CN101891539B - Water hyacinth biogas slurry-based plant source foliar insecticide-fertilizer, preparation method and application - Google Patents
Water hyacinth biogas slurry-based plant source foliar insecticide-fertilizer, preparation method and application Download PDFInfo
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- CN101891539B CN101891539B CN2010102211776A CN201010221177A CN101891539B CN 101891539 B CN101891539 B CN 101891539B CN 2010102211776 A CN2010102211776 A CN 2010102211776A CN 201010221177 A CN201010221177 A CN 201010221177A CN 101891539 B CN101891539 B CN 101891539B
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Abstract
The invention discloses a water hyacinth biogas slurry-based plant source foliar insecticide-fertilizer. The plant source foliar insecticide-fertilizer comprises the following components in percentage by weight: 0.1 to 1 percent of eugenol, 0.5 to 3 percent of water hyacinth biogas slurry, 0.1 to 1 percent of absolute ethanol and the balance of water. The invention also discloses a preparation method and the application of the plant source foliar insecticide-fertilizer. The water hyacinth biogas slurry-based plant source foliar insecticide-fertilizer of the invention has an active ingredient which is derived from a plant or an extract thereof with an insecticidal function and a nutritional ingredient which is derived from industrial, agricultural and animal husbandry production waste treated by innocuous technology, has effects of prompting plant growth and development, increasing production and yield, improving quality, improving nutrient utilization rate, preventing and controlling injurious insects, non-pollution and the like, and is suitable for non-polluted, green and organic agriculture product production. The foliar insecticide-fertilizer has the characteristics of remarkable application effect, easily-obtained raw materials, simple production process, great market potential, obvious economic benefit and social benefit, and very board application prospect.
Description
Technical field
The invention belongs to field of agricultural production technologies, be specifically related to a kind of plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry and preparation method thereof and working method.
Background technology
For a long time, China still is in a kind of " embarrassment " position as " agricultural chemicals big country ", promptly produce and the riskiest pesticide that uses far above world average level, eco-friendly biological pesticide is corresponding to world average level.Because it is chemical pesticide that China is used to prevent and treat the agricultural chemicals of corps diseases mostly extremely; Yet the life-time service chemical pesticide causes a series of adverse consequencess; Mainly show several respects: the one, ecotope constantly worsens; Chemical pesticide not only has restraining effect to disease, has also destroyed the natural eubiosis simultaneously; The 2nd, the life-time service chemical pesticide makes disease produce resistance, thereby has increased the amount of application and the access times of agricultural chemicals; The 3rd, because a large amount of uses of chemical pesticide cause agricultural chemicals accumulation gradually in environment, produced the pesticidal contamination environmental problem, especially soil quality constantly reduces, and has reduced the sustainable use ability of soil; The 4th, the poisoning of the residual initiation of chemical pesticide happens occasionally, because of most of chemical pesticide residual period, is longer, agricultural-food particularly vegetables, melon and fruit be vulnerable to severe contamination, people's the healthy potential threat that just exists.Simultaneously because for a long time to the too dependence of chemical fertilizer, excessive use, thereby produced the series of negative influence: the one, using of a large amount of chemical fertilizer descends soil quality, the soil salinization, harden, phenomenon such as acidifying occurs; The 2nd, uneven fertilising causes soil nutrient unbalance, and crop physiological disease takes place, and from malicious product accumulation aggravation, soil microflora is unbalance; The 3rd, quality of agricultural product constantly descends; The 4th, superfluous nutrient gets into water body and has increased the weight of body eutrophication.
The Phytophthora capsici disease is a kind of worldwide soil-borne disease, has a strong impact on the agriculture prodn of China and countries in the world, causes enormous economic loss.Medicine through processing after the improvement of vegetable source natural compound is fertile, to fruit, flower, the Ye Douwu harm of plant, to the person poultry safety, has efficient noresidue, no poisoning, advantages such as the non-resistant property of medicine on the one hand; Owing to nutritive element balance in the medicine fertilizer, can effectively reduce the usage quantity of chemical fertilizer on the other hand; The 3rd, in the control disease, can effectively improve quality of agricultural product.Therefore, manage to take effective technical measures, develop out the focus that environmentally friendly medicine fertilizer just becomes research of agricultural science.
Summary of the invention
Technical problem to be solved by this invention provides a kind of plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry, and this medicine fertilizer is that the friendly medicine of many effects novel environmental that a kind ofly integrates antibiotic, nutrition, improves quality is fertile.
The technical problem that the present invention also will solve provides the preparation method of above-mentioned plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry.
The technical problem that the present invention will solve at last provides the fertile application of above-mentioned medicine.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is following:
A kind of plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry, it comprises the component of following weight percentage: Eugenol 0.1～1%, water hyacinth biogas slurry 0.5～3%, absolute ethyl alcohol 0.1～1%, all the other are water.
Wherein, Described water hyacinth biogas slurry prepares as follows and gets: after Herba Eichhorniae is pulverized, add 0.5～2 times water of Herba Eichhorniae weight, adopt anaerobic activated sludge or existing water hyacinth biogas slurry to carry out microbial inoculant; Inoculum size is 10～40% (v/v); 25～50 ℃ of bottom fermentations 10～15 days, extract natural pond liquid, promptly get through removing by filter solid impurity.
The preparation method of above-mentioned plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry adds water hyacinth biogas slurry in the entry earlier and mixes, and adds in the above-mentioned mixing solutions after then Eugenol being dissolved in absolute ethyl alcohol again.
The above-mentioned application of plant source foliar insecticide-fertilizer in promoting plant growth based on water hyacinth biogas slurry.
Wherein, described crop is capsicum, summer squash, cucumber, eggplant, tomato or green vegetables.
The above-mentioned application of plant source foliar insecticide-fertilizer in control crop Phytophthora capsici disease based on water hyacinth biogas slurry.
Wherein, described crop is capsicum, summer squash, cucumber, eggplant, tomato, watermelon, pumpkin or yam.
Beneficial effect: its effective component of plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry of the present invention derives from plant or its extract with insecticidal function; Waste is produced in industrial or agricultural, livestock industry that nutritive ingredient derives from after innoxious technical finesse; Have promote crop growth, increasing both production and income, improve quality, improve plant recovery of nutrient, pest control, multi-efficiency such as pollution-free, be applicable to nuisanceless, green and organic farm products production.This Pesticidal foliage fertilizer effect significantly, starting material are easy to get, and production technique is simple, market potential is big, economic benefit and social benefit are obvious, has the wide application prospect of ten minutes.
Embodiment
According to following embodiment, can understand the present invention better.Yet, those skilled in the art will readily understand that the described concrete material proportion of embodiment, processing condition and result thereof only are used to explain the present invention, and the present invention that should also can not limit in claims to be described in detail.
Embodiment 1:
The preparation of water hyacinth biogas slurry:
After Herba Eichhorniae pulverized, add 1.2 times water of Herba Eichhorniae weight, adopt anaerobic activated sludge to carry out microbial inoculant, inoculum size is 15% (v/v), 30 ℃ of bottom fermentations 10 days, extracts natural pond liquid, promptly gets through removing by filter solid impurity.Wherein contain following component by mass percent: NH in the liquid of natural pond
4 +0.038%, NO
3 -0.037%, P
2O
50.022%, K
2O0.152%, amino acid 0.252%, organic matter 0.209%, water cut 99.29%.
The component that comprises following weight percentage based on the plant source foliar insecticide-fertilizer of water hyacinth biogas slurry: Eugenol 0.3%, water hyacinth biogas slurry 1.5%, absolute ethyl alcohol 0.44%, all the other are water.
Preparing method based on the plant source foliar insecticide-fertilizer of water hyacinth biogas slurry: the water hyacinth biogas slurry of formula ratio is added in the entry mix earlier, Eugenol is dissolved in adds again behind the absolute ethyl alcohol in the above-mentioned mixing solutions (promptly dilute water hyacinth biogas slurry) then.
Embodiment 2:
With the method for embodiment 1, the prescription of the plant source foliar insecticide-fertilizer of different are based on water hyacinth biogas slurry is different, and it comprises the component of following weight percentage: Eugenol 1%, and water hyacinth biogas slurry 3%, absolute ethyl alcohol 1%, all the other are water.
Embodiment 3:
With the method for embodiment 1, the prescription of the plant source foliar insecticide-fertilizer of different are based on water hyacinth biogas slurry is different, and it comprises the component of following weight percentage: Eugenol 0.1%, and water hyacinth biogas slurry 0.5%, absolute ethyl alcohol 0.1%, all the other are water.
Embodiment 4: based on the plant source foliar insecticide-fertilizer of water hyacinth biogas slurry to the promotion of plant growth with to the improvement effect of quality.
Formula I: 1.5% (w/w) water hyacinth biogas slurry (water hyacinth biogas slurry that makes by embodiment 1 method), 98.5% (w/w) water.
Formula I I:0.3% (w/w) Eugenol, absolute ethyl alcohol 0.4%, 99.3% (w/w) water.
The biological Pesticidal foliage fertilizer prescription of the plant-sourced of formula I II: embodiment 1.
Seed is with the H of 0.3% (w/w)
2O
2After the sterilization, clean, select the petridish (diameter 15cm) that homogeneous, the normal seed of form place shop 3 metafiltration paper then, train seedling with zero(ppm) water.5d after waiting to emerge chooses the consistent material of growing way it is transferred in the plastic tub alms bowl, behind the seedling age 20d, sprays with containing different treatment liquid respectively, and each handles repetition 3 times.Treatment solution is every to spray once at a distance from 5d, samples behind the 60d, measures and respectively handles green vegetables relevant physiological biochemical indicator.(annotate: contrast CK is a clear water)
Measuring method
Fresh weight is measured: after the off-test, every basin is the consistent seedling of 3 upgrowth situations of picking at random, measures its fresh weight with the clean back of blotting of deionized water then.
Protein content determination: close generation method with reference to Lee, adopt the Xylene Brilliant Cyanine G method.(Li Hesheng. plant physiology and biochemistry experimental principle and technology. Beijing Higher Education Publishing House, 2000)
Nitrate content is measured: with reference to methods such as Lu Qiming, measure and adopt ultraviolet spectrophotometry.(Lu Qiming, Chen Min, Liao Zongwen. the improvement of determined by ultraviolet spectrophotometry nitrate nitrogen on vegetables. Agricultural University Of South China's journal, 1997,8 (4): 104-106.)
Vc measures: with reference to high friend's method, get about testing sample 2g, add a small amount of 2% hydrochloric acid, in tissue mashing machine, process homogenate; Move in the 100mL volumetric flask, to scale, absorbent cotton filters with 1% oxalic acid constant volume; Get 10mL filtrating, with the 2,6 dichlorophenol indophenol solution titration determination Vc content of having demarcated.(high friend. the agrochemistry common analysis. Xi'an: Shaanxi science tech publishing house, 1980.)
Soluble sugar is measured: with reference to the Zou Qi method, adopt the anthrone colourimetry.(Zou Qi. plant physiology experiment instructs. Beijing: Chinese agriculture press, 2000.)
Table 1 different treatment is to the influence of green vegetables, capsicum, cucumber, tomato living weight and quality
Can be known that by table 1 green vegetables are handled back fresh weight, protein contnt, Vc content and soluble sugar in formula I and compared respectively according to having increased by 15.6%, 45.1%, 39.9% and 14.1%, the nitrate content comparison is according to reducing 11.8%; Formula I I handles back green vegetables fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 6.3%, 32.9%, 19.8% and 5.1%, and the nitrate content comparison is according to reducing 2.2%; Formula I II handles back fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 31.2%, 59.8%, 52.3% and 20.5%, and the nitrate content comparison is according to reducing 17.3%.
Capsicum is handled back fresh weight, protein contnt, Vc content and soluble sugar in formula I and compares respectively according to having increased by 43.2%, 12.0%, 44.9% and 46.6%, and the nitrate content comparison is according to reducing 22.5%; Formula I I handles back green vegetables fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 18.3%, 7.5%, 9.7% and 17.9%, and the nitrate content comparison is according to reducing 7.8%; Formula I II handles back fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 65.9%, 20.7%, 60.8% and 72.0%, and the nitrate content comparison is according to reducing 27%.
Cucumber is handled back fresh weight, protein contnt, Vc content and soluble sugar in formula I and compares respectively according to having increased by 24.2%, 25.5%, 39.4% and 28.2%, and the nitrate content comparison is according to reducing 23.7%; Formula I I handles back green vegetables fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 11.0%, 19.3%, 32.7% and 15.2%, and the nitrate content comparison is according to reducing 13.0%; Formula I II handles back fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 37.6%, 39.2%, 47.3% and 36.4%, and the nitrate content comparison is according to reducing 53.9%.
Tomato is handled back fresh weight, protein contnt, Vc content and soluble sugar in formula I and compares respectively according to having increased by 9.0%, 13.9%, 44.4% and 22.6%, and the nitrate content comparison is according to reducing 10.5%; Formula I I handles back green vegetables fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 1.9%, 2.9%, 18.1% and 8.3%, and the nitrate content comparison is according to reducing 2.4%; Formula I II handles back fresh weight, protein contnt, Vc content and soluble sugar and compares respectively according to having increased by 14.3%, 19.3%, 64.2% and 35.2%, and the nitrate content comparison is according to reducing 16.3%.
Can know on having, with formula I II handle to green vegetables, capsicum, cucumber and tomato living weight and quality to improve effect best.
Embodiment 5: based on the plant source foliar insecticide-fertilizer of water hyacinth biogas slurry at the preventive and therapeutic effect sick to the crop Phytophthora capsici.
Formula I: 1.5% (w/w) water hyacinth biogas slurry (water hyacinth biogas slurry that makes by embodiment 1 method), 98.5% (w/w) water.
Formula I I:0.3% (w/w) Eugenol, absolute ethyl alcohol 0.4%, 99.3% (w/w) water.
The biological Pesticidal foliage fertilizer prescription of the plant-sourced of formula I II: embodiment 1.
Seed is with the H of 0.3% (w/w)
2O
2After the sterilization, clean, select the petridish (diameter 15cm) that homogeneous, the normal seed of form place shop 3 metafiltration paper then, train seedling with zero(ppm) water.5d after waiting to emerge chooses the consistent material of growing way it is transferred in the plastic tub alms bowl, and behind the seedling age 20d, inoculation sprays with containing different treatment liquid respectively, and each handles repetition 3 times.Treatment solution is every to spray once at a distance from 5d, samples after company sprays 2 times.(annotate: contrast CK is a clear water)
Measuring method
The mensuration of disease index and control effect: with reference to Dou Rui flitch method.(Dou Rui wood .3 plants endogenetic bacterium is to the control effect of graw mold of tomato. the Henan agricultural sciences, and 2010,4:77-79.)
Can know that by table 2 on capsicum, formula I is 28.09% to the preventive effect of Phytophthora capsici; Formula I I is 47.59% to the preventive effect of Phytophthora capsici; Formula I II is 72.16% to the preventive effect of Phytophthora capsici.
As far as cucumber, formula I is 25.82% to the preventive effect of Phytophthora capsici; Formula I I is 40.83% to the preventive effect of Phytophthora capsici; Formula I II is 65.30% to the preventive effect of Phytophthora capsici.
As far as tomato, formula I is 24.02% to the preventive effect of Phytophthora capsici; Formula I I is 43.83% to the preventive effect of Phytophthora capsici; Formula I II is 67.55% to the preventive effect of Phytophthora capsici.
By on can know, handle best to the control effect of Phytophthora capsici on capsicum, cucumber and the tomato with formula I II.
Table 2 different treatment is to Phytophthora capsici control effect on capsicum, cucumber, the tomato
Claims (7)
1. plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry is characterized in that it is made up of the component of following weight percentage: Eugenol 0.1～1%, and water hyacinth biogas slurry 0.5～3%, absolute ethyl alcohol 0.1～1%, all the other are water.
2. the plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry according to claim 1; It is characterized in that described water hyacinth biogas slurry prepares as follows and gets: after Herba Eichhorniae is pulverized, add 0.5～2 times water of Herba Eichhorniae weight, adopt anaerobic activated sludge or existing water hyacinth biogas slurry to carry out microbial inoculant; Inoculum size is 10～40% (v/v); 25～50 ℃ of bottom fermentations 10～15 days, extract natural pond liquid, promptly get through removing by filter solid impurity.
3. the preparation method of the described plant source foliar insecticide-fertilizer based on water hyacinth biogas slurry of claim 1 is characterized in that earlier water hyacinth biogas slurry being added in the entry mixing, and adds in the above-mentioned mixing solutions after then Eugenol being dissolved in absolute ethyl alcohol again.
4. the described application of plant source foliar insecticide-fertilizer in promoting plant growth of claim 1 based on water hyacinth biogas slurry.
5. application according to claim 4 is characterized in that described crop is capsicum, summer squash, cucumber, eggplant, tomato or green vegetables.
6. the described application of plant source foliar insecticide-fertilizer in control crop Phytophthora capsici disease of claim 1 based on water hyacinth biogas slurry.
7. application according to claim 6 is characterized in that described crop is capsicum, summer squash, cucumber, eggplant, tomato, watermelon, pumpkin or yam.
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| CN108513897A (en) * | 2018-03-25 | 2018-09-11 | 卓小玲 | A kind of aquaculture method of epipremnum aureum |
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| CN108450259A (en) * | 2018-06-07 | 2018-08-28 | 和县海豪蔬菜种植有限责任公司 | A kind of implantation methods of high yield high nutrition green vegetables |
| CN113912461A (en) * | 2021-11-18 | 2022-01-11 | 海南大学 | Foliar fertilizer for resisting plant leaf fungal diseases |
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| JPWO2004100660A1 (en) * | 2003-05-13 | 2006-07-13 | 出光興産株式会社 | Antibacterial and antiviral composition |
| CN100488359C (en) * | 2007-04-26 | 2009-05-20 | 江苏省农业科学院 | Eugenol micro-emulsion |
| CN101275150A (en) * | 2008-05-13 | 2008-10-01 | 江苏省农业科学院 | Fermentation method for changing methane into resource by using water hyacinth and application of product produced thereby |
| CN101423424B (en) * | 2008-11-14 | 2010-08-11 | 庄明儒 | Liquid bacterial manure production technique by comprehensive utilization of marsh liquid and method thereof |
| CN101627756A (en) * | 2009-06-25 | 2010-01-20 | 江苏省农业科学院 | Application of eugenol in preparing pesticide preventing and treating crop virosis |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108513897A (en) * | 2018-03-25 | 2018-09-11 | 卓小玲 | A kind of aquaculture method of epipremnum aureum |
| CN108513897B (en) * | 2018-03-25 | 2020-12-15 | 浙江鼎兴企业管理有限公司 | Underwater cultivation method of scindapsus aureus |
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