CN101790510B - 制备异氰酸酯的方法 - Google Patents

制备异氰酸酯的方法 Download PDF

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Publication number
CN101790510B
CN101790510B CN2008801048496A CN200880104849A CN101790510B CN 101790510 B CN101790510 B CN 101790510B CN 2008801048496 A CN2008801048496 A CN 2008801048496A CN 200880104849 A CN200880104849 A CN 200880104849A CN 101790510 B CN101790510 B CN 101790510B
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CN
China
Prior art keywords
tdi
evaporator
temperature
mixture
helical tube
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN2008801048496A
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English (en)
Chinese (zh)
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CN101790510A (zh
Inventor
B·拉姆普夫
M·伯克
M·菲纳
E·史特约弗
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN2008801048496A 2007-08-31 2008-08-27 制备异氰酸酯的方法 Expired - Fee Related CN101790510B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07115380 2007-08-31
EP07115380.3 2007-08-31
PCT/EP2008/061188 WO2009027418A1 (de) 2007-08-31 2008-08-27 Verfahren zur herstellung von isocyanaten

Publications (2)

Publication Number Publication Date
CN101790510A CN101790510A (zh) 2010-07-28
CN101790510B true CN101790510B (zh) 2013-07-24

Family

ID=40090056

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2008801048496A Expired - Fee Related CN101790510B (zh) 2007-08-31 2008-08-27 制备异氰酸酯的方法

Country Status (7)

Country Link
US (1) US8273915B2 (enExample)
EP (1) EP2197836B1 (enExample)
JP (1) JP5398714B2 (enExample)
KR (1) KR101578565B1 (enExample)
CN (1) CN101790510B (enExample)
MX (1) MX2010001396A (enExample)
WO (1) WO2009027418A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100810828B1 (ko) * 2006-03-17 2008-03-06 와이케이케이 가부시끼가이샤 정음 면파스너
CN102803200B (zh) 2009-04-24 2014-12-31 巴斯夫欧洲公司 制备颜色稳定的mda和mdi的方法
JP5386038B2 (ja) 2009-06-24 2014-01-15 ビーエーエスエフ ソシエタス・ヨーロピア ホスゲン処理プラントへの水の進入を測定する方法
PT2445869E (pt) 2009-06-26 2015-02-05 Basf Se Processo para a produção de isocianatos, de preferência di-isocianatos e poli-isocianatos com recirculação de solvente
WO2011006807A2 (en) 2009-07-14 2011-01-20 Basf Se Process for preparing light-coloured isocyanates of the diphenylmethane series
CN102471071B (zh) 2009-07-16 2015-01-28 巴斯夫欧洲公司 制备二苯基甲烷二异氰酸酯系列的浅色异氰酸酯的方法
HUE035678T2 (en) 2012-03-19 2018-05-28 Covestro Deutschland Ag Process for the preparation of isocyanates
CN113444022B (zh) * 2020-03-24 2022-11-08 万华化学（宁波）有限公司 一种制备低色号长保质期耐低温的mdi-50的方法
CN111961185B (zh) * 2020-08-27 2022-07-12 万华化学集团股份有限公司 一种多亚甲基多苯基多异氰酸酯组合物及其制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1307497A (zh) * 1998-06-23 2001-08-08 拜尔公司 从溶液中分离聚合物的方法
CN1729166A (zh) * 2002-12-19 2006-02-01 巴斯福股份公司 从反应混合物中分离异氰酸酯的方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3140305A (en) 1962-12-17 1964-07-07 Fmc Corp Preparation of diisocyanates
DE2452805A1 (de) * 1974-11-07 1976-05-20 Basf Ag Verfahren zur abtrennung von rueckstaenden der toluylendiisocyanatherstellung
DE4127514A1 (de) 1991-08-20 1993-02-25 Bayer Ag Verfahren zur gewinnung von polyisocyanaten aus destillationsrueckstaenden der toluylendiisocyanatherstellung
DE4142769A1 (de) 1991-12-23 1993-06-24 Bayer Hispania Ind S A Verfahren zur herstellung von isocyanaten und aufarbeitung des rueckstandes
US5962728A (en) * 1997-10-31 1999-10-05 Arco Chemical Technology, L.P. Isocyanate residue purification
DE10260092A1 (de) 2002-12-19 2004-07-01 Basf Ag Verfahren zur Reinigung von Isocyanaten

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1307497A (zh) * 1998-06-23 2001-08-08 拜尔公司 从溶液中分离聚合物的方法
CN1729166A (zh) * 2002-12-19 2006-02-01 巴斯福股份公司 从反应混合物中分离异氰酸酯的方法

Also Published As

Publication number Publication date
JP2010536928A (ja) 2010-12-02
US20110124908A1 (en) 2011-05-26
CN101790510A (zh) 2010-07-28
KR20100082831A (ko) 2010-07-20
MX2010001396A (es) 2010-03-01
JP5398714B2 (ja) 2014-01-29
US8273915B2 (en) 2012-09-25
EP2197836A1 (de) 2010-06-23
KR101578565B1 (ko) 2015-12-17
EP2197836B1 (de) 2013-04-24
WO2009027418A1 (de) 2009-03-05

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Granted publication date: 20130724

Termination date: 20160827

CF01 Termination of patent right due to non-payment of annual fee