CN105532754B - A kind of infested natural plants combined extracts to go mouldy of prevention grain - Google Patents
A kind of infested natural plants combined extracts to go mouldy of prevention grain Download PDFInfo
- Publication number
- CN105532754B CN105532754B CN201610075361.1A CN201610075361A CN105532754B CN 105532754 B CN105532754 B CN 105532754B CN 201610075361 A CN201610075361 A CN 201610075361A CN 105532754 B CN105532754 B CN 105532754B
- Authority
- CN
- China
- Prior art keywords
- grain
- combined extracts
- natural plants
- mouldy
- infested
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Microbiology (AREA)
- Environmental Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Dentistry (AREA)
- Mycology (AREA)
- Polymers & Plastics (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Botany (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A kind of infested natural plants combined extracts to go mouldy of prevention grain, including following components in percentage by weight：Soapberry fruit 20%~60%, dried orange peel 10%~20%, fennel seeds 10%~20%, cloves 10%~20%, the fruit of a cubeb litsea tree 10%~20%.The advantage of the invention is that component is reasonable, safety is good, can effectively prevent that grain is infested to go mouldy, and preparation method is simple, and raw material is easy to get, is at low cost, and dosage is smaller, environment-friendly high-efficiency, application easy to spread.
Description
Technical field
The present invention relates to a kind of natural plants combined extracts, more particularly, to a kind of prevention grain it is infested go mouldy it is natural
Plant society extract.
Background technology
With science and technology rapid advances and socio-economic development mode transformation, grain storage technology emphasis to " peace
The direction of full nutrition, green ecological, pollution-free, fresh and healthy " is developed, and " extensively store up grain, accumulated grain, stored up grain well " is truly realized, full
Sufficient consumers in general are food-safe, nutrition, health demand.And grain is during storage, main harm be exactly insect pest with
And mould generate go mouldy.It generally uses now and the best grain entomophthora control method of effect is exactly to utilize toxic chemical substance
As aluminum phosphate is fumigated, but this chemical substance is stifling can bring food safety hazards and problem of environmental pollution.
Paddy, wheat and corn are the main food types of China's agricultural planting, and national grain depot and peasant household it is main
Store grain kind.Therefore, the stifling natural green plant extracts of can effectively replace toxic chemical substance is developed as grain worm
Mould control agent is the major issue of Ensuring Food Safety.
Invention content
The technical problem to be solved by the present invention is to overcome the deficiencies in the prior art avoids the poison of chemical synthesis additive secondary
Effect, providing a kind of can effectively prevent the infested infested natural plants combined extracts to go mouldy of prevention grain to go mouldy of grain.
The present invention solve its technical problem the technical solution adopted is that, a kind of infested natural plants group gone mouldy of prevention grain
Close extract, including following components in percentage by weight：Soapberry fruit 20%~60%, dried orange peel 10%~20%, fennel seeds 10%~
20%, cloves 10%~20%, the fruit of a cubeb litsea tree 10%~20%.
The preparation method of the natural plants combined extracts：
Take all raw materials, smash it through 100 mesh sieve, be added be equivalent to 5~20 times of raw material weight water or volumetric concentration≤
95% ethanol solution impregnates 20~60 minutes at 25 DEG C~60 DEG C, then the 500-600w ultrasonic wave extractions 4 at 30 DEG C~60 DEG C
~6 hours, vacuum filtration, obtained filtrate carried out ultrafiltration through the ultrafiltration membrane that molecular cut off is 5kD and 50kD respectively, obtains
The solution of fraction is natural plants combined extracts among 5kD to 50kD.
Application method：By the natural plants combined extracts of the present invention, to be equivalent to the use of grain weight 0.5-1.0%
Amount is uniformly sprayed at grain surface.
The advantage of the invention is that component is reasonable, safety is good, can effectively prevent that grain is infested to go mouldy, preparation method letter
Single, raw material is easy to get, is at low cost, and dosage is smaller, environment-friendly high-efficiency, application easy to spread.
Specific implementation mode
The invention will be further described with reference to embodiments.
Embodiment 1
The infested natural plants combined extracts to go mouldy of the prevention grain of the present embodiment, include the group of following weight percent
Point：Soapberry fruit 20%, dried orange peel 20%, fennel seeds 20%, cloves 20%, the fruit of a cubeb litsea tree 20%.
The preparation method of the natural plants combined extracts：
All raw materials are taken, 100 mesh sieve is smashed it through, the water for being equivalent to 5 times of raw material weight is added, is impregnated 40 minutes at 30 DEG C
Afterwards, then at 30 DEG C 500w ultrasonic wave extractions are carried out 4 hours, vacuum filtration, obtained filtrate is respectively 5kD through molecular cut off
Ultrafiltration is carried out with the ultrafiltration membrane of 50kD, the solution of fraction is natural plants combined extracts among obtained 5kD to 50kD.
Application method：The natural plants combined extracts of the present embodiment are uniform by the dosage for being equivalent to grain weight 0.5%
It is sprayed at grain（Paddy, corn, wheat etc.）Surface.
Control 1（Blank control）：Water is uniformly sprayed at grain by the dosage for being equivalent to grain weight 0.5%（Paddy, jade
Rice, wheat etc.）Surface.
Control 2：It is uniform by the dosage for being equivalent to grain weight 0.5% by soapberry fruit after the extraction of the method for the present invention
It is sprayed at grain（Paddy, corn, wheat etc.）Surface.
The result shows that after the natural plants combined extracts of the sprinkling present invention, grain can be made in 30 DEG C, relative humidity 80%
Under conditions of（This condition is the bacterium condition that easily mildews）Storage 20 days or more does not go mouldy；Grain can be made to place under field conditions (factors)
One summer（The Changsha 6-9 months）It is insect-free.
And compare 1（Blank control）Grain under conditions of 30 DEG C, relative humidity 80% 3 days i.e. can go mouldy；Meanwhile grain
Food places a summer under field conditions (factors)（The Changsha 6-9 months）, there are a large amount of infested phenomenons.
And compare 2（100% soapberry fruit actually raw material water extract obtained and by above-mentioned as stated above is used alone
Method is used）, grain can be made not go mouldy within 8 days under conditions of 30 DEG C, relative humidity 80%, grain is in natural conditions
One summer of lower placement（The Changsha 6-9 months）, infested rate is less than the grain of control 1, but is more than and uses the embodiment of the present invention 1
Plant extracts processing grain.
Embodiment 2
The infested natural plants combined extracts to go mouldy of the prevention grain of the present embodiment, include the group of following weight percent
Point：Soapberry fruit 40%, dried orange peel 15%, fennel seeds 15%, cloves 15%, the fruit of a cubeb litsea tree 15%.
The preparation method of the natural plants combined extracts：
All raw materials are taken, 100 mesh sieve is smashed it through, it is 55% ethyl alcohol to be added and be equivalent to the volumetric concentration of 10 times of raw material weight
Aqueous solution impregnates 20 minutes at 50 DEG C, then progress 500w ultrasonic wave extractions 5 hours at 40 DEG C, vacuum filtration, obtained filter
Liquid carries out ultrafiltration through the ultrafiltration membrane that molecular cut off is 5kD and 50kD respectively, and the solution of the obtained centres 5kD to 50kD fraction is i.e.
For natural plants combined extracts.
Application method：The natural plants combined extracts of the present embodiment are uniform by the dosage for being equivalent to grain weight 0.5%
It is sprayed at grain（Paddy, corn, wheat etc.）Surface.
Control 1（Blank control）：It is that 55% ethanol water is equal by the dosage for being equivalent to grain weight 0.5% by volumetric concentration
It is even to be sprayed at grain（Paddy, corn, wheat etc.）Surface.
Control 2：It is uniform by the dosage for being equivalent to grain weight 0.5% by soapberry fruit after the extraction of the method for the present invention
It is sprayed at grain（Paddy, corn, wheat etc.）Surface.
The result shows that after the natural plants combined extracts of the sprinkling present invention, grain can be made in 30 DEG C, relative humidity 80%
Under conditions of（This condition is the bacterium condition that easily mildews）Storage 50 days or more does not go mouldy；Grain can be made to place under field conditions (factors)
One summer（The Changsha 6-9 months）It is insect-free.
And compare 1（Blank control）Grain under conditions of 30 DEG C, relative humidity 80% 6 days i.e. can go mouldy；Meanwhile grain
Food places a summer under field conditions (factors)（The Changsha 6-9 months）, there are a large amount of infested phenomenons.
And compare 2（100% soapberry fruit actually raw material water extract obtained and by above-mentioned as stated above is used alone
Method is used）, grain can be made not go mouldy within 15 days under conditions of 30 DEG C, relative humidity 80%, grain is in natural conditions
One summer of lower placement（The Changsha 6-9 months）, only a small amount of infested, infested rate is less than the grain of control 1, but more than use
The grain of the plant extracts processing of the embodiment of the present invention 1.
Embodiment 3
The infested natural plants combined extracts to go mouldy of the prevention grain of the present embodiment, include the group of following weight percent
Point：Soapberry fruit 60%, dried orange peel 10%, fennel seeds 10%, cloves 10%, the fruit of a cubeb litsea tree 10%.
The preparation method of the natural plants combined extracts：
All raw materials are taken, 100 mesh sieve is smashed it through, the ethyl alcohol for the volumetric concentration 95% for being equivalent to 20 times of raw material weight is added
Aqueous solution impregnates 20 minutes at 60 DEG C, then carries out at 60 DEG C 500w ultrasonic wave extractions 4 hours, vacuum filtration, obtained filtrate
Ultrafiltration is carried out through the ultrafiltration membrane that molecular cut off is 5kD and 50kD respectively, the solution of the obtained centres 5kD to 50kD fraction is
Natural plants combined extracts.
Application method：The natural plants combined extracts of the present embodiment are uniform by the dosage for being equivalent to grain weight 0.5%
It is sprayed at grain（Paddy, corn, wheat etc.）Surface.
Control 1（Blank control）：The ethanol water of volumetric concentration 95% is equal by the dosage for being equivalent to grain weight 0.5%
It is even to be sprayed at grain（Paddy, corn, wheat etc.）Surface.
Control 2：It is uniform by the dosage for being equivalent to grain weight 0.5% by soapberry fruit after the extraction of the method for the present invention
It is sprayed at grain（Paddy, corn, wheat etc.）Surface.
The result shows that after the natural plants combined extracts of the sprinkling present invention, grain can be made in 30 DEG C, relative humidity 80%
Under conditions of（This condition is the bacterium condition that easily mildews）Storage 30 days or more does not go mouldy；Grain can be made to place under field conditions (factors)
One summer（The Changsha 6-9 months）It is insect-free.
And compare 1（Blank control）Grain under conditions of 30 DEG C, relative humidity 80% 7 days i.e. can go mouldy；Meanwhile grain
Food places a summer under field conditions (factors)（The Changsha 6-9 months）, there are a large amount of infested phenomenons.
And compare 2（100% soapberry fruit actually raw material water extract obtained and by above-mentioned as stated above is used alone
Method is used）, grain can be made not go mouldy within 10 days under conditions of 30 DEG C, relative humidity 80%, grain is in natural conditions
One summer of lower placement（The Changsha 6-9 months）, have a small amount of infested, infested rate is less than the grain of control 1, but more than using this
The grain of the plant extracts processing of inventive embodiments 1.
Claims (2)
1. a kind of infested natural plants combined extracts to go mouldy of prevention grain, which is characterized in that including following weight percent
Component：Soapberry fruit 20%~60%, dried orange peel 10%~20%, fennel seeds 10%~20%, cloves 10%~20%, the fruit of a cubeb litsea tree 10%
~20%；
The preparation method of the natural plants combined extracts：
All raw materials are taken, 100 mesh sieve is smashed it through, the water or volumetric concentration≤95% for being equivalent to 5~20 times of raw material weight is added
Ethanol solution impregnates 20~60 minutes at 25 DEG C~60 DEG C, then 500-600w ultrasonic wave extractions 4~6 are small at 30 DEG C~60 DEG C
When, vacuum filtration, obtained filtrate carries out ultrafiltration through the ultrafiltration membrane that molecular cut off is 5kD and 50kD respectively, and obtained 5kD is arrived
The solution of fraction is natural plants combined extracts among 50kD.
2. the infested natural plants combined extracts to go mouldy of prevention grain according to claim 1, which is characterized in that it makes
Use method：Dosage to be equivalent to grain weight 0.5-1.0% is uniformly sprayed at grain surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610075361.1A CN105532754B (en) | 2016-02-03 | 2016-02-03 | A kind of infested natural plants combined extracts to go mouldy of prevention grain |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610075361.1A CN105532754B (en) | 2016-02-03 | 2016-02-03 | A kind of infested natural plants combined extracts to go mouldy of prevention grain |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105532754A CN105532754A (en) | 2016-05-04 |
| CN105532754B true CN105532754B (en) | 2018-08-07 |
Family
ID=55812756
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610075361.1A Expired - Fee Related CN105532754B (en) | 2016-02-03 | 2016-02-03 | A kind of infested natural plants combined extracts to go mouldy of prevention grain |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105532754B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110228322A (en) * | 2019-07-12 | 2019-09-13 | 平凉可蓝山庄创意文化传媒有限责任公司 | A kind of production method that craft grain is drawn |
| CN111869729A (en) * | 2020-08-20 | 2020-11-03 | 岳阳弘昱农产品仓储有限公司 | Composite plant mildew preventive for paddy and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072819A (en) * | 1991-12-03 | 1993-06-09 | 北京市海淀区海得水产有限公司 | Grain protective agent and manufacture method |
| CN1095217A (en) * | 1993-05-19 | 1994-11-23 | 蒋立科 | The Chinese herbal medicine anti-mould anthelmintic |
| CN101731328A (en) * | 2009-12-22 | 2010-06-16 | 陈昕 | Application of caryophyllus oil as grain storage pest controlling agent |
| CN101946811A (en) * | 2010-08-26 | 2011-01-19 | 天津绿新低温科技有限公司 | Microencapsulated botanical insect-resist agent |
| CN104886183A (en) * | 2015-05-27 | 2015-09-09 | 闭炳春 | Cinnamon oil contained insect repelling mildew preventive for grain storage |
| CN105145633A (en) * | 2015-07-31 | 2015-12-16 | 北京泰克美高新技术有限公司 | Drug controlling plant nematodes |
-
2016
- 2016-02-03 CN CN201610075361.1A patent/CN105532754B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1072819A (en) * | 1991-12-03 | 1993-06-09 | 北京市海淀区海得水产有限公司 | Grain protective agent and manufacture method |
| CN1095217A (en) * | 1993-05-19 | 1994-11-23 | 蒋立科 | The Chinese herbal medicine anti-mould anthelmintic |
| CN101731328A (en) * | 2009-12-22 | 2010-06-16 | 陈昕 | Application of caryophyllus oil as grain storage pest controlling agent |
| CN101946811A (en) * | 2010-08-26 | 2011-01-19 | 天津绿新低温科技有限公司 | Microencapsulated botanical insect-resist agent |
| CN104886183A (en) * | 2015-05-27 | 2015-09-09 | 闭炳春 | Cinnamon oil contained insect repelling mildew preventive for grain storage |
| CN105145633A (en) * | 2015-07-31 | 2015-12-16 | 北京泰克美高新技术有限公司 | Drug controlling plant nematodes |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105532754A (en) | 2016-05-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104072280B (en) | A kind of preparation method of chitin active calcium fertilizer | |
| CN106363733B (en) | A kind of green mould proof insecticide of timber | |
| CN104496572A (en) | Plant enzyme biological fertilizer and preparation method thereof | |
| CN106615085A (en) | Microorganism and plant derived composite fresh keeping agent for fruits and vegetables | |
| CN106431660A (en) | Multifunctional biostimulant and preparation and application methods thereof | |
| CN104892086B (en) | A kind of compound seaweed fertilizer and preparation method thereof | |
| CN103999885A (en) | Bamboo wood preservative made from natural plant source and preparation method thereof | |
| CN104945144A (en) | Agricultural planting liquid fertilizer prepared from pure traditional Chinese medicines and plant extracting solutions | |
| CN106614815A (en) | Fruit and vegetable bactericide and production technique | |
| CN104892087A (en) | Plant cytolemma regulator solution | |
| CN101869042A (en) | Leechee longan before and after picking matched refreshing method | |
| CN101828596B (en) | Method for storage and fresh preservation of litchi fruits | |
| CN104522089A (en) | Green pollution-free plant compound preparation for preventing and treating virus, fungal and bacterial diseases of crops and preparation method and application thereof | |
| CN105532754B (en) | A kind of infested natural plants combined extracts to go mouldy of prevention grain | |
| CN106042117A (en) | Fading method for wheat straw | |
| CN104351329A (en) | Composite leaching vegetable fresh-keeping agent for tragus berteronianus and preparation method of fresh-keeping agent | |
| CN106116880A (en) | A kind of Pericarpium Zanthoxyli flower and fruit protecting nutrient | |
| CN104430636A (en) | Composition for preventing and treating diseases and insect pests of asparagus | |
| CN107467045A (en) | Preparation method using biogas slurry as the jamaicin aqua of solvent | |
| CN109526551B (en) | Cultivation method of natural selenium-rich agaricus bisporus | |
| KR20150068152A (en) | Method for manufacturing health supplement food using fermented and germinated grains | |
| CN104557154A (en) | Method for producing amino acid fertilizer from soybean meal through solid-state fermentation | |
| CN105918450A (en) | Fruit preservative as well as preparation method and use thereof | |
| CN106242671A (en) | A kind of magnetization charcoal base manure and preparation method thereof | |
| CN105985194A (en) | Ginkgo foliage spray fertilizer additive and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180807 Termination date: 20220203 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |