CN101607882A - 一种干法生产硬脂酸盐的工艺及装置 - Google Patents
一种干法生产硬脂酸盐的工艺及装置 Download PDFInfo
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- CN101607882A CN101607882A CNA2009103045060A CN200910304506A CN101607882A CN 101607882 A CN101607882 A CN 101607882A CN A2009103045060 A CNA2009103045060 A CN A2009103045060A CN 200910304506 A CN200910304506 A CN 200910304506A CN 101607882 A CN101607882 A CN 101607882A
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- Prior art keywords
- stearate
- reaction
- reaction vessel
- water
- technology
- Prior art date
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- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 title claims abstract description 23
- 238000005516 engineering process Methods 0.000 title claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 86
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 50
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 16
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000008117 stearic acid Substances 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 229910000765 intermetallic Inorganic materials 0.000 claims abstract description 11
- 230000007246 mechanism Effects 0.000 claims abstract description 9
- 230000009467 reduction Effects 0.000 claims abstract description 8
- 238000009434 installation Methods 0.000 claims abstract description 4
- 239000008367 deionised water Substances 0.000 claims description 22
- 229910021641 deionized water Inorganic materials 0.000 claims description 22
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 12
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 10
- 239000000498 cooling water Substances 0.000 claims description 8
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
- 239000011787 zinc oxide Substances 0.000 claims description 5
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 4
- 239000000920 calcium hydroxide Substances 0.000 claims description 4
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 4
- 150000002500 ions Chemical group 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 claims description 2
- 239000012154 double-distilled water Substances 0.000 claims description 2
- 239000000395 magnesium oxide Substances 0.000 claims description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 2
- 229910000000 metal hydroxide Inorganic materials 0.000 claims description 2
- 150000004692 metal hydroxides Chemical class 0.000 claims description 2
- 229910044991 metal oxide Inorganic materials 0.000 claims description 2
- 150000004706 metal oxides Chemical class 0.000 claims description 2
- 239000011667 zinc carbonate Substances 0.000 claims description 2
- 235000004416 zinc carbonate Nutrition 0.000 claims description 2
- 229910000010 zinc carbonate Inorganic materials 0.000 claims description 2
- UDCHRKDUVGFMLO-UHFFFAOYSA-M calcium magnesium oxygen(2-) hydroxide Chemical compound [OH-].[Ca+2].[O-2].[Mg+2] UDCHRKDUVGFMLO-UHFFFAOYSA-M 0.000 claims 1
- 239000002351 wastewater Substances 0.000 abstract description 9
- 238000005265 energy consumption Methods 0.000 abstract description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 30
- 239000007789 gas Substances 0.000 description 23
- 239000000047 product Substances 0.000 description 21
- 229910052757 nitrogen Inorganic materials 0.000 description 15
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical class [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 8
- 239000008116 calcium stearate Substances 0.000 description 7
- 235000013539 calcium stearate Nutrition 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 238000006073 displacement reaction Methods 0.000 description 5
- 238000012423 maintenance Methods 0.000 description 5
- 239000003643 water by type Substances 0.000 description 5
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 4
- 239000000292 calcium oxide Substances 0.000 description 4
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 4
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 4
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 3
- 235000012254 magnesium hydroxide Nutrition 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000000347 magnesium hydroxide Substances 0.000 description 2
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 2
- 235000019359 magnesium stearate Nutrition 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 238000004065 wastewater treatment Methods 0.000 description 2
- 238000003723 Smelting Methods 0.000 description 1
- -1 Zinic stearas Chemical compound 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- AGXUVMPSUKZYDT-UHFFFAOYSA-L barium(2+);octadecanoate Chemical compound [Ba+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O AGXUVMPSUKZYDT-UHFFFAOYSA-L 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- UQLDLKMNUJERMK-UHFFFAOYSA-L di(octadecanoyloxy)lead Chemical compound [Pb+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O UQLDLKMNUJERMK-UHFFFAOYSA-L 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- IPCXNCATNBAPKW-UHFFFAOYSA-N zinc;hydrate Chemical compound O.[Zn] IPCXNCATNBAPKW-UHFFFAOYSA-N 0.000 description 1
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Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2009103045060A CN101607882B (zh) | 2009-07-17 | 2009-07-17 | 一种干法生产硬脂酸盐的工艺及装置 |
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CN2009103045060A CN101607882B (zh) | 2009-07-17 | 2009-07-17 | 一种干法生产硬脂酸盐的工艺及装置 |
Publications (2)
Publication Number | Publication Date |
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CN101607882A true CN101607882A (zh) | 2009-12-23 |
CN101607882B CN101607882B (zh) | 2012-11-21 |
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CN2009103045060A Active CN101607882B (zh) | 2009-07-17 | 2009-07-17 | 一种干法生产硬脂酸盐的工艺及装置 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106278872A (zh) * | 2016-08-24 | 2017-01-04 | 上海制皂(集团)如皋有限公司 | 干法生产硬脂酸锌的新型生产工艺 |
CN108467340A (zh) * | 2018-06-28 | 2018-08-31 | 湖州市菱湖新望化学有限公司 | 一种固相法生产乙酰丙酮盐的反应装置及其工艺 |
CN110183324A (zh) * | 2019-06-11 | 2019-08-30 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
CN110204435A (zh) * | 2019-06-11 | 2019-09-06 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN2530718Y (zh) * | 2002-01-15 | 2003-01-15 | 上海建筑材料集团新材料有限公司 | 碳化包覆反应釜 |
CN101182291A (zh) * | 2007-12-11 | 2008-05-21 | 王传华 | 一步合成脂肪酸锌盐的清洁合成工艺 |
-
2009
- 2009-07-17 CN CN2009103045060A patent/CN101607882B/zh active Active
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106278872A (zh) * | 2016-08-24 | 2017-01-04 | 上海制皂(集团)如皋有限公司 | 干法生产硬脂酸锌的新型生产工艺 |
CN108467340A (zh) * | 2018-06-28 | 2018-08-31 | 湖州市菱湖新望化学有限公司 | 一种固相法生产乙酰丙酮盐的反应装置及其工艺 |
CN108467340B (zh) * | 2018-06-28 | 2024-04-30 | 湖州市菱湖新望化学有限公司 | 一种固相法生产乙酰丙酮盐的反应装置及其工艺 |
CN110183324A (zh) * | 2019-06-11 | 2019-08-30 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
CN110204435A (zh) * | 2019-06-11 | 2019-09-06 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
WO2020248483A1 (zh) * | 2019-06-11 | 2020-12-17 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
CN110183324B (zh) * | 2019-06-11 | 2021-09-21 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
Also Published As
Publication number | Publication date |
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CN101607882B (zh) | 2012-11-21 |
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Denomination of invention: Technique for producing stearate by dry method and device Effective date of registration: 20170810 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd West Branch Pledgor: Huzhou Linghu Xinwang Chemical Co., Ltd. Registration number: 2017990000736 |
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Denomination of invention: Technique for producing stearate by dry method and device Effective date of registration: 20180731 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd Pledgor: Huzhou Linghu Xinwang Chemical Co., Ltd. Registration number: 2018110000018 |
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Date of cancellation: 20190725 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd Pledgor: Huzhou Linghu Xinwang Chemical Co., Ltd. Registration number: 2018110000018 |
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Denomination of invention: Technique for producing stearate by dry method and device Effective date of registration: 20190730 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd Pledgor: Huzhou Linghu Xinwang Chemical Co., Ltd. Registration number: 2019990000806 |
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Date of cancellation: 20200724 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd. Pledgor: HUZHOU CITY LINGHU XINWANG CHEMICAL Co.,Ltd. Registration number: 2019990000806 |
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Denomination of invention: A process and device for dry production of Stearate Effective date of registration: 20200818 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd. Pledgor: HUZHOU CITY LINGHU XINWANG CHEMICAL Co.,Ltd. Registration number: Y2020990000985 |
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Date of cancellation: 20210816 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd. Pledgor: HUZHOU CITY LINGHU XINWANG CHEMICAL Co.,Ltd. Registration number: Y2020990000985 |
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Denomination of invention: A process and device for producing stearate by dry method Effective date of registration: 20210816 Granted publication date: 20121121 Pledgee: Bank of Huzhou Limited by Share Ltd. Pledgor: HUZHOU CITY LINGHU XINWANG CHEMICAL Co.,Ltd. Registration number: Y2021990000725 |
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