CN101913910B - Multicolor furnace transmutation glaze ground coat and manufacturing method thereof - Google Patents
Multicolor furnace transmutation glaze ground coat and manufacturing method thereof Download PDFInfo
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Abstract
The invention relates to a multicolor furnace transmutation glaze ground coat and a manufacturing method thereof. The manufacturing method comprises the step of adding a part of chromogenic oxides into feldspar, quartz, calcite, talc and kaolin which are selected as ground coat raw materials. Moreover, the ratio of silicate to aluminium of the ground coat must be over six, so that solution can be decomposed at high temperature to release gas to form a plurality of fine and dense small bubbles and defects are formed on the surface of a glaze layer; and then suitable cover glazes are matched to generate various furnace transmutation effects. According to a process formula of the glaze of the ground coat, the multicolor furnace transmutation glaze ground coat comprises the following components in part by weight: 45 parts of feldspar, 18 to 25 parts of quartz, 12 to 18 parts of calcite, 2 to 5 parts of talc, 5 to 12 parts of kaolin, 10 to 14 parts of iron oxide red and 2 to 5 parts of manganese carbonate. The ground coat prepared according to the process formula comprises the following chemical compositions: 58 to 64 percent of SiO2, 8 to 11 percent of Al2O3, 7 to 9.8 percent of CaO, 0.4 to 1.6 percent of MgO, 4 to 5.8 percent of K2O, 0.9 to 1.2 percent of Na2O, 9 to 13 percent of Fe2O3 and 0.9 to 2.3 percent of MnO.
Description
Technical field
The present invention relates to a kind of domestic ceramics glaze and preparation method thereof, refer in particular to a kind of adaptation domestic ceramics and display art pottery ground-coat enamel and preparation method thereof, this kind glaze is the ground-coat enamel that can produce multiple transmutation effect.The ceramic glaze technical field that belongs to ceramic.
Background technology
The transmutation glaze is ceramic glaze produces the artistic glaze of transmutation effect in sintering process a general designation.The ceramic glaze technical field that belongs to ceramic, the whole glaze and the part that are used for the domestic ceramics and the art pottery are decorated.The transmutation glaze is divided into individual layer and bilayer and multilayer transmutation glaze, and wherein individual layer transmutation glaze is just like zinc silicate crystalline glaze, titanium silicate crystalline glaze, lead silicate crystalline glaze and manganese crystalline glaze, iron crystalline glaze, aventurine glaze etc.; The famous rose violet that an ancient unit of weight kiln in the Northern Song Dynasty is arranged of double-deck transmutation glaze, Vermilion etc., it has broken through the unicolor limitation of coloured glaze, can produce changeable mobile line in burning till; Multilayer transmutation glaze is to execute two kinds and two or more glaze on base substrate, need rest several times, have plenty of a kind of color glaze branch and be suspended to certain thickness several times, have plenty of and execute earlier after one deck ground-coat enamel, divide color glaze or the colorant of hanging other several times more in the above, be used for the porcelain that the transmutation glaze is decorated, the glaze layer is thick with fixed attention, interlaced green grass or young crops, indigo plant, purple, brown Huang, multiple color such as bluish white appear in the glaze, and needle-like, radial luminous point, piece spot or crystallization arranged, add that glaze has the glass texture of light, makes glaze colours resplendent.But present transmutation fancy glaze product major part is the art display porcelain, how to apply it to domestic porcelain, particularly on the tableware for daily use, because the cover-coat enamel and the porcelain embryo of existing furnace transmutation glaze ground coat and domestic porcelain not really adapt to, mainly be perplexed by viscosity problem, so limited the popularization of this kind ground-coat enamel transmutation glaze on domestic ceramics.Therefore, a kind of suitability of necessary development is ground-coat enamel widely, makes it adapt to domestic ceramics and uses, and enriches ceramic glaze and decorates beautify life.
Summary of the invention
The deficiency that purpose of the present invention not really adapts to for the cover-coat enamel that overcomes existing furnace transmutation glaze ground coat and domestic porcelain and porcelain embryo, provide a kind of can combining to form the transmutation effect with multiple cover-coat enamel, the existing furnace transmutation glaze ground coat of energy improvement combines with cover-coat enamel, and with domestic ceramics and the good multicolor furnace transmutation glaze ground coat of art pottery blank associativity, can be fit to domestic ceramics again fully and be extensive use of, with the good multicolor furnace transmutation glaze ground coat of domestic ceramics idiosome associativity.
Another object of the present invention is to provide a kind of making method of making above-mentioned furnace transmutation glaze ground coat.
The technical solution adopted for the present invention to solve the technical problems is: a kind of multicolor furnace transmutation glaze ground coat and preparation method thereof, traditional transmutation glaze is all prepared according to cover-coat enamel of a ground-coat enamel coupling, because traditional transmutation glaze theory is thought only in this way just can bring about the desired effect.And crucial part of the present invention is exactly to wish to break through the compound method of traditional transmutation glaze, finds out a kind of multiple effect that can produce simultaneously, adapts to ground-coat enamel and its chemical constitution and the manufacture craft thereof of the common use of multiple color.
Through a large amount of repeatedly analysis of experimentss, we have found out rule wherein, and formulated technical scheme, main points are as follows: at first be to select material, avoid using the raw material that is easy to generate crystallization and phase-splitting, as zinc oxide, titanium dioxide etc., can dwindle its differentiation influence to cover-coat enamel, find out the ground-coat enamel composition rule that can adapt to multiple color, multiple reaction effect, and the starting material that are suitable for, by selection, we select feldspar, quartz, calcite, talcum, kaolin is the ground-coat enamel raw material, adds a part of color development oxide compound and gets final product.Next is that the silica alumina ratio of ground-coat enamel must be more than 6 times, and it can make the solution pyrolytic decomposition emit and form many tiny intensive gas small bubbles, form defective at the glaze laminar surface, is equipped with the cover-coat enamel that adapts again, can produce various effects.The technical recipe of the ground-coat enamel glaze that is proposed according to the method described above with the parts by weight proportioning is:
Feldspar: 45 parts of quartz: 18-25 part calcite: 12-18 part talcum powder: 2-5 part
Kaolin: 5-12 part iron oxide red: 10-14 part manganous carbonate: 2-5 part;
The chemical constitution of the ground-coat enamel that makes according to above-mentioned technical recipe is as follows:
SiO
2：58-64％ Al
2O
3：8-11％ CaO：7-9.8％ MgO：0.4-1.6％
K
2O：4-5.8％ Na
2O：0.9-1.2％ Fe
2O
3：9-13％ MnO：0.9-2.3％
From above composition as can be seen, the material of crystallizations such as oxygen-free zinc, titanium dioxide, phase-splitting class in the prescription, silicon, aluminum ratio are being equipped with calcium magnesium oxide increase gloss and solute effect again more than 6 times, be equipped with iron oxide red, manganous carbonate and form black brown background color, this basic ingredient can guarantee that solution emits gas and form many intensive small bubbles through pyrolytic decomposition, forms defective on the surface of glaze, is equipped with the cover-coat enamel that adapts again, burn till fast at 1150 ℃-1280 ℃, just can produce various transmutation effects of all kinds.
Described ground-coat enamel making method is as follows:
By the various starting material of the accurate weighing of technical recipe requirement, in starting material and ball and water input ball mill; Starting material: ball: water is strict with 1: 1.5-1.8: 0.5-0.7 carries out, with feldspar, quartz, calcite, talcum, kaolin, iron oxide red, the disposable adding ball mill of manganous carbonate, milling time is 15-18 hour, fineness is between the surplus 0.03-0.08% of 10000-hole sieve, glaze slip with ball after thin adds water and is transferred to the 43-46 degree, after 120 mesh sieves promptly become can glazing the ground-coat enamel glaze.
Ground-coat enamel glaze enameling method can soak glaze also can drench glaze, treat that ground-coat enamel dries in the shade after, spray (or drench glaze, Freehandhand-drawing) cover-coat enamel again, go into kiln after doing and burn till for 1150 ℃-1280 ℃.
The advantage of this ground-coat enamel is:
1, material therefor all is made up of raw material, and complete processing is easy, does not use high price raw materials such as titanium dioxide, zinc oxide, and is with low cost;
2, adaptive temperature a wider range (1150 ℃-1280 ℃), it is little that the high temperature viscosity of glaze varies with temperature amplitude, can effectively prevent the problem of sagging;
3, applied widely, can be used on the multiple daily and artistic porcelain base substrate, as: Shi porcelain base substrate, ceramic whiteware base substrate, greenwave etc.; Can and the cover-coat enamel combination on multiple basis, can combine with the crystal type cover-coat enamel, also can with the coventional type transparency enamel, or zirconium primary colours glaze combines its effect stability.
Embodiment
The invention will be further described below in conjunction with specific embodiment.
Embodiment one:
Embodiment one is an optimum implementation, is the ground-coat enamel scheme of a kind of suitable domestic ceramics Shi porcelain and ceramic whiteware, and concrete technical scheme is described below:
Oxygen-free zinc in the prescription, crystallizations such as titanium dioxide, phase-separable material are with feldspar, quartzy, calcite, talcum, kaolin are the ground-coat enamel raw material, silica alumina ratio is 6.1, being equipped with an amount of calcium, magnesium material increases gloss and fusion effect, is equipped with iron oxide red, manganous carbonate forms black brown background color, guarantees that solution can emit gas and form many intensive small bubbles through pyrolytic decomposition, surface at ground-coat enamel forms defective, is equipped with the cover-coat enamel that adapts again.Parts by weight proportioning with ground-coat enamel is:
Feldspar: 45 parts of quartz: 20 parts of calcites: 15 parts of talcum powder: 5 parts
Kaolin: 10 parts of iron oxide reds: 12 parts of manganous carbonates: 3 parts
The chemical ingredients of the ground-coat enamel that makes according to above-mentioned prescription is as follows:
SiO
2：61.2％ Al
2O
3：10.1％ CaO：8.23％ MgO：1.58％
K
2O：4.48％ Na
2O：0.97％ Fe
2O
3：12.1％ MnO：1.34％
Making method is as follows:
By the various starting material of the accurate weighing of technical recipe requirement, in starting material and ball and water input ball mill; Starting material: ball: water is strict to be carried out by 1: 1.6: 0.6, with feldspar, quartz, calcite, talcum, kaolin, iron oxide red, the disposable adding ball mill of manganous carbonate, milling time is 15-18 hour, fineness is between the surplus 0.03-0.08% of 10000-hole sieve, glaze slip with ball after thin adds water and is transferred to the 43-46 degree, after 120 mesh sieves can be used for the ground-coat enamel of glazing.The enameling method of ground-coat enamel can soak glaze also can drench glaze, treat that ground-coat enamel dries in the shade after, spray (or drench glaze, Freehandhand-drawing) cover-coat enamel again, go into kiln after doing and burn till for 1150 ℃-1280 ℃.
Embodiment two:
The ground-coat enamel scheme of a kind of suitable domestic ceramics Shi porcelain and ceramic whiteware, concrete technical scheme is described below:
Oxygen-free zinc in the prescription, crystallizations such as titanium dioxide, phase-separable material are with feldspar, quartzy, calcite, talcum, kaolin are the ground-coat enamel raw material, silica alumina ratio is 6.5, being equipped with an amount of calcium, magnesium material increases gloss and fusion effect, is equipped with iron oxide red, manganous carbonate forms black brown background color, guarantees that solution can emit gas and form many intensive small bubbles through pyrolytic decomposition, surface at ground-coat enamel forms defective, is equipped with the cover-coat enamel that adapts again.Parts by weight with ground-coat enamel are:
Feldspar: 45 parts of quartz: 25 parts of calcites: 12 parts of talcum powder: 5 parts
Kaolin: 8 parts of iron oxide reds: 14 parts of manganous carbonates: 2 parts
The chemical ingredients of the ground-coat enamel that makes according to above-mentioned prescription is as follows:
SiO
2：64％ Al
2O
3：9.8％ CaO：7.7％ MgO：1.58％
K
2O：4.3％ Na
2O：0.95％ Fe
2O
3：13.9％ MnO：0.92％
Making method is as follows:
By the various starting material of the accurate weighing of technology west requirement, in starting material and ball and water input ball mill; Starting material: ball: water is strict to be carried out by 1: 1.5: 0.5, with feldspar, quartz, calcite, talcum, kaolin, iron oxide red, the disposable adding ball mill of manganous carbonate, milling time is 15-18 hour, fineness is between the surplus 0.03-0.08% of 10000-hole sieve, and the glaze slip with ball after thin adds water and is transferred to the 43-46 degree, promptly can be used for glazing after 120 mesh sieves, enameling method can soak glaze also can drench glaze, after treating that ground-coat enamel dries in the shade, spray (or drenching glaze, Freehandhand-drawing) cover-coat enamel again, go into kiln after doing and burn till for 1150 ℃-1280 ℃.
Embodiment three:
The ground-coat enamel scheme of a kind of suitable domestic ceramics Shi porcelain, ceramic whiteware and greenwave, concrete technical scheme is described below:
Oxygen-free zinc in the prescription, crystallizations such as titanium dioxide, phase-separable material are with feldspar, quartzy, calcite, talcum, kaolin are the ground-coat enamel raw material, silica alumina ratio is 7, being equipped with an amount of calcium, magnesium material increases gloss and fusion effect, is equipped with iron oxide red, manganous carbonate forms black brown background color, guarantees that solution can emit gas and form many intensive small bubbles through pyrolytic decomposition, surface at ground-coat enamel forms defective, is equipped with the cover-coat enamel that adapts again.Parts by weight with ground-coat enamel are:
Feldspar: 40 parts of quartz: 28 parts of calcites: 18 parts of talcum powder: 2 parts
Kaolin: 5 parts of iron oxide reds: 10 parts of manganous carbonates: 5 parts
The chemical ingredients of the ground-coat enamel that makes according to above-mentioned prescription is as follows:
SiO
2：66.2％ Al
2O
3：9.6％ CaO：9.8％ MgO：0.55％
K
2O：4.48％ Na
2O：0.97％ Fe
2O
3：9.87％ MnO：2.4％
Making method is as follows:
By the various starting material of the accurate weighing of technology west requirement, in starting material and ball and water input ball mill; Starting material: ball: water is strict to be carried out by 1: 1.8: 0.7, with feldspar, quartz, calcite, talcum, kaolin, iron oxide red, the disposable adding ball mill of manganous carbonate, milling time is 15-18 hour, fineness is between the surplus 0.03-0.08% of 10000-hole sieve, and the glaze slip with ball after thin adds water and is transferred to the 43-46 degree, promptly can be used for glazing after 120 mesh sieves, enameling method can soak glaze also can drench glaze, after treating that ground-coat enamel dries in the shade, spray (or drenching glaze, Freehandhand-drawing) cover-coat enamel again, go into kiln after doing and burn till for 1150 ℃-1280 ℃.
The raw-material chemical ingredients of using as follows:
| Material name | SiO 2 | Al 2O 3 | Fe 2O 3 | CaO | MgO | MnO | K 2O | Na 2O | I.L |
| Feldspar | 71.33 | 15.61 | 0.19 | 0.36 | 0.23 | / | 9.52 | 2.12 | 0.61 |
| Quartzy | 98.26 | 0.58 | 0.22 | 0.28 | 0.28 | / | / | / | 0.3 |
| Calcite | 1.03 | / | 0.05 | 54.03 | 0.27 | / | / | / | 43.43 |
| Talcum | 58.29 | / | 0.09 | / | 27.69 | / | / | / | 10.37 |
| Kaolin | 70.36 | 20.11 | 0.56 | 0.05 | 0.12 | / | 0.34 | 0.23 | 7.71 |
| Iron oxide red | / | / | 98.68 | / | / | / | / | / | / |
| Manganous carbonate | / | / | / | / | / | 44.5 | / | / | 55.5 |
Claims (3)
1. multicolor furnace transmutation glaze ground coat is characterized in that: selected feldspar, and quartz, calcite, talcum, kaolin add a part of color development oxide compound; And the silica alumina ratio of ground-coat enamel must be more than 6 times, and it can make the solution pyrolytic decomposition emit gas and form many tiny intensive small bubbles, forms defective at the glaze laminar surface, is equipped with the cover-coat enamel that adapts again, can produce various transmutation effects; Do not contain crystallization, phase-separable material in the prescription, the technical recipe of ground-coat enamel glaze with the parts by weight proportioning is:
Feldspar: 45 parts of quartz: 18-25 part calcite: 12-18 part talcum powder: 2-5 part
Kaolin: 5-12 part iron oxide red: 10-14 part manganous carbonate: 2-5 part;
The chemical constitution of the ground-coat enamel that makes according to above-mentioned technical recipe is as follows:
SiO
2：58-64% Al
2O
3：8-11% CaO：7-9.8% MgO：0.4-1.6%
K
2O：4-5.8% Na
2O：0.9-1.2% Fe
2O
3：9-13% MnO：0.9-2.3%。
2. multicolor furnace transmutation glaze ground coat as claimed in claim 1 is characterized in that: the technical recipe of ground-coat enamel glaze with the parts by weight proportioning is:
Feldspar: 45 parts of quartz: 20 parts of calcites: 15 parts of talcum powder: 5 parts
Kaolin: 10 parts of iron oxide reds: 12 parts of manganous carbonates: 3 parts
The chemical ingredients of the ground-coat enamel that makes according to above-mentioned prescription is as follows:
SiO
2：61.2% Al
2O
3：10.1% CaO：8.23% MgO：1.58%
K
2O：4.48% Na
2O：0.97% Fe
2O
3：12.1% MnO：1.34%。
3. making method of multicolor furnace transmutation glaze ground coat according to claim 1, it is characterized in that: the ground-coat enamel making method is as follows:
By the various starting material of the accurate weighing of technical recipe requirement, in starting material and ball and water input ball mill; Starting material: ball: the strict 1:1.5-1.8:0.5-0.7 that presses of water carries out, with feldspar, quartz, calcite, talcum, kaolin, iron oxide red, the disposable adding ball mill of manganous carbonate, milling time is 15-18 hour, fineness is between the surplus 0.03-0.08% of 10000-hole sieve, glaze slip with ball after thin adds water and is transferred to the 43-46 degree, after 120 mesh sieves promptly become can glazing the ground-coat enamel glaze.
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| JP4787112B2 (en) * | 2006-04-12 | 2011-10-05 | 宮脇グレイズ工業株式会社 | Glaze for incoming ceramics, incoming ceramic products and methods for producing the products |
| CN100455549C (en) * | 2007-06-14 | 2009-01-28 | 湖南华联瓷业股份有限公司 | Medium and high temperature sintered coarse crystalline Fe-Ti glaze and its prepn process |
| CN101348329B (en) * | 2008-08-22 | 2011-05-18 | 福建省佳美集团公司 | Manufacturing process of furnace transmutation enamel |
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