Jasmine long-acting mosquito-driving agent and preparation method thereof
CN110637839A (en) * 2019-10-18 2020-01-03 周梦斯 Jasmine flower mosquito repellent with nerve calming and sleep aiding effects and preparation method thereof
CN110810444A (en) * 2019-11-21 2020-02-21 信阳农林学院 Insecticidal synergistic composition of camphor essential oil and bifenthrin
CN112294870A (en) * 2020-11-06 2021-02-02 江苏省中医药研究院 Cinnamon oil microsphere inclusion compound and preparation method and application thereof
CN112494405A (en) * 2020-12-25 2021-03-16 泰州市榕兴医疗用品股份有限公司 Long-acting skin-care mosquito-repellent cream
CN112457126A (en) * 2021-02-01 2021-03-09 江西绿博士生物科技有限公司 Cortex meliae extract microcapsule, preparation method and application in soil improvement fertilizer
CN114768697A (en) * 2022-04-03 2022-07-22 湖州市食品药品检验研究院(湖州市药品和医疗器械不良反应监测中心、湖州市医疗器械监督检验中心、湖州市食品认证审评和粮油质量监测中心) Preparation process and preparation device of cinnamon essential oil microcapsules

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101946811A (en) * 2010-08-26 2011-01-19 天津绿新低温科技有限公司 Microencapsulated botanical insect-resist agent
CN102808361A (en) * 2011-06-02 2012-12-05 金红叶纸业集团有限公司 Paper for daily use with mosquito repellent function and production method thereof
CN103349006A (en) * 2013-07-16 2013-10-16 东北林业大学 Black pepper essential oil microcapsule and preparation method thereof

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060165746A1 (en) * 2005-01-24 2006-07-27 Arie Markus Formulations containing microencapsulated essential oils

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101946811A (en) * 2010-08-26 2011-01-19 天津绿新低温科技有限公司 Microencapsulated botanical insect-resist agent
CN102808361A (en) * 2011-06-02 2012-12-05 金红叶纸业集团有限公司 Paper for daily use with mosquito repellent function and production method thereof
CN103349006A (en) * 2013-07-16 2013-10-16 东北林业大学 Black pepper essential oil microcapsule and preparation method thereof

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
"Microencapsulation:industrial appraisal of existing technologies and trends";Se´bastien Gouin,;《Trends in Food Science & Technology》;20040831;第15卷(第7期);第330-347页 *
"复合凝聚法制备避蚊胺微胶囊的研究";胡云峰等,;《辽宁化工》;20080620;第37卷(第6期);第378-380,384页 *
"微囊技术在驱蚊长袜工艺中的应用";郑光洪等,;《成都纺织高等专科学校学报》;19971015;第14卷(第4期);第42页2.1节,第43页2.7节 *
"蚊虫驱避剂及其剂型的研究进展";郑璐璐等,;《药学实践杂志》;20120525;第30卷(第3期);第168-170,202页 *

Also Published As

Publication number Publication date
CN104872215A (en) 2015-09-02

Similar Documents

Publication Publication Date Title
CN104872215B (en) Microencapsulation plants essential oil culicifuge containing cinnamon oil
CN104186565A (en) Electric-heating liquid mosquito-repellent incense with natural plant fragrance of agilawood and preparation method of electric-heating liquid mosquito-repellent incense
CN103392748B (en) Natural mosquito repellent incense and preparation method thereof
CN104585255A (en) Mosquito-repelling bactericide
CN105230685B (en) Herbaceous plant essential oil composition with repelling effect
CN106265147A (en) A kind of floral water containing natural plant essential oils and preparation method thereof
CN105594766A (en) Natural bamboo charcoal mosquito-repellent incense and manufacturing method thereof
CN110037059B (en) Mosquito-repellent insect-prevention sachet and preparation method thereof
KR101488642B1 (en) Compact air purifier exuding fragrance of oriental medical herb
CN108419810A (en) A kind of natural plant composition compound bio insect aerosol
CN104621192A (en) Natural plant anti-mite insert-killing fragrant agent
CN104875693A (en) Natural mosquito repelling plant and active mineral composed automobile front-wall sound insulating pad
CN104758322A (en) Composition capable of expelling insects, killing bacteria, sterilizing, and relieving nerve, and applications thereof
CN110352993A (en) A kind of plant bacteria-removing liquid
CN105708763A (en) Artemisia argyi Levl extract-containing floral water and preparation method thereof
KR101898060B1 (en) Natural aroma essential oil water soluble composition for humidifier disinfectant and the method of manufaturing the same
CN104186577A (en) Slow-release electrothermal mosquito incense liquor containing ambergris extract and preparation method
CN104186569A (en) Electric heating liquid mosquito-repellent incense with mint fragrance and preparation method thereof
CN104186572A (en) Sustained-release calamus electric heating liquid mosquito-repellent incense and preparation method thereof
CN106577841A (en) Electric heating type Chinese mugwort essential oil mosquito repellent
CN110522678A (en) A kind of Jasmine long-acting mosquito-driving agent and preparation method thereof
CN105030124A (en) Azedarach functional-type tissue box with air purification function
CN104511042A (en) Water lily flower incense coil
CN104888260A (en) Traditional Mongolian and Chinese medicine air freshener for realizing insect expelling and sterilization of muniment room
CN104186579A (en) Electric-heating liquid mosquito-repellent incense utilizing natural extracts of aloe and preparation method of electric-heating liquid mosquito-repellent incense

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
EXSB Decision made by sipo to initiate substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20171103

Termination date: 20210527

CF01 Termination of patent right due to non-payment of annual fee