CN100545175C - 一种棉籽低聚糖粉的生产方法 - Google Patents
一种棉籽低聚糖粉的生产方法 Download PDFInfo
- Publication number
- CN100545175C CN100545175C CNB2007100988904A CN200710098890A CN100545175C CN 100545175 C CN100545175 C CN 100545175C CN B2007100988904 A CNB2007100988904 A CN B2007100988904A CN 200710098890 A CN200710098890 A CN 200710098890A CN 100545175 C CN100545175 C CN 100545175C
- Authority
- CN
- China
- Prior art keywords
- cottonseed
- methyl alcohol
- extraction
- raffinate
- gossypol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000012343 cottonseed oil Nutrition 0.000 title claims abstract description 55
- 229920001542 oligosaccharide Polymers 0.000 title claims abstract description 22
- 150000002482 oligosaccharides Chemical class 0.000 title claims abstract description 22
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 213
- QBKSWRVVCFFDOT-UHFFFAOYSA-N gossypol Chemical compound CC(C)C1=C(O)C(O)=C(C=O)C2=C(O)C(C=3C(O)=C4C(C=O)=C(O)C(O)=C(C4=CC=3C)C(C)C)=C(C)C=C21 QBKSWRVVCFFDOT-UHFFFAOYSA-N 0.000 claims abstract description 44
- QHOPXUFELLHKAS-UHFFFAOYSA-N Thespesin Natural products CC(C)c1c(O)c(O)c2C(O)Oc3c(c(C)cc1c23)-c1c2OC(O)c3c(O)c(O)c(C(C)C)c(cc1C)c23 QHOPXUFELLHKAS-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229930000755 gossypol Natural products 0.000 claims abstract description 22
- 229950005277 gossypol Drugs 0.000 claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000000126 substance Substances 0.000 claims abstract description 12
- 239000011343 solid material Substances 0.000 claims abstract description 9
- MUPFEKGTMRGPLJ-RMMQSMQOSA-N Raffinose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 MUPFEKGTMRGPLJ-RMMQSMQOSA-N 0.000 claims abstract description 7
- MUPFEKGTMRGPLJ-UHFFFAOYSA-N UNPD196149 Natural products OC1C(O)C(CO)OC1(CO)OC1C(O)C(O)C(O)C(COC2C(C(O)C(O)C(CO)O2)O)O1 MUPFEKGTMRGPLJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 7
- MUPFEKGTMRGPLJ-ZQSKZDJDSA-N raffinose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)O)O1 MUPFEKGTMRGPLJ-ZQSKZDJDSA-N 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000010298 pulverizing process Methods 0.000 claims abstract description 5
- 235000019750 Crude protein Nutrition 0.000 claims abstract description 4
- UQZIYBXSHAGNOE-USOSMYMVSA-N Stachyose Natural products O(C[C@H]1[C@@H](O)[C@H](O)[C@H](O)[C@@H](O[C@@]2(CO)[C@H](O)[C@@H](O)[C@@H](CO)O2)O1)[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@H](CO[C@@H]2[C@@H](O)[C@@H](O)[C@@H](O)[C@H](CO)O2)O1 UQZIYBXSHAGNOE-USOSMYMVSA-N 0.000 claims abstract description 4
- UQZIYBXSHAGNOE-XNSRJBNMSA-N stachyose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO[C@@H]3[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O3)O)O2)O)O1 UQZIYBXSHAGNOE-XNSRJBNMSA-N 0.000 claims abstract description 4
- 238000000605 extraction Methods 0.000 claims description 56
- 238000000034 method Methods 0.000 claims description 14
- 239000000284 extract Substances 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 9
- 235000019198 oils Nutrition 0.000 claims description 8
- 241000209094 Oryza Species 0.000 claims description 6
- 235000007164 Oryza sativa Nutrition 0.000 claims description 6
- 238000002425 crystallisation Methods 0.000 claims description 6
- 230000008025 crystallization Effects 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 235000009566 rice Nutrition 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000006188 syrup Substances 0.000 claims description 3
- 235000020357 syrup Nutrition 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims 1
- 235000008504 concentrate Nutrition 0.000 claims 1
- 238000001704 evaporation Methods 0.000 abstract description 6
- 235000013305 food Nutrition 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 5
- 230000008020 evaporation Effects 0.000 abstract description 5
- 239000013538 functional additive Substances 0.000 abstract description 5
- 238000009776 industrial production Methods 0.000 abstract description 3
- 238000011084 recovery Methods 0.000 abstract description 3
- 239000000470 constituent Substances 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 6
- 102000004169 proteins and genes Human genes 0.000 description 5
- 108090000623 proteins and genes Proteins 0.000 description 5
- 239000004519 grease Substances 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000004925 denaturation Methods 0.000 description 2
- 230000036425 denaturation Effects 0.000 description 2
- 210000001035 gastrointestinal tract Anatomy 0.000 description 2
- 238000003672 processing method Methods 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 244000144987 brood Species 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 235000015872 dietary supplement Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 244000005709 gut microbiome Species 0.000 description 1
- 230000001077 hypotensive effect Effects 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 206010025482 malaise Diseases 0.000 description 1
- 238000003808 methanol extraction Methods 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2007100988904A CN100545175C (zh) | 2007-04-29 | 2007-04-29 | 一种棉籽低聚糖粉的生产方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2007100988904A CN100545175C (zh) | 2007-04-29 | 2007-04-29 | 一种棉籽低聚糖粉的生产方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101037482A CN101037482A (zh) | 2007-09-19 |
CN100545175C true CN100545175C (zh) | 2009-09-30 |
Family
ID=38888680
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2007100988904A Expired - Fee Related CN100545175C (zh) | 2007-04-29 | 2007-04-29 | 一种棉籽低聚糖粉的生产方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN100545175C (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101785527B (zh) * | 2009-12-22 | 2012-09-26 | 晨光生物科技集团股份有限公司 | 一种脱酚棉籽蛋白和棉籽糖的制取方法 |
CN107232387A (zh) * | 2016-07-18 | 2017-10-10 | 湖南欣瑞生物科技有限公司 | 一种棉籽蛋白的提取方法 |
-
2007
- 2007-04-29 CN CNB2007100988904A patent/CN100545175C/zh not_active Expired - Fee Related
Non-Patent Citations (9)
Title |
---|
Optimization of extraction methods for determinationoftheraffinose family oligosaccharides in leguminousvinepeasand effects of blanching. J Ekvall etc.Journal of Food Composition and Analysis,Vol.第20卷 No.第1期. 2006 |
Optimization of extraction methods for determinationoftheraffinose family oligosaccharides in leguminousvinepeasand effects of blanching. J Ekvall etc.Journal of Food Composition and Analysis,Vol.20 No.1. 2006 * |
从无腺体棉籽中提取棉籽糖的研究. 张大煜等.中国油脂,第21卷第5期. 1996 |
从无腺体棉籽中提取棉籽糖的研究. 张大煜等.中国油脂,第21卷第5期. 1996 * |
棉籽低聚糖. 焦洋等.中国棉花加工,第2007年卷第1期. 2007 |
棉籽低聚糖. 焦洋等.中国棉花加工,第2007年卷第1期. 2007 * |
用乙醇-水从双液相棉粕中提取棉子糖的研究. 詹少春等.南京工业大学学报,第28卷第1期. 2006 |
脱脂棉籽粕中棉籽糖提取方法的研究. 王兴国等.中国油脂,第30卷第3期. 2005 |
脱脂棉籽粕中棉籽糖提取方法的研究. 王兴国等.中国油脂,第30卷第3期. 2005 * |
Also Published As
Publication number | Publication date |
---|---|
CN101037482A (zh) | 2007-09-19 |
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Denomination of invention: Cottonseed oligosaccharide production method Effective date of registration: 20101028 Granted publication date: 20090930 Pledgee: Bank of Communications Ltd Beijing Zhongguancun Park sub branch Pledgor: Beijing Zhongmian Ziguang Biological Technology Co., Ltd.|Beijing China Cotton Unis Cotton Industry Technology Co. Ltd. Registration number: 2010990000943 |
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Date of cancellation: 20120315 Granted publication date: 20090930 Pledgee: Bank of Communications Ltd Beijing Zhongguancun Park sub branch Pledgor: Beijing Zhongmian Ziguang Biological Technology Co., Ltd.|Beijing China Cotton Unis Cotton Industry Technology Co. Ltd. Registration number: 2010990000943 |
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