CN101836659A - Compound potassium hydrogen persulfate disinfectant - Google Patents
Compound potassium hydrogen persulfate disinfectant Download PDFInfo
- Publication number
- CN101836659A CN101836659A CN 201010144652 CN201010144652A CN101836659A CN 101836659 A CN101836659 A CN 101836659A CN 201010144652 CN201010144652 CN 201010144652 CN 201010144652 A CN201010144652 A CN 201010144652A CN 101836659 A CN101836659 A CN 101836659A
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- potassium hydrogen
- hydrogen persulfate
- disinfectant
- compound potassium
- major ingredient
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Abstract
The invention relates to a compound potassium hydrogen persulfate disinfectant prepared from main materials and auxiliary materials, wherein the main materials comprise potassium hydrogen persulfate, citric acid, aminosulfuric acid, sodium chloride, sodium citrate and the like; the auxiliary materials comprise film coating materials, hydroxylpropyl cellulose, hydroxypropyl methyl cellulose, polyvinylpyrrolidone, soluble starch, ethyl cellulose and the like; and the weight ratio of the auxiliary materials to the main materials is 0-0.15:1. Because the prescription of the compound potassium hydrogen persulfate disinfectant is optimized, the compound potassium hydrogen persulfate disinfectant solves the problems of strong irritation, easy moisture absorption, poor stability, short action time and the like, and because P-containing components are not used in the prescription, the compound potassium hydrogen persulfate disinfectant is beneficial to environmental protection.
Description
Technical field
The present invention relates to disinfectant, particularly a kind of compound potassium hydrogen persulfate disinfectant.
Background technology
Set up reasonable eqpidemic disease control system, take measures such as decontamination, sterilization, isolation, purification, quarantine and desinsection respectively at social environment, people, animal fowl, four aspects of material.Wherein, sterilization is particularly crucial, along with the notion of improving feeding environment is promoted gradually, the exploitation of animal sterile products more and more is subject to people's attention, in recent years, the compound potassium hydrogen persulfate disinfectant exploitation, and some patents have appearred, from the patent of having announced, the main not enough performance of issued patents product is as follows:
1. production technology falls behind.
2. the product excitant is strong, and is bigger to production, user and mucous membrane of animal excitant.
3. the easy moisture absorption of product, poor stability.
4. product is short action time.
5. use in the product prescription to contain the P composition, product produces irritative gas, causes environmental pollution.
Summary of the invention
The object of the present invention is to provide a kind of compound potassium hydrogen persulfate disinfectant of high reliability.
The objective of the invention is to realize: a kind of compound potassium hydrogen persulfate disinfectant by following approach, it is made of major ingredient and auxiliary material, major ingredient by weight percentage, the proportioning of its component is potassium hydrogen persulfate 40-60%, citric acid 10-20%, dithiocarbamic acid 5-15%, sodium chloride 1-5%, sodium citrate 1-5%, sodium alkyl benzene sulfonate 5-20%, sodium alkyl sulfate 1-5%;
Auxiliary material by weight percentage, the proportioning of its component is film-coating material 1-8%, L-HPC 1-2%, hydroxypropyl methylcellulose 2-5%, polyvinylpyrrolidone 1-2%, soluble starch 2-5%, ethyl cellulose 1-5%, polyethylene glycol 0.003-0.01%, Tween 80 0.003-0.01%, ethanol 40-85%;
By weight, above-mentioned auxiliary material is 0～0.15: 1 than major ingredient.
On the basis of above-mentioned prescription, optimum proportion scheme is, compound potassium hydrogen persulfate disinfectant is made of major ingredient and auxiliary material, major ingredient by weight percentage, the proportioning of its component is potassium hydrogen persulfate 58%, citric acid 12%, dithiocarbamic acid 8%, sodium chloride 3%, sodium citrate 2%, sodium alkyl benzene sulfonate 15%, sodium alkyl sulfate 2%;
Auxiliary material by weight percentage, the proportioning of its component is film-coating material 8%, L-HPC 1%, hydroxypropyl methylcellulose 2.5%, polyvinylpyrrolidone 1%, soluble starch 2%, ethyl cellulose 4%, polyethylene glycol 0.008%, Tween 80 0.003%, ethanol 81.489%;
By weight, above-mentioned auxiliary material is 0.06: 1 with the major ingredient ratio.
Compound potassium hydrogen persulfate disinfectant of the present invention is optimized prescription, and production technology is upgraded.Production technology application of advanced film-coating technique and slow release method, it is strong to have solved the product excitant, the easy moisture absorption of product, poor stability, problems such as product weak point action time are used in the product prescription to contain the P composition, are beneficial to environmental protection.
Embodiment
Compound potassium hydrogen persulfate disinfectant of the present invention, it is made of major ingredient and auxiliary material, major ingredient by weight percentage, the proportioning of its component is potassium hydrogen persulfate 40-60%, citric acid 10-20%, dithiocarbamic acid 5-15%, sodium chloride 1-5%, sodium citrate 1-5%, sodium alkyl benzene sulfonate 5-20%, sodium alkyl sulfate 1-5%;
Auxiliary material by weight percentage, the proportioning of its component is film-coating material 1-8%, L-HPC 1-2%, hydroxypropyl methylcellulose 2-5%, polyvinylpyrrolidone 1-2%, soluble starch 2-5%, ethyl cellulose 1-5%, polyethylene glycol 0.003-0.01%, Tween 80 0.003-0.01%, ethanol 40-85%;
By weight, above-mentioned auxiliary material is 0～0.15: 1 than major ingredient.
In the above-mentioned prescription, potassium hydrogen persulfate is an oxidant, in the sodium chloride available chlorine and chloride-ion source, dithiocarbamic acid is an acidulant, it is right that citric acid and sodium citrate form buffering, sodium alkyl benzene sulfonate, sodium alkyl sulfate is a surfactant, the film-coating material is a mask agent, make the potassium hydrogen persulfate Disinfection Effect strengthen greatly after the said components combination, single potassium hydrogen persulfate has only the oxidation sterilizing effect, the generation of combination back available chlorine has increased halogen bunch Disinfection Effect, changed the bacteria live environment and played the cinic acid effect, citric acid and sodium citrate form buffering to playing stable acidic environmental activity, sodium alkyl benzene sulfonate, sodium alkyl sulfate is a complexed surfactant, and detergency is stronger.
Embodiment: compound potassium hydrogen persulfate disinfectant is made of major ingredient and auxiliary material, major ingredient by weight percentage, the proportioning of its component is potassium hydrogen persulfate 58%, citric acid 12%, dithiocarbamic acid 8%, sodium chloride 3%, sodium citrate 2%, sodium alkyl benzene sulfonate 15%, sodium alkyl sulfate 2%;
Auxiliary material by weight percentage, the proportioning of its component is film-coating material 8%, L-HPC 1%, hydroxypropyl methylcellulose 2.5%, polyvinylpyrrolidone 1%, soluble starch 2%, ethyl cellulose 4%, polyethylene glycol 0.008%, Tween 80 0.003%, ethanol 81.489%;
By weight, above-mentioned auxiliary material is 0.06: 1 with the major ingredient ratio.
The preparation technology of compound potassium hydrogen persulfate disinfectant
1. sodium chloride and auxiliary material are made slow-releasing granules, and the bag film-coating.
2. Main Ingredients and Appearance wraps film-coating together or wraps film-coating respectively.
3. accurately taking by weighing behind each dressing material by prescription puts in the mixer and mixes packing.
The using method of compound potassium hydrogen persulfate disinfectant: soak, spray
1. animal house environment, drinking equipment and 1: 200 concentration dilution of air sterillization.
2. terminal disinfection, equipment disinfection, hatchery sterilization, 1: 200 concentration dilution of foot washing basin sterilization.
3. 1: 1000 concentration dilution of drinking water disinfection.
4. aquiculture animal, water 1: 300-500 is complete, and evenly spray in the pond.Treatment: per 1 cubic metre of water restrains with this product 0.1-0.18, and 3 days once, and prevention: 15 days once.
Effect
1) bactericidal effect:
A. kill bacterium (virus) experiment:
| Test organisms | Concentration | The result |
| Escherichia coli | ??1∶400 | Kill |
| Staphylococcus aureus | ??1∶400 | Kill |
| Test organisms | Concentration | The result |
| Streptococcus | ??1∶800 | Kill |
| Bird flu | ??1∶1600 | Kill |
| Aftosa | ??1∶1000 | Kill |
| Pig vesicle disease | ??1∶400 | Kill |
| The bursa of farbricius | ??1∶400 | Kill |
B. air ambient, water body disinfection test:
A, air ambient: with φ 90 aseptic plates, inject about 20ml nutrient agar, solidify, expose the 30min sampling, cover aseptic plate, put 33 ± 1 ℃ of inversions of biochemical incubator and cultivate 48 hours countings respectively at 0.8m place before and after the sterilization.Do negative control simultaneously.
B, water body: respectively at sterilization back sampling 1ml, be diluted to 1: 10 with aseptic sodium chloride-peptone buffer agent, 1: 100,1: 1000 (being diluted to 1: 100 with aseptic sodium chloride-peptone buffer agent before the sterilization, 1: 10000,1: 1000000) waited and diluted grade injection φ 90 aseptic plates, inject about 20ml nutrient agar, solidify, cover aseptic plate, put 33 ± 1 ℃ of biochemical incubators and be inverted 48 hours countings of cultivation.Do negative control simultaneously.
The laboratory reference document:
A. State Standard of the People's Republic of China's " sterilization with sterilization effect evaluation method and standard ", Ministry of Public Health's promulgation.
B. " People's Republic of China's veterinary drug allusion quotation version in 2005 ", Ministry of Agriculture's promulgation.
C. " People's Republic of China's import veterinary drug standard ", Ministry of Agriculture's promulgation.
2) technical advance
New technology and old technology comparative analysis
| Project | The invention new technology | Old technology |
| Preparation technology's method | Partial elements is made dressing behind the slow-releasing granules, mix again; Avoided storeroom directly to contact and the generation chemical reaction, | With mixing of materials; Storeroom directly contacts and chemical reaction takes place. |
| Project | The invention new technology | Old technology |
| Constant product quality | Product is difficult for the moisture absorption, constant product quality. | The easy moisture absorption of product, unstable product quality. |
| The product excitant | Nonirritant almost before the molten water does not have injury to production, user and animal. | Excitant is bigger before the molten water.Mucous membrane injury to production, user and animal is bigger, causes upper respiratory disease easily. |
| Prescription relatively | There is not phosphorous composition. | Phosphorous composition is arranged. |
| Environmental protection | Avoid taking place chemical reaction, promptly prevent the chlorine discharging.No phosphorous composition is beneficial to environmental protection in the composition. | The inevitable chemical reaction that takes place promptly has a large amount of chlorine dischargings.Phosphorous composition is arranged, all unfavorable environmental protection in the composition. |
Claims (2)
1. compound potassium hydrogen persulfate disinfectant, it is characterized in that: it is made of major ingredient and auxiliary material, major ingredient by weight percentage, the proportioning of its component is potassium hydrogen persulfate 40-60%, citric acid 10-20%, dithiocarbamic acid 5-15%, sodium chloride 1-5%, sodium citrate 1-5%, sodium alkyl benzene sulfonate 5-20%, sodium alkyl sulfate 1-5%;
Auxiliary material by weight percentage, the proportioning of its component is film-coating material 1-8%, L-HPC 1-2%, hydroxypropyl methylcellulose 2-5%, polyvinylpyrrolidone 1-2%, soluble starch 2-5%, ethyl cellulose 1-5%, polyethylene glycol 0.003-0.01%, Tween 80 0.003-0.01%, ethanol 40-85%;
By weight, above-mentioned auxiliary material is 0～0.15: 1 than major ingredient.
2. compound potassium hydrogen persulfate disinfectant as claimed in claim 1, it is characterized in that: it is made of major ingredient and auxiliary material, major ingredient by weight percentage, the proportioning of its component is potassium hydrogen persulfate 58%, citric acid 12%, dithiocarbamic acid 8%, sodium chloride 3%, sodium citrate 2%, sodium alkyl benzene sulfonate 15%, sodium alkyl sulfate 2%;
Auxiliary material by weight percentage, the proportioning of its component is film-coating material 8%, L-HPC 1%, hydroxypropyl methylcellulose 2.5%, polyvinylpyrrolidone 1%, soluble starch 2%, ethyl cellulose 4%, polyethylene glycol 0.008%, Tween 80 0.003%, ethanol 81.489%;
By weight, above-mentioned auxiliary material is 0.06: 1 with the major ingredient ratio.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010144652 CN101836659A (en) | 2010-04-12 | 2010-04-12 | Compound potassium hydrogen persulfate disinfectant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201010144652 CN101836659A (en) | 2010-04-12 | 2010-04-12 | Compound potassium hydrogen persulfate disinfectant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101836659A true CN101836659A (en) | 2010-09-22 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201010144652 Pending CN101836659A (en) | 2010-04-12 | 2010-04-12 | Compound potassium hydrogen persulfate disinfectant |
Country Status (1)
| Country | Link |
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Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102265904A (en) * | 2011-06-03 | 2011-12-07 | 宋海鹏 | Compound potassium hydrogen persulfate disinfectant and manufacturing process thereof |
| CN103891767A (en) * | 2012-12-31 | 2014-07-02 | 青岛锦涟鑫商贸有限公司 | Bleaching disinfectant |
| CN104719336A (en) * | 2015-02-02 | 2015-06-24 | 山东威高药业股份有限公司 | Low-corrosion potassium peroxymonosulfate disinfector |
| CN106937632A (en) * | 2017-05-11 | 2017-07-11 | 江苏苏沃尚新材料科技有限公司 | A kind of swimming pool long-acting fungicide |
| CN106942271A (en) * | 2017-04-25 | 2017-07-14 | 清远海贝生物技术有限公司 | A kind of compound potassium hydrogen persulfate disinfectant and preparation method thereof |
| CN106973939A (en) * | 2017-05-11 | 2017-07-25 | 江苏苏沃尚新材料科技有限公司 | A kind of monopersulfate hydrogen potassium composite disinfectant |
| CN107758829A (en) * | 2017-11-16 | 2018-03-06 | 刘黛 | A kind of space station urine pretreating agent, it is prepared and the preprocess method of urine |
| CN109319913A (en) * | 2018-10-11 | 2019-02-12 | 仲恺农业工程学院 | A kind of slow-release oxone and preparation method thereof |
| CN110498499A (en) * | 2019-08-01 | 2019-11-26 | 同济大学 | A kind of disinfectant reducing Disinfection Byproducts in Drinking Water concentration |
| CN110839622A (en) * | 2019-11-01 | 2020-02-28 | 仲恺农业工程学院 | Potassium hydrogen persulfate sustained-release agent and preparation method and application thereof |
| CN112430508A (en) * | 2020-12-09 | 2021-03-02 | 淄博鑫欧瑞环保科技有限公司 | Disinfectant powder atomizing device cleaning agent, application and cleaning method thereof |
| CN113367155A (en) * | 2021-05-18 | 2021-09-10 | 武汉科缘生物发展有限责任公司 | Potassium hydrogen persulfate compound disinfectant and application thereof |
| CN113994973A (en) * | 2021-11-05 | 2022-02-01 | 开封恩科生物科技有限公司 | Potassium monopersulfate microencapsulated compound disinfectant and production process thereof |
| CN116267919A (en) * | 2023-03-26 | 2023-06-23 | 广州叁个圆消毒技术有限公司 | Potassium hydrogen persulfate compound powder and preparation method thereof |
| WO2023219867A1 (en) * | 2022-05-11 | 2023-11-16 | Arxada Ag | Single dose disinfectant |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1545883A (en) * | 2003-12-15 | 2004-11-17 | 韶山大北农动物药业有限公司 | Water soluble composite potassium monopersulfate powder disinfectant |
| CN101049107A (en) * | 2006-07-11 | 2007-10-10 | 成都润兴消毒药业有限公司 | Sterilization powder, and preparation method. |
-
2010
- 2010-04-12 CN CN 201010144652 patent/CN101836659A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1545883A (en) * | 2003-12-15 | 2004-11-17 | 韶山大北农动物药业有限公司 | Water soluble composite potassium monopersulfate powder disinfectant |
| CN101049107A (en) * | 2006-07-11 | 2007-10-10 | 成都润兴消毒药业有限公司 | Sterilization powder, and preparation method. |
Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102265904B (en) * | 2011-06-03 | 2015-01-07 | 宋海鹏 | Compound potassium hydrogen persulfate disinfectant and manufacturing process thereof |
| CN102265904A (en) * | 2011-06-03 | 2011-12-07 | 宋海鹏 | Compound potassium hydrogen persulfate disinfectant and manufacturing process thereof |
| CN103891767A (en) * | 2012-12-31 | 2014-07-02 | 青岛锦涟鑫商贸有限公司 | Bleaching disinfectant |
| CN104719336A (en) * | 2015-02-02 | 2015-06-24 | 山东威高药业股份有限公司 | Low-corrosion potassium peroxymonosulfate disinfector |
| CN106942271B (en) * | 2017-04-25 | 2018-09-18 | 石家庄卫科生物科技有限公司 | A kind of compound potassium hydrogen persulfate disinfectant and preparation method thereof |
| CN106942271A (en) * | 2017-04-25 | 2017-07-14 | 清远海贝生物技术有限公司 | A kind of compound potassium hydrogen persulfate disinfectant and preparation method thereof |
| CN106937632A (en) * | 2017-05-11 | 2017-07-11 | 江苏苏沃尚新材料科技有限公司 | A kind of swimming pool long-acting fungicide |
| CN106973939A (en) * | 2017-05-11 | 2017-07-25 | 江苏苏沃尚新材料科技有限公司 | A kind of monopersulfate hydrogen potassium composite disinfectant |
| CN107758829A (en) * | 2017-11-16 | 2018-03-06 | 刘黛 | A kind of space station urine pretreating agent, it is prepared and the preprocess method of urine |
| CN109319913A (en) * | 2018-10-11 | 2019-02-12 | 仲恺农业工程学院 | A kind of slow-release oxone and preparation method thereof |
| CN109319913B (en) * | 2018-10-11 | 2022-07-01 | 仲恺农业工程学院 | Slow-release potassium hydrogen persulfate preparation and preparation method thereof |
| CN110498499A (en) * | 2019-08-01 | 2019-11-26 | 同济大学 | A kind of disinfectant reducing Disinfection Byproducts in Drinking Water concentration |
| CN110839622A (en) * | 2019-11-01 | 2020-02-28 | 仲恺农业工程学院 | Potassium hydrogen persulfate sustained-release agent and preparation method and application thereof |
| CN112430508A (en) * | 2020-12-09 | 2021-03-02 | 淄博鑫欧瑞环保科技有限公司 | Disinfectant powder atomizing device cleaning agent, application and cleaning method thereof |
| CN113367155A (en) * | 2021-05-18 | 2021-09-10 | 武汉科缘生物发展有限责任公司 | Potassium hydrogen persulfate compound disinfectant and application thereof |
| CN113994973A (en) * | 2021-11-05 | 2022-02-01 | 开封恩科生物科技有限公司 | Potassium monopersulfate microencapsulated compound disinfectant and production process thereof |
| WO2023219867A1 (en) * | 2022-05-11 | 2023-11-16 | Arxada Ag | Single dose disinfectant |
| CN116267919A (en) * | 2023-03-26 | 2023-06-23 | 广州叁个圆消毒技术有限公司 | Potassium hydrogen persulfate compound powder and preparation method thereof |
| CN116267919B (en) * | 2023-03-26 | 2023-09-12 | 广州叁个圆消毒技术有限公司 | Potassium hydrogen persulfate compound powder and preparation method thereof |
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Application publication date: 20100922 |