CN101313673A - Corrosion protection preservative fluid for reliquiae, preparing method and application of the same - Google Patents
Corrosion protection preservative fluid for reliquiae, preparing method and application of the same Download PDFInfo
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- CN101313673A CN101313673A CNA2007100415654A CN200710041565A CN101313673A CN 101313673 A CN101313673 A CN 101313673A CN A2007100415654 A CNA2007100415654 A CN A2007100415654A CN 200710041565 A CN200710041565 A CN 200710041565A CN 101313673 A CN101313673 A CN 101313673A
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Abstract
The invention relates to a body anti-corrosive preservation solution. The raw materials in percentage by weight of the preservation solution are: 10 to 40 percent of glycerol, 10 to 70 percent of ethanol, 1 to 20 percent of metacetonic acid, 0.1 to 20 percent of hexamethylene tetramine, 0.2 to 10 percent of 5-chloro-2-methyl-4-isothiazoline-3-ketone, 0.1 to 1 percent of peppermint oil and the balance being water. The application mode of the preservation solution comprises the following steps: the anti-corrosive preservation solution is injected into the digestive system of a body from the oral cavity or the nose and the throat of the body; the anti-corrosive preservation solution is injected through an aortic arch, a brachial artery or a femoral artery; and the anti-corrosive preservation solution can also be used to wipe the surface of a body by a tampon dipped in the preservation solution. The body anti-corrosive preservation solution is nontoxic and harmless to an operator and is easy to operate; moreover, the preservation solution has no influence on the environment and excellent anti-corrosive effects, and can ensure that a body maintains a natural state and softness in a natural state (at room temperature) for 5 to 12 days. In addition, the preservation solution can be used repeatedly and has a simple preparing method, easily obtained raw materials and strong maneuverability; moreover, the preservation solution has convenient practical application and is propitious to popularize and use.
Description
[technical field]
The present invention relates to the preservation technical field of human or animal body, specifically, is that a kind of Gentle Repose is preserved liquid and its production and application.
[background technology]
People's living or death is the natural law.For various reasons, people often need the deceased's remains are kept several days or a period of time, and this has just related to the problem that Gentle Repose is preserved.Be exactly aspect zooscopy, also have pair zoological specimens to carry out the problem of anticorrosion preservation.
Existing Gentle Repose is preserved technology, and traditional anticorrosion means are promptly arranged, and also has to use preservative to carry out anticorrosion preservation.Some place is subjected to condition restriction, has to still to use formalin, or based on the mixing preservative of formalin; The preservative that contains formalin less or do not contain formalin has then been used in some places or area, but contains more inorganic peroxide (as hydrogen peroxide) and/or organic peroxide (as Peracetic acid) in preservative.The shortcoming of these products is obvious: formalin has toxicity, and people's respiratory system is had spread effect, can be carcinogenic, also pollute the environment, and forbidden by many countries and regions; And inorganic peroxide and organic peroxide also have spread effect to skin, make skin exfoliation, colour of skin bleaching or produce gas evaporation, make antiseptic effect undesirable.
In disclosed patent documentation, the introduction of Gentle Repose composition is arranged.But, find that it has advantage, but the deficiency of its existence is also very obvious through analysis and investigation to existing product.Such as, because its component itself makes product still have certain toxicity or excitant, make antiseptic operation quite careful, and the remains after using are easy to generate phenomenons such as flatulence, skin bleaching, decortication, internal organ blackout.The existence of these problems will limit the promotion and application of these anticorrosive composites.
[summary of the invention]
The objective of the invention is to overcome the deficiencies in the prior art, a kind of multi-functional, high efficiency, environment-friendly type are provided, nontoxic to the operator, to the well also reusable antiseptic preserving fluid of Gentle Repose preservation effect; Another object of the present invention provides a kind of preparation method of described antiseptic preserving fluid; A further object of the present invention is that a kind of new application method of described antiseptic preserving fluid is provided.
For achieving the above object, Gentle Repose of the present invention is preserved liquid and is contained glycerine, ethanol, propionic acid, hexa, 5 chloro-2-methyl-4-isothiazoline-3 ketone, peppermint oil, and the percent by volume of its raw material is:
Glycerine 10～40%,
Ethanol 10～70%,
Propionic acid 1～20%,
Hexa 0.1～20%,
5 chloro-2-methyl-4-isothiazoline-3 ketone 0.2～10%,
Peppermint oil 0.1～1%,
Water is added into total amount.
The percent by volume of described raw material is:
Glycerine 15～20%, ethanol 40～60%, propionic acid 1～5%, hexa 0.5～3%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.2～1%, peppermint oil 0.2%, all the other are water.
For realizing purpose of the present invention, the preparation method that Gentle Repose of the present invention is preserved liquid may further comprise the steps:
(1) press the raw material percent by volume---glycerine 15～20%, ethanol 40～60%, propionic acid 1～5%, hexa 0.5～3%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.2～1%, peppermint oil 0.2%---glycerine is sneaked in the ethanol, fully stirring, make its even mixing, is to be first liquid;
(2) earlier hexa, 5 chloro-2-methyl-4-isothiazoline-3 ketone being dissolved in the distilled water by the raw material percent by volume, adding propionic acid again and fully stir, make its even mixing, is to be second liquid;
(3) first liquid and second liquid are mixed, fully stir, drip peppermint oil, mix, promptly get Gentle Repose of the present invention and preserve liquid.
Gentle Repose of the present invention is preserved the raw material that liquid adopts: do not have poisonous and harmful and the strong material of excitant in glycerine, ethanol, propionic acid, hexa, 5 chloro-2-methyl-4-isothiazoline-3 ketone, the peppermint oil.
For example, glycerine is widely used in the clinical treatment preparation, also can be used as food additives simultaneously.When glycerine uses as auxiliary material or food additives, it is generally acknowledged no ill-effect, nontoxic, non-stimulated.Glycerol concentration＜20% o'clock can be used as antibiotic antiseptic, and glycerol concentration≤30% o'clock can be used as softening agent, also can be used as humectant.
The ethanol that the present invention adopts, use can be made antibiotic antiseptic as solution, and the local ethanolic solution that uses can be made promoter and disinfectant.Usually, the ethanolic solution of 〉=10% concentration uses as antibiotic antiseptic, and the ethanolic solution of 60～90% concentration uses as disinfectant, and antibacterial activity adopts the ethanolic solution of 60～95 concentration better, and it also has bactericidal action simultaneously, and its optium concentration is 70%.
The propionic acid that the present invention adopts, belong to acid preservative, all kinds of moulds, aerobic sporebearing bacilli or gram-Negative bacillus there is stronger inhibitory action, to the mushroom that can cause that food is clamminess, fine as the Bacillus subtillis fungistatic effect, and its growth to yeast when mould fungus inhibition is grown does not have influence substantially.Propionic acid is the normal composition of food, also is the normal intermediate of body metabolism, and propionic acid is easily absorbed by digestive system, and no cumulative bad is not discharged with urine, and it can be combined into succinate (ester) with coacetylase and participate in tricarbonic acid cycle metabolism generation carbonic acid gas and water.According to research reports, there are not toxicity in propionic acid and its esters.
The hexa that the present invention adopts is the colourless crystallization material, is medically using as the urinary tract disinfectant, and it runs into aciduria can decompose a spot of formaldehyde of generation, thereby kills the bacterium in the urinary tract.
5 chloro-2-methyl-4-isothiazoline-3 ketone that the present invention adopts is a kind of broad-spectrum mould inhibitor and anti-algae agent, pH value be 3.5～9.5 times effective, no foaminess, to the least concentration of nearly all mould, bacterium for being 1～9 milligram of (mg)/L.This material is synthetic by Profilin, thereby suppresses the synthetic of microbial cell film.
The peppermint oil that the present invention adopts is taken as additive as spices and uses.
From above introduction as can be seen, there are not excitant strong, harmful inorganic peroxide and organic peroxide in the material that the present invention uses, more unharmful materials such as formalin to human and environment to skin.Antiseptic preserving fluid of the present invention can make remains at room temperature, in 5～12 days, keep being stale-proof, meet the funeral custom of China substantially, also can satisfy the specific (special) requirements that the part origin of an incident causes.
For realizing purpose of the present invention, Gentle Repose of the present invention is preserved the anticorrosion preservation that liquid can be applicable to remains, also can be applied to zoological specimens anticorrosion preservation within a certain period of time.
Application mode of the present invention is:
(1) pours into antiseptic preserving fluid 300-500 milliliter from the remains oral cavity or by the nasopharynx larynx, putrefactive digestive system is carried out the preservative treatment of emphasis;
(2) the sustainer arc by remains, or arteria brachialis, or femoral artery injection antiseptic preserving fluid 500-1000 milliliter carry out preservative treatment by hematological system to the whole body of remains;
(3) soak into antiseptic preserving fluid with cotton balls the whole body of remains is smeared wiping, carry out the preservative treatment on surface.
So the principle of using is:
The first, the most concentrated place of bacterium is oral cavity and digestive system in the human body, and after the people died, because the bacterium in the digestive system is many especially, corrupt here was the fastest, therefore, and must be to carrying out the emphasis preservative treatment here.
The second, after the people died, because vascular nutrition is abundant, bacterium can here grow in a large number, breed, because hematological system spreads all over whole body, made the rotten change of remains easily, therefore, and also must be to carrying out the emphasis preservative treatment here.
Three, the whole body to remains that if can assist is smeared the wiping antiseptic preserving fluid, can kill virus to the remains surface, makes the remains surface keep soft, moistening, natural.
The advantage that a kind of Gentle Repose of the present invention is preserved liquid and its production and application is:
(1) provide a kind of nontoxic to the operator, environment is not had influence, and maneuverable antiseptic preserving fluid.
(2) be a kind of multi-functional, high efficiency antiseptic preserving fluid, make remains can be under nature (under the room temperature 5-12 days) anticorrosion, and keep nature, softness, not stiff.
(3) this antiseptic preserving fluid can repeatedly use remains according to the time that the remains needs are preserved.
(4) preparation method is easy, and is workable.
(5) practical application is convenient, is convenient to promote the use of.
[embodiment]
The preparation manipulation method that below provides Gentle Repose of the present invention to preserve liquid, and the some embodiment in research, experiment and enforcement.
The preparation method that Gentle Repose of the present invention is preserved liquid is:
According to the raw material percent by volume
(1) using glassware, glycerine is sneaked in the ethanol, fully stir, make its even mixing, is to be first liquid, places on one side;
(2) using glassware, earlier hexa, 5 chloro-2-methyl-4-isothiazoline-3 ketone are dissolved in the distilled water, add propionic acid again and fully stir, make its even mixing, is to be second liquid;
(3) first liquid and second liquid are mixed, fully stir, drip peppermint oil, mix, promptly get Gentle Repose of the present invention and preserve liquid.
Embodiment 1
The percent by volume of described raw material is:
Glycerine 10%, ethanol 30%, propionic acid 1%, hexa 0.5%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.5%, peppermint oil 0.1%, all the other are water.
Embodiment 2
The percent by volume of described raw material is:
Glycerine 15%, ethanol 40%, propionic acid 3%, hexa 1%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 1%, peppermint oil 0.2%, all the other are water.
Embodiment 3
The percent by volume of described raw material is:
Glycerine 20%, ethanol 50%, propionic acid 5%, hexa 0.5%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.5%, peppermint oil 0.1%, all the other are water.
Embodiment 4
The percent by volume of described raw material is:
Glycerine 40%, ethanol 32%, propionic acid 20%, hexa 0.5%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.5%, peppermint oil 1%, all the other are water.
Embodiment 5
The percent by volume of described raw material is:
Glycerine 10%, ethanol 51%, propionic acid 3%, hexa 20%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 10%, peppermint oil 0.1%, all the other are water.
Embodiment 6
Inject the observation that antiseptic preserving fluid of the present invention carries out by AA chicken to death:
Embodiment 7
By the AA chicken of death being injected the paired observation that Shen dragon board preservative series of products carry out:
Embodiment 8
The observation that the AA chicken of not injecting preservative after the death is carried out:
Embodiment 9
The experiment 1 that remains are done.The woman, three months death times.
(1) pours into antiseptic preserving fluid 300-500 milliliter from the oral cavity with by the nasopharynx larynx;
(2) by sustainer arc injection antiseptic preserving fluid 500-1000 milliliter;
(3) soak into antiseptic preserving fluid with cotton balls the whole body of remains is smeared wiping.
Experimental period: (remains take out in one day and begin to do experiment) 8 day 7 night (4 days-April 11 April in 2007)
Parking environment: indoor.Temperature 18-22 ℃, humidity 60-90%.
The result: profile is observed: the chest belly is flat flat and neat, does not have protuberance, and belly " corpse is green " is almost all decorporated;
Anatomic observation: the fresh odorless of internal organ each several part.
Embodiment 10
The experiment 2 that remains are done.The man, three months death times.
(1) pours into antiseptic preserving fluid 300-500 milliliter from the oral cavity with by the nasopharynx larynx;
(2) by sustainer arc injection antiseptic preserving fluid 500-1000 milliliter;
(3) soak into antiseptic preserving fluid with cotton balls the whole body of remains is smeared wiping.
Experimental period: (remains take out in one day and begin to do experiment) 12 day 11 night (12 days-April 23 April in 2007)
Parking environment: indoor.12-17 day in April, 20 ℃ of temperature, humidity 82%;
April 18,22 ℃ of temperature;
April 19,25 ℃ of temperature, humidity 50%;
The morning-23 day morning in April 20,30 ℃ of temperature, humidity 49%.
The result: profile is observed: belly is flat flat, does not have protuberance, and belly " corpse is green " is almost all decorporated;
Anatomic observation: each organ of internal organ is complete, fresh odorless.
Embodiment 11
The experiment 3 that remains are done.The man, one day death time.
(1) pours into antiseptic preserving fluid 300-500 milliliter from the oral cavity with by the nasopharynx larynx;
(2) by sustainer arc injection antiseptic preserving fluid 500-1000 milliliter;
(3) soak into antiseptic preserving fluid with cotton balls the whole body of remains is smeared wiping.
Experimental period: 3 days (-27 days on the 25th April in 2007)
Parking environment: indoor.Temperature 18.5-20 ℃,
The result: profile is observed: no any unusual, because of family members are satisfied, do not dissect again.
Embodiment 12
The experiment 4 that remains are done.Lung cancer patient, the woman, dead 100 days, corpse was shrivelled, the poor quality.
(1) pours into antiseptic preserving fluid 300-500 milliliter from the oral cavity with by the nasopharynx larynx;
(2) by sustainer arc injection antiseptic preserving fluid 500-1000 milliliter;
(3) soak into antiseptic preserving fluid with cotton balls the whole body of remains is smeared wiping.
Experimental period: (remains take out and begin to do experiment two days later) 7 days (26 days-May 2 April in 2007)
Parking environment: indoor.Temperature 20-30 ℃ (wherein 30 ℃ two days), humidity 79-47%;
The result: profile is observed: the chest belly is flat flat, does not have protuberance;
Anatomic observation: each organ of internal organ is more complete, odorless, and two lungs have the black powder lump, the intestines wall
A plurality of lumps are also arranged, and other organ is better.
Embodiment 13
The experiment 5 that remains are done.Intend being hepatocarcinoma patient, the man, dead four months, corpse whole body blackout, belly has the stitching edge of a knife, the poor quality.
(1) pours into antiseptic preserving fluid 300-500 milliliter from the oral cavity with by the nasopharynx larynx;
(2) by sustainer arc injection antiseptic preserving fluid 500-1000 milliliter;
(3) soak into antiseptic preserving fluid with cotton balls the whole body of remains is smeared wiping.
Experimental period: (remains take out and begin to do experiment two days later) 7 days (26-May 2 April)
Parking environment: indoor.Temperature 20-33 ℃ (wherein 33 ℃ two days), humidity 79-47%;
The result: profile is observed: the chest belly is flat flat, does not have protuberance; Dissect whole health odorless.
Gentle Repose of the present invention is preserved liquid through the graduate check of Shanghai City preventive medicine, and assay and evaluation are:
One, acute oral toxicity test: the nontoxic level in true border.
Two, acute skin irritation test: belong to nonirritant.
Gentle Repose of the present invention is preserved the detection of liquid through central laboratory of Shanghai Mucun Biotechnology Co., Ltd. employing inhibition zone method, and testing result is:
Bacterium inhibition zone (mm): 43;
Mould inhibition zone (mm): 0.
Claims (7)
1, a kind of Gentle Repose is preserved liquid, it is characterized in that contain glycerine, ethanol, propionic acid, hexa, 5 chloro-2-methyl-4-isothiazoline-3 ketone, peppermint oil, its raw material percent by volume is:
Glycerine 10～40%,
Ethanol 10～70%,
Propionic acid 1～20%,
Hexa 0.1～20%,
5 chloro-2-methyl-4-isothiazoline-3 ketone 0.2～10%,
Peppermint oil 0.1～1%,
Water is added into total amount.
2, Gentle Repose according to claim 1 is preserved liquid, it is characterized in that, the percent by volume of described raw material is: glycerine 15～20%, ethanol 40～60%, propionic acid 1～5%, hexa 0.5～3%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.2～1%, peppermint oil 0.2%, all the other are water.
3, a kind of Gentle Repose is preserved the preparation method of liquid, it is characterized in that, may further comprise the steps:
(1) press the raw material percent by volume---glycerine 15～20%, ethanol 40～60%, propionic acid 1～5%, hexa 0.5～3%, 5 chloro-2-methyl-4-isothiazoline-3 ketone 0.2～1%, peppermint oil 0.2%---glycerine is sneaked in the ethanol, fully stirring, make its even mixing, is to be first liquid;
(2) earlier hexa, 5 chloro-2-methyl-4-isothiazoline-3 ketone being dissolved in the distilled water by the raw material percent by volume, adding propionic acid again and fully stir, make its even mixing, is to be second liquid;
(3) first liquid and second liquid are mixed, fully stir, drip peppermint oil, mix, promptly get Gentle Repose of the present invention and preserve liquid.
4, a kind of Gentle Repose as claimed in claim 1 is preserved liquid, the application on remains and zoological specimens.
5, Gentle Repose according to claim 4 is preserved the application of liquid, it is characterized in that, the mode that described antiseptic preserving fluid is used is:
(1) from the remains oral cavity or by the nasopharynx larynx antiseptic preserving fluid is poured into digestive system;
(2) the sustainer arc by remains, or arteria brachialis, or femoral artery injection antiseptic preserving fluid;
(3) soak into antiseptic preserving fluid with cotton balls the remains whole body is smeared wiping.
6, Gentle Repose according to claim 4 is preserved the application of liquid, it is characterized in that, the mode that described antiseptic preserving fluid is used is:
(1) from the remains oral cavity or by the nasopharynx larynx antiseptic preserving fluid is poured into digestive system;
(2) the sustainer arc by remains, or arteria brachialis, or femoral artery injection antiseptic preserving fluid.
7, according to claim 5, or the application of 6 described Gentle Reposes preservation liquid, it is characterized in that the mode that described antiseptic preserving fluid is used is:
(1) from the remains oral cavity or the amount that pours into the antiseptic preserving fluid of digestive system by the nasopharynx larynx be 300～500 milliliters;
(2) the sustainer arc by remains, or arteria brachialis, or the amount of the antiseptic preserving fluid of femoral artery injection is 500～1000 milliliters.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2007100415654A CN101313673B (en) | 2007-06-01 | 2007-06-01 | Corrosion protection preservative fluid for reliquiae, preparing method and application of the same |
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| CN2007100415654A CN101313673B (en) | 2007-06-01 | 2007-06-01 | Corrosion protection preservative fluid for reliquiae, preparing method and application of the same |
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| CN101878755A (en) * | 2010-07-06 | 2010-11-10 | 苏州博克精细化学品有限公司 | Shampoo for body preservation |
| CN101889568A (en) * | 2010-07-06 | 2010-11-24 | 苏州博克精细化学品有限公司 | Bath lotion for preservation of remains |
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| CN1172589C (en) * | 2000-09-28 | 2004-10-27 | 上海遗体防腐研究所 | Reconversion method for putrefactive cadaver |
| CN1732775A (en) * | 2004-08-10 | 2006-02-15 | 任祖翰 | Composition for short-term remains preservation, its preparation process and application |
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| CN102175496B (en) * | 2011-01-21 | 2013-04-03 | 哈尔滨格林标本技术开发有限公司 | Formaldehyde-free fixative for tissue sample |
| CN102175496A (en) * | 2011-01-21 | 2011-09-07 | 哈尔滨格林标本技术开发有限公司 | Formaldehyde-free fixative for tissue sample |
| CN105010303A (en) * | 2015-07-10 | 2015-11-04 | 毕爱胜 | Corruption remains restoring method |
| EP3542627A1 (en) * | 2018-03-23 | 2019-09-25 | Soto Rodino, Ramon Angel | Composition for preservation of corpses, method of obtaining said composition and its use |
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