CN101658480A - Production method of sophora alopecuroide bacteriostatic bath foam - Google Patents
Production method of sophora alopecuroide bacteriostatic bath foam Download PDFInfo
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- CN101658480A CN101658480A CN200910175652A CN200910175652A CN101658480A CN 101658480 A CN101658480 A CN 101658480A CN 200910175652 A CN200910175652 A CN 200910175652A CN 200910175652 A CN200910175652 A CN 200910175652A CN 101658480 A CN101658480 A CN 101658480A
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- total alkaloids
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- 239000006260 foam Substances 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 230000003385 bacteriostatic effect Effects 0.000 title claims abstract description 11
- 241001145009 Sophora alopecuroides Species 0.000 title claims abstract description 10
- 239000007788 liquid Substances 0.000 claims abstract description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000003814 drug Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 241000208340 Araliaceae Species 0.000 claims abstract description 14
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims abstract description 14
- 235000003140 Panax quinquefolius Nutrition 0.000 claims abstract description 14
- 235000008434 ginseng Nutrition 0.000 claims abstract description 14
- 239000012153 distilled water Substances 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 239000000341 volatile oil Substances 0.000 claims abstract description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000284 extract Substances 0.000 claims abstract description 9
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 4
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 4
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 4
- 239000008367 deionised water Substances 0.000 claims abstract description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 4
- 229930195729 fatty acid Natural products 0.000 claims abstract description 4
- 239000000194 fatty acid Substances 0.000 claims abstract description 4
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 4
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 4
- 238000002156 mixing Methods 0.000 claims abstract description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 4
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 4
- 229930013930 alkaloid Natural products 0.000 claims description 22
- 241000628997 Flos Species 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 238000010992 reflux Methods 0.000 claims description 9
- 239000008155 medical solution Substances 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 5
- 244000060011 Cocos nucifera Species 0.000 claims description 3
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 3
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 3
- 238000013019 agitation Methods 0.000 claims description 3
- 239000009188 angelicae sinensis extract Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 229940071826 hydroxyethyl cellulose Drugs 0.000 claims description 3
- 238000005304 joining Methods 0.000 claims description 3
- 239000012567 medical material Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims description 2
- 241000196324 Embryophyta Species 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 5
- 239000008280 blood Substances 0.000 abstract description 3
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- 244000223014 Syzygium aromaticum Species 0.000 abstract 2
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 abstract 1
- 229920006217 cellulose acetate butyrate Polymers 0.000 abstract 1
- 235000019864 coconut oil Nutrition 0.000 abstract 1
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- 244000046052 Phaseolus vulgaris Species 0.000 description 6
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- 206010000496 acne Diseases 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 241000222122 Candida albicans Species 0.000 description 4
- 241000588724 Escherichia coli Species 0.000 description 4
- 241000191967 Staphylococcus aureus Species 0.000 description 4
- 229940095731 candida albicans Drugs 0.000 description 4
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- 208000002874 Acne Vulgaris Diseases 0.000 description 3
- 206010048222 Xerosis Diseases 0.000 description 3
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- 229940079593 drug Drugs 0.000 description 3
- 230000002401 inhibitory effect Effects 0.000 description 3
- 241000233866 Fungi Species 0.000 description 2
- 241000219784 Sophora Species 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 210000004185 liver Anatomy 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
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- 239000002994 raw material Substances 0.000 description 2
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- 241000894006 Bacteria Species 0.000 description 1
- 241001300479 Macroptilium Species 0.000 description 1
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Abstract
The invention discloses a production method of sophora alopecuroide bacteriostatic bath foam. The main technique processes comprise: extracting cartialgenous with ethanol; extracting ginseng with distilled water; extracting essential oil from clove and angelica sinensis with distilled water; mixing the essential oil and extracted liquid medicine, adding total matrines extractum to make liquid traditional Chinese medicine, putting de-ionized water in a reaction vessel, adding hydroxyethyl cellulose, stirring evenly, adding mixed liquid traditional Chinese medicine, heating and adding dodecyl sodium sulfate, coconut oil fatty acid ethanolamide sulfosuccinates, fatty alcohol-polyoxyethylene ether sodium sulfate and pearly-luster slurry to stir for dissolution, heating to certain temperature,stirring to be dissolved, cooling, adding cellulose acetate butyrate and glycerine for stirring, and obtaining a finished product after passing inspection. The production method extracts essence fromsophora alopecuroide, ginseng, cartialgenous, angelica sinensis and clove, the produced finished product is pure natural plant effective bacteriostatic bath foam which has no irritation to skin, has the functions of invigorating circulation of blood, detoxicating, moistening skin and beautifying, and is a good bath product for effectively activating activity of dormant cells.
Description
Technical field
The present invention relates to a kind of production method of bath foam, refer in particular to a kind of method that is the antibacterial bath foam of raw material production with bitter bean bean.
Background technology
At present, symptoms such as owing to many-sided reasons such as natural environment, daily life and operating pressures, many person skins appearance are dry, nonelastic, speckle acne, this has brought worry to daily life.The traditional Chinese medical science thinks that symptoms such as xerosis cutis, comedo and acne, macule brown patch, endogenous cause of ill are that wind and heat in the lung meridian is fumigated and accumulate temperature, stagnation of QI due to depression of the liver, liver and gall fire of passion in skin, retention of heat in the spleen and stomach to cause the skin function to be lost smooth; Exopathogenic factor be wind, wet, hot heresy visitor in skin flesh table, cause the stagnant or wind and dryness blocking in skin due to blood-deficiency of the smooth stasis of blood of QI and blood, the skin skin losing its nutrition forms.And modern medicine is thought, above-mentioned symptom removes human body and the endocrine disturbance occurs, and antibacterial, virus are to cause the main cause of dermatopathy.
The medicinal function of the bitter bean bean of Sophora leguminous plant is in the clinical proof that obtained.For these reasons, developing a kind of is main effective ingredient with bitter bean bean total alkali, utilize it that staphylococcus aureus, fungus, Candida albicans, escherichia coli are had stronger killing action, be equipped with Chinese crude drugs such as Radix Ginseng, Cornu Cervi Pantotrichum, Radix Angelicae Sinensis, Flos Caryophylli again and make the bacterium skin moistening that disappears, promote the shower good merchantable brand of cytoactive to meet market demand.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of production method of sophora alopecuroide bacteriostatic bath foam, the preferred Chinese medicine preparation of this production method, adopt modern biotechnology, from multiple famous and precious plant, extract elite, adopt advanced extraction process, separation and purification forms to have and moistens the pure Chinese medicine bath foam of preserving moisture, activating the epidermis cell activity, strengthen skin immunity effect.
The technical problem to be solved in the present invention is realized by following scheme: the production method of sophora alopecuroide bacteriostatic bath foam, it is characterized in that: Cornu Cervi Pantotrichum, Radix Ginseng, Radix Angelicae Sinensis, four kinds of pulverizing medicinal materials of Flos Caryophylli are become coarse powder, the weight ratio of four kinds of medical materials is 1: 3-4: 10: 10, the Cornu Cervi Pantotrichum alcohol heating reflux secondary of concentration 95%, each ethanol that adds 6-8 times of weight extracted 1-2 hour, merged extracted twice liquid, recovery section ethanol, medicinal liquid is placed stand-by; Radix Ginseng adds the distilled water of 6-8 times of weight with distilled water reflux secondary at every turn, extracts 1-2 hour, merges extracted twice liquid, and it is stand-by that water-bath concentrates placement; Flos Caryophylli, Radix Angelicae Sinensis extract volatile oil respectively, add the distilled water of 8-12 times of weight separately, heating and refluxing extraction 8-9 hour, leave and take volatile oil; Extracting solution mixing and stirring with above-mentioned two kinds of volatile oil and Cornu Cervi Pantotrichum, Radix Ginseng becomes herb liquid then, again the water-bath of Radix Sophorae Flavescentis total alkaloids liquid is condensed into extractum, and joining by the weight of herb liquid 5% becomes the Chinese medicine admixing medical solutions in the herb liquid, leave and take stand-by after stirring; The deionized water of measuring 3 times of weight of Chinese medicine admixing medical solutions is put into reaction pot, the hydroxyethyl-cellulose that adds Radix Sophorae Flavescentis total alkaloids extractum weight 30%-50%, being stirred to fully, the dissolving back adds above-mentioned Chinese medicine admixing medical solutions wherein, be stirred to fully evenly, the citric acid that adds Radix Sophorae Flavescentis total alkaloids extractum weight 8%-12% again stirred 5 minutes, begin to heat and under agitation slowly add the cocoanut fatty acid diethanolamide of 10-15 times of weight of Radix Sophorae Flavescentis total alkaloids extractum, the polyoxyethylenated alcohol sodium sulfate of 12-15 times of weight of Radix Sophorae Flavescentis total alkaloids extractum, the sodium lauryl sulphate of 6-10 times of weight of Radix Sophorae Flavescentis total alkaloids extractum, the Pearl Concentrate that adds 3-5 times of weight of Radix Sophorae Flavescentis total alkaloids extractum when being warming up to 75 ℃, be stirred to dissolving fully, be warming up to 80 ℃ and stop heating, insulated and stirred 15 minutes, treat to dissolve fully, deaeration, begin to be cooled to below 50 ℃, the acetylbutyrylcellulose that adds 5-8 times of weight of Radix Sophorae Flavescentis total alkaloids extractum successively, the glycerol of 10-13 times of weight of Radix Sophorae Flavescentis total alkaloids extractum stirs after 20 minutes pick test and is finished product after qualified.
Advantage of the present invention is: this production method craft science is reasonable, its preferred Chinese medicine preparation, adopt modern biotechnology, with bitter bean bean is primary raw material, from rare Chinese medicines such as bitter bean bean, Radix Ginseng, Cornu Cervi Pantotrichum, extract elite, and be aided with the Chinese herbal medicine of dampness deinsectization such as Radix Angelicae Sinensis, Flos Caryophylli, heat-clearing and toxic substances removing, sterilizing and itch-relieving effect, and adopting advanced extraction process, separation and purification becomes sophora alopecuroide bacteriostatic bath foam.Experiment shows that sophora alopecuroide bacteriostatic bath foam has good inhibitory effect to pathogenic bacterias such as antibacterial, funguses.Wherein, bitter bean Macroptilium is a herbaceos perennial in the pulse family Sophora, has the drought-enduring effect of checking winds and fixing drifting sand, and its effective ingredient Radix Sophorae Flavescentis total alkaloids is as the loaded national drug standards of antibiosis anti-inflammatory drug.Have and studies show that: Radix Sophorae Flavescentis total alkaloids all has stronger inhibitory action to various pathogens such as staphylococcus aureus, Candida albicans, escherichia coli and Diplococcus gonorrhoeae, and fungistatic effect is stable, to skin and mucosa nonirritant, belong to nontoxic level, aspect skin and mucous membrane disinfection, have good application prospects.The ginsenoside's class that contains in amino acids that contains in the Cornu Cervi Pantotrichum and the Radix Ginseng all has skin repairs and moist, maintenance effect.And the volatile oil in the Radix Angelicae Sinensis, Flos Caryophylli all has certain inhibitory action to pathogenic bacterium such as staphylococcus aureus, Candida albicans, escherichia coli.These auxiliary Chinese crude drugs have synergism to Radix Sophorae Flavescentis total alkaloids extractum antibiotic, can significantly strengthen the prescription fungistatic effect.In addition, the composition that contains skin care in the prescription can improve the xerosis cutis degree, further alleviates the burden of damaged skin, the care that doubles to skin.Sophora alopecuroide bacteriostatic bath foam is by pure natural plant extraction, the purified effective antibacterial product of pure medicinal plants, be applicable to symptoms such as the xerosis cutis that causes by pathogenic bacterium such as staphylococcus aureus, escherichia coli, Candida albicans, antibacterial, harmful microorganism, comedo and acne, pinta brown patch, it skin is not had any stimulation and have preserve moisture, moisten, the effect of skin-care and beautifying.When this finished product using method is each bathing, extrudes on a small quantity and take in bath, get foam with a spot of water and clean whole body with it then, massage is moments later washed off with clear water.
Description of drawings
Fig. 1 is sophora alopecuroide bacteriostatic bath foam technological process of production figure
The specific embodiment
One embodiment is described in detail in detail below: medical material Cornu Cervi Pantotrichum 1.5kg, the Radix Ginseng 5kg after will cleaning, Radix Angelicae Sinensis 15kg, Flos Caryophylli 15kg pulverize separately become coarse powder.Cornu Cervi Pantotrichum adds ethanol 12kg for the first time with the alcohol heating reflux secondary of concentration 95%, extracts 2 hours, adds ethanol 9kg for the second time and extracts 1.5 hours, merges extracted twice liquid, reclaims ethanol, obtains medicinal liquid 9.5kg and places stand-by; Radix Ginseng adds distilled water 40kg for the first time with distilled water reflux secondary, extracts 2 hours, adds distilled water 30kg for the second time and extracts 1.5 hours, merges extracted twice liquid, and water-bath is concentrated into 27kg, places stand-by; Flos Caryophylli, Radix Angelicae Sinensis extract volatile oil with volatile oil extractor respectively, add distilled water 150kg, and heating and refluxing extraction 8 hours reclaims two kinds of volatile oil of mixing and obtains 8.5kg stand-by (ratio of oil water mixture is 1: 10); The extraction medicinal liquid of mixed volatilization oil and Cornu Cervi Pantotrichum, Radix Ginseng is stirred into herb liquid 45kg then.Again the water-bath of Radix Sophorae Flavescentis total alkaloids liquid is condensed into extractum and gets 2.25kg, joining becomes the Chinese medicine admixing medical solutions in the above-mentioned herb liquid, leave and take stand-by after stirring; The deionized water of measuring 135kg is put into reaction pot, add hydroxyethyl-cellulose 0.9kg, be stirred to dissolving fully, the Chinese medicine admixing medical solutions is added wherein, be stirred to fully evenly, add citric acid 0.21kg again and stirred 5 minutes, begin heating and under agitation slowly add cocoanut fatty acid diethanolamide (6501) 27kg, polyoxyethylenated alcohol sodium sulfate (AES-A) 30kg, sodium lauryl sulphate (k
12) adding Pearl Concentrate 9kg when 18kg is warming up to 75 ℃, be stirred to dissolving fully, be warming up to 80 ℃ and stop heating, insulated and stirred 15 minutes, treat to dissolve fully, deaeration begins to be cooled to below 50 ℃, add acetylbutyrylcellulose (CAB) 15kg, glycerol 24kg and several antiseptic and spice successively, stir after 20 minutes pick test and be finished product after qualified.
Claims (1)
1, the production method of sophora alopecuroide bacteriostatic bath foam, it is characterized in that: Cornu Cervi Pantotrichum, Radix Ginseng, Radix Angelicae Sinensis, four kinds of pulverizing medicinal materials of Flos Caryophylli are become coarse powder, the weight ratio of four kinds of medical materials is 1: 3-4: 10: 10, the Cornu Cervi Pantotrichum alcohol heating reflux secondary of concentration 95%, each ethanol that adds 6-8 times of weight extracted 1-2 hour, merged extracted twice liquid, recovery section ethanol, medicinal liquid is placed stand-by; Radix Ginseng adds the distilled water of 6-8 times of weight with distilled water reflux secondary at every turn, extracts 1-2 hour, merges extracted twice liquid, and it is stand-by that water-bath concentrates placement; Flos Caryophylli, Radix Angelicae Sinensis extract volatile oil respectively, add the distilled water of 8-12 times of weight separately, heating and refluxing extraction 8-9 hour, leave and take volatile oil; Extracting solution mixing and stirring with above-mentioned two kinds of volatile oil and Cornu Cervi Pantotrichum, Radix Ginseng becomes herb liquid then, again the water-bath of Radix Sophorae Flavescentis total alkaloids liquid is condensed into extractum, and joining by the weight of herb liquid 5% becomes the Chinese medicine admixing medical solutions in the herb liquid, leave and take stand-by after stirring; The deionized water of measuring 3 times of weight of Chinese medicine admixing medical solutions is put into reaction pot, the hydroxyethyl-cellulose that adds Radix Sophorae Flavescentis total alkaloids extractum weight 30%-50%, being stirred to fully, the dissolving back adds above-mentioned Chinese medicine admixing medical solutions wherein, be stirred to fully evenly, the citric acid that adds Radix Sophorae Flavescentis total alkaloids extractum weight 8%-12% again stirred 5 minutes, begin to heat and under agitation slowly add the cocoanut fatty acid diethanolamide of 10-15 times of weight of Radix Sophorae Flavescentis total alkaloids extractum, the polyoxyethylenated alcohol sodium sulfate of 12-15 times of weight of Radix Sophorae Flavescentis total alkaloids extractum, the sodium lauryl sulphate of 6-10 times of weight of Radix Sophorae Flavescentis total alkaloids extractum, the Pearl Concentrate that adds 3-5 times of weight of Radix Sophorae Flavescentis total alkaloids extractum when being warming up to 75 ℃, be stirred to dissolving fully, be warming up to 80 ℃ and stop heating, insulated and stirred 15 minutes, treat to dissolve fully, deaeration, begin to be cooled to below 50 ℃, the acetylbutyrylcellulose that adds 5-8 times of weight of Radix Sophorae Flavescentis total alkaloids extractum successively, the glycerol of 10-13 times of weight of Radix Sophorae Flavescentis total alkaloids extractum stirs after 20 minutes pick test and is finished product after qualified.
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| CN2009101756528A CN101658480B (en) | 2009-09-19 | 2009-09-19 | Production method of sophora alopecuroide bacteriostatic bath foam |
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| CN2009101756528A CN101658480B (en) | 2009-09-19 | 2009-09-19 | Production method of sophora alopecuroide bacteriostatic bath foam |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302439A (en) * | 2011-09-15 | 2012-01-04 | 孙淑萍 | Health-care bath foam and preparation method thereof |
| CN102415985A (en) * | 2011-12-12 | 2012-04-18 | 大连创达技术交易市场有限公司 | Body-beautifying Chinese medicine bath powder |
| TWI485243B (en) * | 2012-11-26 | 2015-05-21 | ||
| CN105076252A (en) * | 2015-09-28 | 2015-11-25 | 江苏振宇环保科技有限公司 | Preparation method of tableware disinfectant |
| CN105581922A (en) * | 2016-02-22 | 2016-05-18 | 苏州锐耐洁电子科技新材料有限公司 | Specific skin cleaning liquid for infants |
| CN111437229A (en) * | 2020-05-28 | 2020-07-24 | 赵双 | Shampoo product capable of purifying scalp and improving hair and preparation method thereof |
-
2009
- 2009-09-19 CN CN2009101756528A patent/CN101658480B/en active Active
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302439A (en) * | 2011-09-15 | 2012-01-04 | 孙淑萍 | Health-care bath foam and preparation method thereof |
| CN102302439B (en) * | 2011-09-15 | 2013-01-23 | 孙淑萍 | Health-care bath foam and preparation method thereof |
| CN102415985A (en) * | 2011-12-12 | 2012-04-18 | 大连创达技术交易市场有限公司 | Body-beautifying Chinese medicine bath powder |
| TWI485243B (en) * | 2012-11-26 | 2015-05-21 | ||
| CN105076252A (en) * | 2015-09-28 | 2015-11-25 | 江苏振宇环保科技有限公司 | Preparation method of tableware disinfectant |
| CN105581922A (en) * | 2016-02-22 | 2016-05-18 | 苏州锐耐洁电子科技新材料有限公司 | Specific skin cleaning liquid for infants |
| CN111437229A (en) * | 2020-05-28 | 2020-07-24 | 赵双 | Shampoo product capable of purifying scalp and improving hair and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN101658480B (en) | 2011-09-07 |
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