CN101613506B - 耐高温无卤阻燃电缆护套料及其制备方法 - Google Patents
耐高温无卤阻燃电缆护套料及其制备方法 Download PDFInfo
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- CN101613506B CN101613506B CN2009100601479A CN200910060147A CN101613506B CN 101613506 B CN101613506 B CN 101613506B CN 2009100601479 A CN2009100601479 A CN 2009100601479A CN 200910060147 A CN200910060147 A CN 200910060147A CN 101613506 B CN101613506 B CN 101613506B
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- 239000003063 flame retardant Substances 0.000 title claims abstract description 149
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 143
- 239000000463 material Substances 0.000 title claims abstract description 84
- 229910052736 halogen Inorganic materials 0.000 title claims abstract description 57
- 150000002367 halogens Chemical class 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title abstract description 22
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 215
- 239000000945 filler Substances 0.000 claims abstract description 89
- 229920001971 elastomer Polymers 0.000 claims abstract description 86
- 239000005060 rubber Substances 0.000 claims abstract description 86
- 230000003712 anti-aging effect Effects 0.000 claims abstract description 72
- 239000007822 coupling agent Substances 0.000 claims abstract description 70
- 238000000034 method Methods 0.000 claims abstract description 24
- 230000008569 process Effects 0.000 claims abstract description 18
- 239000000126 substance Substances 0.000 claims abstract description 12
- -1 alkylated diphenylamine compound Chemical class 0.000 claims description 97
- 238000002156 mixing Methods 0.000 claims description 90
- 229920001897 terpolymer Polymers 0.000 claims description 74
- 239000004698 Polyethylene Substances 0.000 claims description 51
- 229920000573 polyethylene Polymers 0.000 claims description 51
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 36
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 36
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 36
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 36
- 239000012188 paraffin wax Substances 0.000 claims description 36
- 239000011701 zinc Substances 0.000 claims description 36
- 229910052725 zinc Inorganic materials 0.000 claims description 36
- 239000000347 magnesium hydroxide Substances 0.000 claims description 34
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 34
- 238000005303 weighing Methods 0.000 claims description 34
- 239000000654 additive Substances 0.000 claims description 31
- 239000006096 absorbing agent Substances 0.000 claims description 24
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical class C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 20
- 230000000996 additive effect Effects 0.000 claims description 19
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 18
- 235000021355 Stearic acid Nutrition 0.000 claims description 17
- 238000001994 activation Methods 0.000 claims description 17
- 238000005469 granulation Methods 0.000 claims description 17
- 230000003179 granulation Effects 0.000 claims description 17
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 17
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 17
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 16
- 239000005977 Ethylene Substances 0.000 claims description 16
- 239000000178 monomer Substances 0.000 claims description 16
- OJOWICOBYCXEKR-KRXBUXKQSA-N (5e)-5-ethylidenebicyclo[2.2.1]hept-2-ene Chemical group C1C2C(=C/C)/CC1C=C2 OJOWICOBYCXEKR-KRXBUXKQSA-N 0.000 claims description 9
- 229940094989 trimethylsilane Drugs 0.000 claims description 9
- BJELTSYBAHKXRW-UHFFFAOYSA-N 2,4,6-triallyloxy-1,3,5-triazine Chemical compound C=CCOC1=NC(OCC=C)=NC(OCC=C)=N1 BJELTSYBAHKXRW-UHFFFAOYSA-N 0.000 claims description 8
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 8
- 229910000077 silane Inorganic materials 0.000 claims description 8
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims description 7
- 235000012204 lemonade/lime carbonate Nutrition 0.000 claims description 7
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical group C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims description 6
- 239000004927 clay Substances 0.000 claims description 6
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 6
- NALFRYPTRXKZPN-UHFFFAOYSA-N 1,1-bis(tert-butylperoxy)-3,3,5-trimethylcyclohexane Chemical compound CC1CC(C)(C)CC(OOC(C)(C)C)(OOC(C)(C)C)C1 NALFRYPTRXKZPN-UHFFFAOYSA-N 0.000 claims description 5
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 5
- 239000012964 benzotriazole Substances 0.000 claims description 5
- 238000003801 milling Methods 0.000 claims description 4
- RYPKRALMXUUNKS-UHFFFAOYSA-N 2-Hexene Natural products CCCC=CC RYPKRALMXUUNKS-UHFFFAOYSA-N 0.000 claims description 3
- DPUXQWOMYBMHRN-UHFFFAOYSA-N hexa-2,3-diene Chemical compound CCC=C=CC DPUXQWOMYBMHRN-UHFFFAOYSA-N 0.000 claims description 3
- ZXDDPOHVAMWLBH-UHFFFAOYSA-N 2,4-Dihydroxybenzophenone Chemical compound OC1=CC(O)=CC=C1C(=O)C1=CC=CC=C1 ZXDDPOHVAMWLBH-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000000779 smoke Substances 0.000 abstract description 3
- 238000004073 vulcanization Methods 0.000 abstract description 3
- 229920002943 EPDM rubber Polymers 0.000 abstract 2
- 230000000979 retarding effect Effects 0.000 abstract 2
- 235000012254 magnesium hydroxide Nutrition 0.000 description 34
- 230000035515 penetration Effects 0.000 description 15
- PRBHEGAFLDMLAL-GQCTYLIASA-N (4e)-hexa-1,4-diene Chemical group C\C=C\CC=C PRBHEGAFLDMLAL-GQCTYLIASA-N 0.000 description 7
- 230000032683 aging Effects 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 150000004820 halides Chemical class 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- DQXBYHZEEUGOBF-UHFFFAOYSA-N but-3-enoic acid;ethene Chemical compound C=C.OC(=O)CC=C DQXBYHZEEUGOBF-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000005038 ethylene vinyl acetate Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 238000010092 rubber production Methods 0.000 description 2
- 206010051246 Photodermatosis Diseases 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- HQQADJVZYDDRJT-UHFFFAOYSA-N ethene;prop-1-ene Chemical group C=C.CC=C HQQADJVZYDDRJT-UHFFFAOYSA-N 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000008845 photoaging Effects 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 239000012815 thermoplastic material Substances 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Organic Insulating Materials (AREA)
- Insulated Conductors (AREA)
Abstract
Description
序号 | 性能指标 | 单位 | 数值 |
11.11.21.3 | 原始机械性能:抗拉强度断裂伸长率撕裂强度 | MPa%N/mm | 12.638010 |
22.12.22.32.4 | 158℃×168h空气箱老化后机械性能:抗拉强度抗拉强度变化率断裂伸长率断裂伸长率变化率 | MPa%%% | 13.24.8350-7.9 |
3 | 热延伸试验(250±3℃,15min,20N/cm2)载荷下伸长率最大冷却后永久变形最大 | %% | 15-1 |
4 | 邵氏硬度 | 度 | 50 |
5 | 氧指数 | - | 32 |
序号 | 性能指标 | 单位 | 数值 |
11.11.21.3 | 原始机械性能:抗拉强度断裂伸长率撕裂强度 | MPa%N/mm | 13.136511 |
22.12.22.32.4 | 158℃×168h空气箱老化后机械性能:抗拉强度抗拉强度变化率断裂伸长率断裂伸长率变化率 | MPa%%% | 13.74.6330-9.6 |
3 | 热延伸试验(250±3℃,15min,20N/cm2)载荷下伸长率最大冷却后永久变形最大 | %% | 100 |
4 | 邵氏硬度 | 度 | 52 |
5 | 氧指数 | - | 33 |
Claims (9)
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CN101613506B true CN101613506B (zh) | 2011-07-20 |
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CN101831115B (zh) * | 2010-04-29 | 2011-12-21 | 江苏远洋东泽电缆股份有限公司 | 舰船纵向高压水密电缆用乙丙橡胶绝缘料及其生产方法 |
CN102617936B (zh) * | 2012-01-11 | 2014-01-01 | 广东信力材料科技有限公司 | 一种无卤阻燃橡胶复合材料的制备方法 |
CN102682870A (zh) * | 2012-03-05 | 2012-09-19 | 安徽江淮电缆集团有限公司 | 一种轨道交通用乙丙胶绝缘防鼠防蚁低烟无卤阻燃直流高压电缆绝缘料 |
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CN103483697A (zh) * | 2013-08-28 | 2014-01-01 | 绿宝电缆(集团)有限公司 | 一种多纳米材料的电缆护套料 |
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CN104893126A (zh) * | 2015-06-19 | 2015-09-09 | 建新赵氏集团有限公司 | 一种耐高温阻燃的三元乙丙橡胶及其制备方法 |
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CN105482272A (zh) * | 2015-12-30 | 2016-04-13 | 合肥星辰电线电缆股份有限公司 | 一种电力电缆用绝缘橡皮 |
CN106065124A (zh) * | 2016-06-12 | 2016-11-02 | 芜湖航飞科技股份有限公司 | 一种船用低烟无卤阻燃电缆护套材料及其制备方法 |
CN106366474A (zh) * | 2016-08-31 | 2017-02-01 | 余姚市楷瑞电子有限公司 | 煤矿用阻燃电缆料 |
CN106928560A (zh) * | 2017-04-17 | 2017-07-07 | 沈阳市新异阻燃材料厂 | 一种阻燃乙丙绝缘橡皮 |
CN108129714A (zh) * | 2017-11-22 | 2018-06-08 | 新宇电缆集团股份有限公司 | 一种环保型防干扰电缆护套料 |
CN109651720A (zh) * | 2018-12-27 | 2019-04-19 | 尚纬股份有限公司 | 一种核反应堆中压电缆用导体屏蔽料及其制备方法 |
CN109651719A (zh) * | 2018-12-27 | 2019-04-19 | 尚纬股份有限公司 | 一种核反应堆中压电缆用可剥离绝缘屏蔽料及其制备方法 |
CN109627610A (zh) * | 2018-12-27 | 2019-04-16 | 尚纬股份有限公司 | 一种海上小型核反应堆电缆用绝缘材料及其制备方法 |
CN109880237A (zh) * | 2019-01-28 | 2019-06-14 | 芜湖航天特种电缆厂股份有限公司 | 耐高温高韧性电缆及其制备方法 |
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CN1261716A (zh) * | 1999-12-24 | 2000-08-02 | 中国科学院上海原子核研究所 | 辐射交联低烟无卤阻燃热收缩电力电缆附件 |
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CN101205339A (zh) * | 2006-12-21 | 2008-06-25 | 无锡江南电缆有限公司 | 电线电缆用乙丙橡皮 |
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