CN101747232B - 在气相中制备异氰酸酯的方法 - Google Patents
在气相中制备异氰酸酯的方法 Download PDFInfo
- Publication number
- CN101747232B CN101747232B CN200910261576.2A CN200910261576A CN101747232B CN 101747232 B CN101747232 B CN 101747232B CN 200910261576 A CN200910261576 A CN 200910261576A CN 101747232 B CN101747232 B CN 101747232B
- Authority
- CN
- China
- Prior art keywords
- tda
- toluenediamine
- weight
- evaporator
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/14—Derivatives of isocyanic acid containing at least two isocyanate groups bound to the same carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008063991.5 | 2008-12-19 | ||
| DE102008063991A DE102008063991A1 (de) | 2008-12-19 | 2008-12-19 | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101747232A CN101747232A (zh) | 2010-06-23 |
| CN101747232B true CN101747232B (zh) | 2014-01-29 |
Family
ID=41785851
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200910261576.2A Active CN101747232B (zh) | 2008-12-19 | 2009-12-17 | 在气相中制备异氰酸酯的方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9365503B2 (enExample) |
| EP (1) | EP2199276B1 (enExample) |
| JP (1) | JP5574691B2 (enExample) |
| KR (1) | KR101685699B1 (enExample) |
| CN (1) | CN101747232B (enExample) |
| DE (1) | DE102008063991A1 (enExample) |
| HU (1) | HUE027797T2 (enExample) |
| RU (1) | RU2526621C2 (enExample) |
| TW (1) | TWI440620B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12080779B2 (en) * | 2019-08-23 | 2024-09-03 | Taiwan Semiconductor Manufacturing Co., Ltd. | Capping layer for gate electrodes |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101912751B (zh) * | 2010-09-03 | 2012-12-12 | 烟台万华聚氨酯股份有限公司 | 一种胺汽化器及其用于制备异氰酸酯的方法 |
| PL214497B1 (pl) * | 2010-12-10 | 2013-08-30 | Inst Chemii Przemyslowej Im Prof Ignacego Moscickiego | Sposób otrzymywania toluilenodiizocyjanianu (TDI) w procesie fosgenowania toluilenodiaminy (TDA) w fazie gazowej |
| JP5744619B2 (ja) * | 2011-05-18 | 2015-07-08 | 三井化学株式会社 | トリレンジイソシアネートの製造方法 |
| CN104302617A (zh) * | 2012-05-04 | 2015-01-21 | 拜耳材料科技股份有限公司 | 处理包含芳香胺的物质混合物,特别是粗制苯胺的物质混合物的方法 |
| HUE030188T2 (en) * | 2013-01-22 | 2017-04-28 | Covestro Deutschland Ag | Process for the preparation of aromatic amines |
| HUE047167T2 (hu) * | 2015-09-24 | 2020-04-28 | Covestro Deutschland Ag | Eljárás izocianátok elõállítására |
| HUE054424T2 (hu) | 2017-01-27 | 2021-09-28 | Covestro Llc | Eljárás stabil toluol-diamin származék/víz elegyek elõállítására, kapcsolódó készítmények, és az elegyek üzemanyagként történõ alkalmazásának eljárásai |
| EP3904336B1 (en) | 2018-12-26 | 2023-05-03 | Wanhua Chemical Group Co., Ltd. | Method for preparing isocyanate in gaseous phase |
| WO2022248448A1 (en) * | 2021-05-25 | 2022-12-01 | Basf Se | Process for preparing at least one polyisocyanate |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0570799A1 (de) * | 1992-05-22 | 1993-11-24 | Bayer Ag | Verfahren zur Herstellung von aromatischen Diisocyanaten |
| CN1052473C (zh) * | 1992-10-16 | 2000-05-17 | 罗纳·布朗克化学公司 | 在气相中制备芳族异氰酸酯型化合物的方法 |
| CN1907964A (zh) * | 2005-08-02 | 2007-02-07 | 拜尔材料科学股份公司 | 气相光气化方法 |
| CN1317262C (zh) * | 2003-02-20 | 2007-05-23 | 拜尔公司 | 在气相中制备(多)异氰酸酯的方法 |
| WO2008071564A1 (de) * | 2006-12-11 | 2008-06-19 | Basf Se | Verfahren zur herstellung von isocyanaten |
| CN101205197A (zh) * | 2006-12-13 | 2008-06-25 | 拜尔材料科学股份公司 | 在气相中制备异氰酸酯的方法 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2135154C3 (de) | 1971-07-14 | 1980-04-30 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Aminoverbindungen durch kontinuierliche Reduktion von Nitroverbindungen |
| DE3714439A1 (de) | 1987-04-30 | 1988-11-10 | Bayer Ag | Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten |
| DE3734344A1 (de) | 1987-10-10 | 1989-04-20 | Bayer Ag | Verfahren zur verdampfung von dinitrotoluolen (dnt) |
| US5081303A (en) * | 1989-04-21 | 1992-01-14 | First Chemical Corporation | Co-production of an aromatic monoamine and an aromatic diamine directly from benzene or a benzene derivative through controlled nitration and reduction |
| DE4230098C1 (enExample) | 1992-09-09 | 1993-06-03 | Bayer Ag, 5090 Leverkusen, De | |
| DE4323687A1 (de) | 1993-07-15 | 1995-01-19 | Bayer Ag | Kontinuierliches Verfahren zur Herstellung von aromatischen Aminen |
| DE4435839A1 (de) | 1994-10-07 | 1996-04-11 | Bayer Ag | Schlammphasenreaktor und dessen Verwendung |
| DE19608443C1 (de) | 1996-03-05 | 1997-07-24 | Bayer Ag | Verfahren zur Aufarbeitung von Amingemischen bei der Diaminotoluol-Herstellung unter Abtrennung der Schwersieder |
| FR2777560B1 (fr) * | 1998-04-17 | 2000-06-09 | Rhodia Chimie Sa | Procede de purification de polyamines aromatiques |
| US6005143A (en) | 1998-08-07 | 1999-12-21 | Air Products And Chemicals, Inc. | Use of a monolith catalyst for the hydrogenation of dinitrotoluene to toluenediamine |
| DE19909168A1 (de) | 1999-03-03 | 2000-09-07 | Basf Ag | Verfahren zur Herstellung von Aminen |
| US6664833B1 (en) | 2000-11-20 | 2003-12-16 | Intersil Americas, Inc. | Dual-edge function clock generator and method of deriving clocking signals for executing reduced instruction sequences in a re-programmable I/O interface |
| US6359177B1 (en) * | 2000-12-15 | 2002-03-19 | Bayer Corporation | Process for separating mixtures of materials having different boiling points |
| US7109378B2 (en) | 2001-08-30 | 2006-09-19 | Air Products And Chemicals, Inc. | Monolith catalytic reactor coupled to static mixer |
| DE10222023A1 (de) | 2002-05-17 | 2003-11-27 | Bayer Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE10335451A1 (de) | 2003-08-02 | 2005-03-10 | Bayer Materialscience Ag | Verfahren zur Entfernung von flüchtigen Verbindungen aus Stoffgemischen mittels Mikroverdampfer |
| DE10349504A1 (de) | 2003-10-23 | 2005-05-25 | Bayer Technology Services Gmbh | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE10359627A1 (de) | 2003-12-18 | 2005-07-21 | Bayer Materialscience Ag | Verfahren zur Herstellung von Diisocyanaten |
| DE102004001456A1 (de) | 2004-01-08 | 2005-08-11 | Basf Ag | Verfahren zur destillativen Aufbereitung von Toluylendiamin |
| EP1746083B1 (de) | 2005-07-12 | 2016-12-21 | Covestro Deutschland AG | Verfahren zur Herstellung von Toluylendiamin |
| DE102005032430A1 (de) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiamin |
| US20070049482A1 (en) | 2005-08-11 | 2007-03-01 | Shin-Etsu Chemical Co., Ltd. | Synthetic quartz glass substrate for excimer lasers and making method |
| DE102005042392A1 (de) | 2005-09-06 | 2007-03-08 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| DE102006060181A1 (de) * | 2006-12-18 | 2008-06-19 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiisocyanat |
| DE102007056511A1 (de) * | 2007-11-22 | 2009-05-28 | Bayer Materialscience Ag | Verfahren zur Herstellung aromatischer Diisocyanate in der Gasphase |
-
2008
- 2008-12-19 DE DE102008063991A patent/DE102008063991A1/de not_active Withdrawn
-
2009
- 2009-11-30 TW TW098140733A patent/TWI440620B/zh not_active IP Right Cessation
- 2009-12-05 EP EP09015100.2A patent/EP2199276B1/de active Active
- 2009-12-05 HU HUE09015100A patent/HUE027797T2/en unknown
- 2009-12-14 US US12/636,925 patent/US9365503B2/en active Active
- 2009-12-15 JP JP2009284086A patent/JP5574691B2/ja not_active Expired - Fee Related
- 2009-12-17 CN CN200910261576.2A patent/CN101747232B/zh active Active
- 2009-12-18 RU RU2009147083/04A patent/RU2526621C2/ru not_active IP Right Cessation
- 2009-12-18 KR KR1020090126860A patent/KR101685699B1/ko active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0570799A1 (de) * | 1992-05-22 | 1993-11-24 | Bayer Ag | Verfahren zur Herstellung von aromatischen Diisocyanaten |
| US5449818A (en) * | 1992-05-22 | 1995-09-12 | Bayer Aktiengesellschaft | Process for the preparation of aromatic diisocyanates |
| CN1052473C (zh) * | 1992-10-16 | 2000-05-17 | 罗纳·布朗克化学公司 | 在气相中制备芳族异氰酸酯型化合物的方法 |
| CN1317262C (zh) * | 2003-02-20 | 2007-05-23 | 拜尔公司 | 在气相中制备(多)异氰酸酯的方法 |
| CN1907964A (zh) * | 2005-08-02 | 2007-02-07 | 拜尔材料科学股份公司 | 气相光气化方法 |
| WO2008071564A1 (de) * | 2006-12-11 | 2008-06-19 | Basf Se | Verfahren zur herstellung von isocyanaten |
| CN101205197A (zh) * | 2006-12-13 | 2008-06-25 | 拜尔材料科学股份公司 | 在气相中制备异氰酸酯的方法 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12080779B2 (en) * | 2019-08-23 | 2024-09-03 | Taiwan Semiconductor Manufacturing Co., Ltd. | Capping layer for gate electrodes |
Also Published As
| Publication number | Publication date |
|---|---|
| TW201035021A (en) | 2010-10-01 |
| KR20100071929A (ko) | 2010-06-29 |
| KR101685699B1 (ko) | 2016-12-12 |
| HUE027797T2 (en) | 2016-11-28 |
| EP2199276B1 (de) | 2015-07-22 |
| RU2526621C2 (ru) | 2014-08-27 |
| TWI440620B (zh) | 2014-06-11 |
| EP2199276A1 (de) | 2010-06-23 |
| DE102008063991A1 (de) | 2010-06-24 |
| US20100160674A1 (en) | 2010-06-24 |
| CN101747232A (zh) | 2010-06-23 |
| US9365503B2 (en) | 2016-06-14 |
| RU2009147083A (ru) | 2011-06-27 |
| JP2010143900A (ja) | 2010-07-01 |
| JP5574691B2 (ja) | 2014-08-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent of invention or patent application | ||
| CB02 | Change of applicant information |
Address after: Germany Leverkusen Applicant after: BAYER MATERIALSCIENCE AG Address before: Germany Leverkusen Applicant before: BAYER MATERIALSCIENCE AG |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: BAYER AG TO: CARCOUSTICS TECHCONSULT GMBH |
|
| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20100623 Assignee: Bayer Intellectual Property GmbH Assignor: BAYER MATERIALSCIENCE AG Contract record no.: 2012990000854 Denomination of invention: Method for producing isocyanates in gas phase License type: Common License Record date: 20121128 |
|
| LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160617 Address after: Germany Leverkusen Patentee after: COVESTRO DEUTSCHLAND AG Address before: German Monheim Patentee before: BAYER INTELLECTUAL PROPERTY GmbH Effective date of registration: 20160617 Address after: German Monheim Patentee after: BAYER INTELLECTUAL PROPERTY GmbH Address before: Germany Leverkusen Patentee before: BAYER MATERIALSCIENCE AG |