CN101512675A - 纯化方法和所纯化的聚合物 - Google Patents
纯化方法和所纯化的聚合物 Download PDFInfo
- Publication number
- CN101512675A CN101512675A CNA2007800325355A CN200780032535A CN101512675A CN 101512675 A CN101512675 A CN 101512675A CN A2007800325355 A CNA2007800325355 A CN A2007800325355A CN 200780032535 A CN200780032535 A CN 200780032535A CN 101512675 A CN101512675 A CN 101512675A
- Authority
- CN
- China
- Prior art keywords
- solution
- polymer
- chelating agent
- metal chelating
- polythiophene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
- H01B1/12—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances organic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/06—Treatment of polymer solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G61/02—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes
- C08G61/04—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes only aliphatic carbon atoms
- C08G61/06—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes only aliphatic carbon atoms prepared by ring-opening of carbocyclic compounds
- C08G61/08—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes only aliphatic carbon atoms prepared by ring-opening of carbocyclic compounds of carbocyclic compounds containing one or more carbon-to-carbon double bonds in the ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G61/12—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G61/12—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule
- C08G61/122—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from five- or six-membered heterocyclic compounds, other than imides
- C08G61/123—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from five- or six-membered heterocyclic compounds, other than imides derived from five-membered heterocyclic compounds
- C08G61/126—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule derived from five- or six-membered heterocyclic compounds, other than imides derived from five-membered heterocyclic compounds with a five-membered ring containing one sulfur atom in the ring
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
- H01B1/12—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances organic substances
- H01B1/124—Intrinsically conductive polymers
- H01B1/127—Intrinsically conductive polymers comprising five-membered aromatic rings in the main chain, e.g. polypyrroles, polythiophenes
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K71/00—Manufacture or treatment specially adapted for the organic devices covered by this subclass
- H10K71/311—Purifying organic semiconductor materials
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K99/00—Subject matter not provided for in other groups of this subclass
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10K—ORGANIC ELECTRIC SOLID-STATE DEVICES
- H10K85/00—Organic materials used in the body or electrodes of devices covered by this subclass
- H10K85/10—Organic polymers or oligomers
- H10K85/111—Organic polymers or oligomers comprising aromatic, heteroaromatic, or aryl chains, e.g. polyaniline, polyphenylene or polyphenylene vinylene
- H10K85/113—Heteroaromatic compounds comprising sulfur or selene, e.g. polythiophene
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E10/00—Energy generation through renewable energy sources
- Y02E10/50—Photovoltaic [PV] energy
- Y02E10/549—Organic PV cells
Abstract
Description
元素分析 | PHT-MeOH | PHT-DMG |
C | 70.93(71.1) | 70.73(71.1) |
H | 8.32(8.3) | 8.34(8.3) |
S | 18.89(19.0) | 18.17(19.0) |
Ash | 1.1 | 无 |
金属(ppm) | PHT-MeOH | PHT-DMG |
Ni* | 747 | 没有检测到 |
Mg* | 539 | 182 |
Claims (25)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US84155006P | 2006-09-01 | 2006-09-01 | |
US60/841,550 | 2006-09-01 | ||
PCT/US2007/077456 WO2008063731A2 (en) | 2006-09-01 | 2007-08-31 | Purification methods and purified conjugated polymers |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101512675A true CN101512675A (zh) | 2009-08-19 |
CN101512675B CN101512675B (zh) | 2014-02-12 |
Family
ID=39381884
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN200780032535.5A Active CN101512675B (zh) | 2006-09-01 | 2007-08-31 | 纯化方法和所纯化的聚合物 |
Country Status (7)
Country | Link |
---|---|
US (1) | US7671173B2 (zh) |
EP (1) | EP2062267B1 (zh) |
JP (1) | JP5559537B2 (zh) |
KR (1) | KR101428117B1 (zh) |
CN (1) | CN101512675B (zh) |
TW (1) | TWI454494B (zh) |
WO (1) | WO2008063731A2 (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9881712B2 (en) * | 2012-07-20 | 2018-01-30 | Rohm And Haas Electronic Materials Llc | Highly crystalline electrically conducting polymers, methods of manufacture thereof and articles comprising the same |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040254336A1 (en) * | 2003-06-16 | 2004-12-16 | Xiao Steven Shuyong | Methods to purify polymers |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US870326A (en) * | 1907-04-01 | 1907-11-05 | Frank J Tone | Electric furnace. |
US4595749A (en) * | 1984-11-23 | 1986-06-17 | Shell Oil Company | Direct removal of NI catalysts |
WO1994015972A1 (en) * | 1993-01-11 | 1994-07-21 | Idemitsu Kosan Co., Ltd. | Method of purifying styrene polymer |
US6166172A (en) | 1999-02-10 | 2000-12-26 | Carnegie Mellon University | Method of forming poly-(3-substituted) thiophenes |
JP2001196662A (ja) * | 2000-01-12 | 2001-07-19 | Japan Science & Technology Corp | 高純度化ポリチオフェン誘導体から成る光電変換素子用光キャリアー生成および輸送材料薄膜 |
US6602974B1 (en) | 2001-12-04 | 2003-08-05 | Carnegie Mellon University | Polythiophenes, block copolymers made therefrom, and methods of forming the same |
TWI255832B (en) | 2003-06-11 | 2006-06-01 | Ind Tech Res Inst | Method of reducing the photoelectric device current leakage in conjugated polymer and conjugated polymer composition |
CN1253448C (zh) * | 2004-09-29 | 2006-04-26 | 徐良衡 | 一种噻吩类聚合物单体的制备及其聚合方法 |
-
2007
- 2007-08-31 EP EP07871053.0A patent/EP2062267B1/en active Active
- 2007-08-31 JP JP2009526944A patent/JP5559537B2/ja active Active
- 2007-08-31 TW TW096132655A patent/TWI454494B/zh active
- 2007-08-31 US US11/849,220 patent/US7671173B2/en active Active
- 2007-08-31 CN CN200780032535.5A patent/CN101512675B/zh active Active
- 2007-08-31 WO PCT/US2007/077456 patent/WO2008063731A2/en active Application Filing
- 2007-08-31 KR KR1020097006604A patent/KR101428117B1/ko active IP Right Grant
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040254336A1 (en) * | 2003-06-16 | 2004-12-16 | Xiao Steven Shuyong | Methods to purify polymers |
Also Published As
Publication number | Publication date |
---|---|
JP2010502790A (ja) | 2010-01-28 |
US20080132670A1 (en) | 2008-06-05 |
EP2062267A2 (en) | 2009-05-27 |
EP2062267B1 (en) | 2014-01-01 |
WO2008063731A2 (en) | 2008-05-29 |
US7671173B2 (en) | 2010-03-02 |
TWI454494B (zh) | 2014-10-01 |
KR20090051242A (ko) | 2009-05-21 |
WO2008063731A3 (en) | 2008-07-24 |
JP5559537B2 (ja) | 2014-07-23 |
KR101428117B1 (ko) | 2014-08-07 |
CN101512675B (zh) | 2014-02-12 |
TW200833723A (en) | 2008-08-16 |
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