CN101785527A - 一种脱酚棉籽蛋白和棉籽糖的制取方法 - Google Patents
一种脱酚棉籽蛋白和棉籽糖的制取方法 Download PDFInfo
- Publication number
- CN101785527A CN101785527A CN200910263903A CN200910263903A CN101785527A CN 101785527 A CN101785527 A CN 101785527A CN 200910263903 A CN200910263903 A CN 200910263903A CN 200910263903 A CN200910263903 A CN 200910263903A CN 101785527 A CN101785527 A CN 101785527A
- Authority
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- Prior art keywords
- raffinose
- oil
- cotton
- cottonseed
- solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000012343 cottonseed oil Nutrition 0.000 title claims abstract description 30
- 108090000623 proteins and genes Proteins 0.000 title claims abstract description 28
- 102000004169 proteins and genes Human genes 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 20
- MUPFEKGTMRGPLJ-RMMQSMQOSA-N Raffinose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 MUPFEKGTMRGPLJ-RMMQSMQOSA-N 0.000 title claims abstract description 19
- MUPFEKGTMRGPLJ-UHFFFAOYSA-N UNPD196149 Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(CO)O2)O)O1 MUPFEKGTMRGPLJ-UHFFFAOYSA-N 0.000 title claims abstract description 19
- MUPFEKGTMRGPLJ-ZQSKZDJDSA-N raffinose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)O)O1 MUPFEKGTMRGPLJ-ZQSKZDJDSA-N 0.000 title claims abstract description 19
- 229920000742 Cotton Polymers 0.000 claims abstract description 40
- 239000003921 oil Substances 0.000 claims abstract description 15
- 235000019198 oils Nutrition 0.000 claims abstract description 15
- 239000002904 solvent Substances 0.000 claims abstract description 13
- 239000010779 crude oil Substances 0.000 claims abstract description 8
- 238000000926 separation method Methods 0.000 claims abstract description 8
- 239000012043 crude product Substances 0.000 claims abstract description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 18
- 239000000047 product Substances 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 12
- 238000001704 evaporation Methods 0.000 claims description 6
- 230000008020 evaporation Effects 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 239000002798 polar solvent Substances 0.000 claims description 5
- 230000000694 effects Effects 0.000 claims description 4
- 238000011084 recovery Methods 0.000 claims description 3
- 238000007670 refining Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- CMXPERZAMAQXSF-UHFFFAOYSA-M sodium;1,4-bis(2-ethylhexoxy)-1,4-dioxobutane-2-sulfonate;1,8-dihydroxyanthracene-9,10-dione Chemical compound [Na+].O=C1C2=CC=CC(O)=C2C(=O)C2=C1C=CC=C2O.CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC CMXPERZAMAQXSF-UHFFFAOYSA-M 0.000 claims description 3
- 230000003068 static effect Effects 0.000 claims description 3
- 239000010409 thin film Substances 0.000 claims description 3
- 238000005516 engineering process Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000003750 conditioning effect Effects 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 2
- 239000010903 husk Substances 0.000 abstract 2
- 238000000746 purification Methods 0.000 abstract 2
- 239000008157 edible vegetable oil Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000012856 packing Methods 0.000 abstract 1
- 238000004062 sedimentation Methods 0.000 abstract 1
- QBKSWRVVCFFDOT-UHFFFAOYSA-N gossypol Chemical compound CC(C)C1=C(O)C(O)=C(C=O)C2=C(O)C(C=3C(O)=C4C(C=O)=C(O)C(O)=C(C4=CC=3C)C(C)C)=C(C)C=C21 QBKSWRVVCFFDOT-UHFFFAOYSA-N 0.000 description 16
- QHOPXUFELLHKAS-UHFFFAOYSA-N Thespesin Natural products CC(C)c1c(O)c(O)c2C(O)Oc3c(c(C)cc1c23)-c1c2OC(O)c3c(O)c(O)c(C(C)C)c(cc1C)c23 QHOPXUFELLHKAS-UHFFFAOYSA-N 0.000 description 8
- 229930000755 gossypol Natural products 0.000 description 8
- 229950005277 gossypol Drugs 0.000 description 8
- 235000019733 Fish meal Nutrition 0.000 description 3
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 3
- 244000046052 Phaseolus vulgaris Species 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 3
- 239000004467 fishmeal Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 230000007850 degeneration Effects 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 1
- 101100020212 Mus musculus Klhdc3 gene Proteins 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 239000004459 forage Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 210000004995 male reproductive system Anatomy 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001850 reproductive effect Effects 0.000 description 1
- 239000012453 solvate Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Abstract
Description
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910263903A CN101785527B (zh) | 2009-12-22 | 2009-12-22 | 一种脱酚棉籽蛋白和棉籽糖的制取方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200910263903A CN101785527B (zh) | 2009-12-22 | 2009-12-22 | 一种脱酚棉籽蛋白和棉籽糖的制取方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101785527A true CN101785527A (zh) | 2010-07-28 |
| CN101785527B CN101785527B (zh) | 2012-09-26 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910263903A Active CN101785527B (zh) | 2009-12-22 | 2009-12-22 | 一种脱酚棉籽蛋白和棉籽糖的制取方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101785527B (zh) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102206290A (zh) * | 2011-04-06 | 2011-10-05 | 武汉普赛特膜技术循环利用有限公司 | 从棉籽粕中提取棉籽低聚糖和棉籽蛋白低聚肽的方法 |
| CN102349595A (zh) * | 2011-10-28 | 2012-02-15 | 晨光生物科技集团股份有限公司 | 一种提高棉籽蛋白的吸收利用率的工业方法 |
| CN103724379A (zh) * | 2013-12-31 | 2014-04-16 | 晨光生物科技集团股份有限公司 | 从棉粕脱酚液中提取棉籽糖的方法 |
| CN104026346A (zh) * | 2014-06-29 | 2014-09-10 | 段茂君 | 一种全脂棉仁蛋白的制备方法及采用的棉籽剥壳设备 |
| CN106380494A (zh) * | 2016-08-19 | 2017-02-08 | 晨光生物科技集团喀什有限公司 | 一种棉籽糖粗品生产工艺 |
| CN107011411A (zh) * | 2017-04-28 | 2017-08-04 | 济南中棉生物科技有限公司 | 一种可提取多种副产品的棉籽蛋白生产方法 |
| CN107382560A (zh) * | 2017-09-18 | 2017-11-24 | 湖南农业大学 | 一种葡萄专用肥及其制备方法与施用方法 |
| CN107522551A (zh) * | 2017-09-18 | 2017-12-29 | 湖南农业大学 | 一种柑橘专用肥及其制备方法与施用方法 |
| CN112385742A (zh) * | 2020-11-17 | 2021-02-23 | 晨光生物科技集团股份有限公司 | 一种低棉酚棉粕生产工艺 |
| CN113444567A (zh) * | 2021-07-22 | 2021-09-28 | 刘庆锋 | 脱酚浓缩棉籽蛋白萃取工艺 |
| CN114874848A (zh) * | 2022-05-31 | 2022-08-09 | 江苏冠军科技集团股份有限公司 | 一种醇酸树脂组合物及其制备方法与应用 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1100134C (zh) * | 2000-12-11 | 2003-01-29 | 北京中棉紫光生物科技有限公司 | 一种棉籽的处理方法 |
| CN1331412C (zh) * | 2005-12-13 | 2007-08-15 | 陕西中恒粮油工程技术有限公司 | 一步法生产脱酚棉蛋白的方法 |
| CN101037455A (zh) * | 2007-04-13 | 2007-09-19 | 孙宁祥 | 一种自棉籽粕中提取棉籽糖的方法 |
| CN100545175C (zh) * | 2007-04-29 | 2009-09-30 | 北京中棉紫光棉业科技有限公司 | 一种棉籽低聚糖粉的生产方法 |
| CN100594215C (zh) * | 2007-07-11 | 2010-03-17 | 山东国信生物蛋白有限公司 | 脱酚棉籽蛋白萃取方法 |
-
2009
- 2009-12-22 CN CN200910263903A patent/CN101785527B/zh active Active
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102206290A (zh) * | 2011-04-06 | 2011-10-05 | 武汉普赛特膜技术循环利用有限公司 | 从棉籽粕中提取棉籽低聚糖和棉籽蛋白低聚肽的方法 |
| CN102206290B (zh) * | 2011-04-06 | 2013-04-10 | 武汉普赛特膜技术循环利用有限公司 | 从棉籽粕中提取棉籽低聚糖和棉籽蛋白低聚肽的方法 |
| CN102349595A (zh) * | 2011-10-28 | 2012-02-15 | 晨光生物科技集团股份有限公司 | 一种提高棉籽蛋白的吸收利用率的工业方法 |
| CN103724379A (zh) * | 2013-12-31 | 2014-04-16 | 晨光生物科技集团股份有限公司 | 从棉粕脱酚液中提取棉籽糖的方法 |
| CN103724379B (zh) * | 2013-12-31 | 2016-03-23 | 晨光生物科技集团股份有限公司 | 从棉粕脱酚液中提取棉籽糖的方法 |
| CN104026346A (zh) * | 2014-06-29 | 2014-09-10 | 段茂君 | 一种全脂棉仁蛋白的制备方法及采用的棉籽剥壳设备 |
| CN104026346B (zh) * | 2014-06-29 | 2016-07-13 | 段茂君 | 一种全脂棉仁蛋白的制备方法及采用的棉籽剥壳设备 |
| CN106380494A (zh) * | 2016-08-19 | 2017-02-08 | 晨光生物科技集团喀什有限公司 | 一种棉籽糖粗品生产工艺 |
| CN107011411A (zh) * | 2017-04-28 | 2017-08-04 | 济南中棉生物科技有限公司 | 一种可提取多种副产品的棉籽蛋白生产方法 |
| CN107011411B (zh) * | 2017-04-28 | 2020-12-18 | 济南中棉生物科技有限公司 | 一种可提取多种副产品的棉籽蛋白生产方法 |
| CN107382560A (zh) * | 2017-09-18 | 2017-11-24 | 湖南农业大学 | 一种葡萄专用肥及其制备方法与施用方法 |
| CN107522551A (zh) * | 2017-09-18 | 2017-12-29 | 湖南农业大学 | 一种柑橘专用肥及其制备方法与施用方法 |
| CN112385742A (zh) * | 2020-11-17 | 2021-02-23 | 晨光生物科技集团股份有限公司 | 一种低棉酚棉粕生产工艺 |
| CN112385742B (zh) * | 2020-11-17 | 2023-01-31 | 晨光生物科技集团股份有限公司 | 一种低棉酚棉粕生产工艺 |
| CN113444567A (zh) * | 2021-07-22 | 2021-09-28 | 刘庆锋 | 脱酚浓缩棉籽蛋白萃取工艺 |
| CN114874848A (zh) * | 2022-05-31 | 2022-08-09 | 江苏冠军科技集团股份有限公司 | 一种醇酸树脂组合物及其制备方法与应用 |
| CN114874848B (zh) * | 2022-05-31 | 2023-10-20 | 江苏冠军科技集团股份有限公司 | 一种醇酸树脂组合物及其制备方法与应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101785527B (zh) | 2012-09-26 |
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Denomination of invention: Method for preparing dephenolization cottonseed protein and raffinose Effective date of registration: 20130128 Granted publication date: 20120926 Pledgee: China Everbright Bank Handan branch Pledgor: Chengguang Natural Pigment Group Co., Ltd. Registration number: 2013990000062 |
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Denomination of invention: Method for preparing dephenolization cottonseed protein and raffinose Effective date of registration: 20170310 Granted publication date: 20120926 Pledgee: China Everbright Bank Handan branch Pledgor: Chengguang Natural Pigment Group Co., Ltd. Registration number: 2017990000180 |
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Denomination of invention: Method for preparing dephenolization cottonseed protein and raffinose Effective date of registration: 20180524 Granted publication date: 20120926 Pledgee: China Everbright Bank Handan branch Pledgor: Chengguang Natural Pigment Group Co., Ltd. Registration number: 2018990000408 |
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Denomination of invention: Method for preparing dephenolization cottonseed protein and raffinose Effective date of registration: 20190628 Granted publication date: 20120926 Pledgee: China Everbright Bank Handan branch Pledgor: Chengguang Natural Pigment Group Co., Ltd. Registration number: 2019990000630 |
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Effective date of registration: 20210519 Address after: 057250 No.16, modern Avenue, modern new industrial park, Quzhou County, Handan City, Hebei Province Patentee after: Handan Chenguang plant protein Co.,Ltd. Address before: 057250 No.1, Chenguang Road, Quzhou County, Hebei Province Patentee before: Chenguang Biotech Group Co.,Ltd. |