CN101214090A - Composite filter tip adsorption material and preparation and application thereof - Google Patents
Composite filter tip adsorption material and preparation and application thereof Download PDFInfo
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- CN101214090A CN101214090A CNA200810058011XA CN200810058011A CN101214090A CN 101214090 A CN101214090 A CN 101214090A CN A200810058011X A CNA200810058011X A CN A200810058011XA CN 200810058011 A CN200810058011 A CN 200810058011A CN 101214090 A CN101214090 A CN 101214090A
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- filter tip
- composite filter
- adsorption material
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Abstract
The invention discloses complex filter tip adsorption material, a preparation method and application thereof. A root, a tuber, a bulb or a corm of a plant are selected to be made into fine particles of 40-60 mesh sieves after being cleaned, dried, wet-steamed, steam-dried and grinded. The particles are added in a filter element to obtain binary composite filter tip. With the specific internal spatial structure of the plant root and the stem, the invention can selectively filter and absorb harmful components in flue gas to improve the cigarette safety. At the same time, because the plant root and the stem contain ketones and saponin materials, the flue gas can be organically resolved in smoke fragrant components when flowing through the filter tip. The richness of the smoke fragrant is increased and the suction quality is improved. The material has the advantages of safety, environmental protection, degradable performance, simple preparation process, low cost and good application prospect.
Description
Technical field
The invention belongs to the cigarette material preparing technical field, be specifically related to a kind of sorbing material that is used for cigarette composite filter tip.Simultaneously, the invention still further relates to the preparation method and the application of this sorbing material.
Background technology
The sixties in 20th century cigarette filter appearance, effectively reduce tar content in cigarette.Filter tip is that to the contribution that reduces harmful components such as coke tar in cigarette, nicotine filter stick is to the granule phase substance generation selective filter in the flue gas, flue gas enters the oral cavity by filter tip during cigarette smoking, granule phase substance in the flue gas is with after the filter fiber tow contacts, and part can be adsorbed and can not turn back in the air-flow again.In the prior art, in order further to strengthen filtration, the adsorption function of filter tip, some have bigger serface more options, the material of strong adsorption capacity, and for example active carbon adds in the filter tow, forms composite filter tip.But this composite filter tip is in the selective absorption harmful ingredients in flue gas, and the loss that flue gas moisture and some flavor components are caused is also bigger, thereby flavor quality of cigarette is exerted an adverse impact.Therefore, development NEW TYPE OF COMPOSITE filter tip adsorption material overcomes these problems, just becomes the focus of production of cigarettes field research and development.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of NEW TYPE OF COMPOSITE filter tip adsorption material is provided, when guaranteeing filter effect, improve cigarette odor-absorbing, improve the comfortableness of suction.
Another object of the present invention is to provide a kind of method for preparing described sorbing material.
The present invention also aims to provide the application of described sorbing material in the preparation cigarette filter.
Technical scheme of the present invention is based on following understanding: plant is expanded, contain rich nutrient substances in the root of meat, stem, and active component comprises flavonoids, carbohydrate, saponin class, alkaloids etc.The verified meeting of these compositions produces positive role to the improvement of cigarette quality.
Purpose of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight.
A kind of composite filter tip adsorption material is characterized in that: with piece root, stem tuber, bulb or the bulb of plant through clean, dry, steam wet, steam drying, pulverizing after, made the fine particle of 40 orders～60 mesh sieves.
Described composite filter tip adsorption material is made by following method:
1, piece root, stem tuber, bulb or the bulb of plant are cleaned, removed impurity such as silt, the section back is standby;
2, raw material does not have obvious moisture vestige through natural drying or with oven drying to surface;
3, dry good raw material steams 5～15 minutes with 100 ℃～150 ℃ steam, with removal bad smell wherein, place 2～5 hours at normal temperatures after, add wet process with steam;
4, with 300 ℃～400 ℃ superheat steam drying raw material, controlling its final moisture content is 10%～15%;
5, with after the raw material pulverizing, cross 40 orders～60 mesh sieves, promptly obtain required composite filter tip adsorption material.
The concrete application of described composite filter tip adsorption material: before the filter tow moulding, described composite filter tip adsorption material is sprinkling upon on the filter core equably, makes the composite particles filter stick; Composite particles filter stick and conventional filter element filtering rod are carried out compound, make the binary composite filter tip.
The addition of this sorbing material is that 5～50mg/ props up, and wherein preferred 15～35mg/ props up, best results be that 25mg/ props up.
The present invention has following advantage with respect to prior art:
1, the binary composite filter tip that uses this composite filter tip adsorption material to make can improve cigarette odor-absorbing effectively, improves the comfortableness of suction;
2, can improve the adsorption effect of composite filter tip pointedly, improve the cigarette security harmful components;
3, this sorbing material safety, environmental protection, degradable can be accomplished " zero-emission ";
The specific embodiment
Below in conjunction with embodiment and experimental example the present invention is described in further detail, but they are not limitation of the invention.
Embodiment 1
Prepare a kind of composite filter tip adsorption material, Dioscoreaceae plant Chinese yam is cleaned, remove impurity such as silt, the section back is standby; The yam slice that cuts was placed under the sunlight airing 12 hours, make its surperficial moisture drying, then yam slice is steamed 15 minutes with 100 ℃ steam, remove the bad smell in the Chinese yam, and place 2 hours again after steam humidification is handled, with 300 ℃ superheat steam drying yam slice, its internal structure is improved, and control its final moisture content in 10%～15% scope.At last yam slice is ground into fine particle, and crosses 40 mesh sieves, promptly obtain required composite filter tip adsorption material.
Embodiment 2
Repeat embodiment 1, following difference is arranged: yam slice steams 5 minutes with 150 ℃ steam, and places 5 hours.
Embodiment 3
Repeat embodiment 1, following difference is arranged: with 350 ℃ superheat steam drying yam slice.
Embodiment 4
Repeat embodiment 1, following difference is arranged: with 400 ℃ superheat steam drying yam slice.
Embodiment 5
Repeat embodiment 1, following difference is arranged: yam slice is pulverized the back and is crossed 50 mesh sieves.
Embodiment 6
Repeat embodiment 1, following difference is arranged: yam slice is pulverized the back and is crossed 60 mesh sieves.
Embodiment 7～19
Repeat embodiment 1, following difference arranged: raw material be selected from respectively radish, yam bean, chestnut, sweet potato, cassava, fragrant taro, goa bean, rhizoma Gastrodiae, the tuber of pinellia, lily, the bulb of fritillary, arrowhead and water chestnut.
Experimental example 1
(1) with common diacetate fiber moulding, filter stick length 120mm wherein, resistance to suction 360mmH
2O, forming paper air permeability 10000CU makes " white rod ";
(2) the described method of embodiment is prepared novel filter tip adsorption material (different raw materials see Table 1), the ratio of propping up in 25mg/ is added, and makes " black rod ", filter stick length 120mm wherein, resistance to suction 360mmH
2O, forming paper air permeability 10000CU;
The different absorption of table 1 examples of materials
| Example | Adopt plant | The source | Use the position | Addition (mg/ props up) | Remarks |
| Example one | Chinese yam | Dioscoreaceae | The piece root | 25 | |
| Example two | Radish | The Cruciferae Rhaphanus | The piece root | 25 | |
| Example three | Yam bean | The pulse family yam bean belongs to | The piece root | 25 | |
| Example four | The ground chestnut | The pulse family Root of Fortune Apios belongs to | The piece root | 25 | |
| Example five | Sweet potato | The Convolvulaceae sweet potato genus | The piece root | 25 | |
| Example six | Cassava | The Euphorbiaceae cassava | The piece root | 25 | |
| Example seven | Fragrant taro | The Araeceae taro belongs to | The piece root | 25 | |
| Example eight | Goa bean | The pulse family goa bean belongs to | The piece root | 25 | |
| Example nine | Rhizoma Gastrodiae | The orchid family | Stem tuber | 25 | |
| Example ten | The tuber of pinellia | Araeceae | Stem tuber | 25 | |
| Example 11 | Lily | The Liliaceae lilium | Bulb | 25 | |
| Example 12 | The bulb of fritillary | Liliaceae | Bulb | 25 | |
| Example 13 | Arrowhead | The Alismataceae arrowhead belongs to | Bulb | 25 | |
| Example 14 | Water chestnut | The Cyperaceae Eleocharis | Bulb | 25 |
(3) above-mentioned two types mouth rod is processed with composite molding machine, select forming paper air permeability 10000CU for use, make the binary composite filter tip, cut back (all six) filter tip total length 20mm, " white rod ", " black rod " respectively account for 10mm, and wherein " white rod " is positioned at the lip end, " black rod " is positioned at the plume end;
(4) select the 200CU tipping paper for use,, make cigarette sample, carry out the test of different material source sorbing material with red certain the brand pipe tobacco of group that converges.
(5) according to the red sample standard of smokeing panel test of converging, have 19 judging panels each sample is carried out sensory evaluation and marking.Statistics score value (the results are shown in Table 2) shows that with respect to improving all have in various degree in the same old way, wherein the action effect of example six (cassava), example eight (goa bean), example ten (tuber of pinellia) is particularly evident aspect organoleptic quality for each sample.
The different sorbing material sample of table 2 organoleptic quality score contrast table
| Sample | Gloss (5) | Fragrance (32) | Harmony (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| To in the same old way | 5.0 | 30.2 | 5.3 | 10.0 | 18.2 | 22.3 | 91.0 |
| Example one | 5.0 | 30.4 | 5.3 | 10.2 | 18.2 | 22.3 | 91.4 |
| Example two | 5.0 | 30.5 | 5.3 | 10.1 | 18.2 | 22.1 | 91.2 |
| Example three | 5.0 | 30.3 | 5.3 | 10.2 | 18.3 | 22.4 | 91.5 |
| Example four | 5.0 | 30.3 | 5.3 | 10.3 | 18.3 | 22.3 | 91.5 |
| Example five | 5.0 | 30.2 | 5.3 | 10.1 | 18.2 | 22.3 | 91.1 |
| Example six | 5.0 | 30.7 | 5.3 | 10.2 | 18.3 | 22.4 | 91.9 |
| Example seven | 5.0 | 30.5 | 5.3 | 10.3 | 18.1 | 22.3 | 91.5 |
| Example eight | 5.0 | 30.7 | 5.3 | 10.4 | 18.3 | 22.2 | 91.9 |
| Example nine | 5.0 | 30.4 | 5.3 | 10.3 | 18.2 | 22.3 | 91.5 |
| Example ten | 5.0 | 30.8 | 5.3 | 10.3 | 18.3 | 22.5 | 92.2 |
| Example 11 | 5.0 | 30.2 | 5.3 | 10.3 | 18.3 | 22.4 | 91.5 |
| Example 12 | 5.0 | 30.6 | 5.3 | 10.2 | 18.3 | 22.3 | 91.7 |
| Example 13 | 5.0 | 30.5 | 5.3 | 10.2 | 18.1 | 22.2 | 91.3 |
| Example 14 | 5.0 | 30.5 | 5.3 | 10.3 | 18.1 | 22.4 | 91.6 |
Experimental example 2
On experimental example 1 basis, example six samples (cassava) are carried out the gradient test, sample design sees Table 3.
Test of table 3 sample gradient and organoleptic quality score contrast table
| Sample | Adding proportion (mg/ props up) | Gloss (5) | Fragrance (32) | Harmony (6) | Assorted gas (12) | Excitant (20) | Pleasant impression (25) | Add up to (100) |
| To in the same old way | 0 | 5.0 | 30.2 | 5.3 | 10 | 18.2 | 22.3 | 91.0 |
| Gradient 1 | 5 | 5.0 | 30.3 | 5.3 | 10.2 | 18.3 | 22.2 | 91.3 |
| Gradient 2 | 15 | 5.0 | 30.4 | 5.3 | 10.2 | 18.3 | 22.3 | 91.5 |
| Gradient 3 | 25 | 5.0 | 30.7 | 5.3 | 10.2 | 18.3 | 22.4 | 91.9 |
| Gradient 4 | 35 | 5.0 | 30.4 | 5.3 | 10.2 | 18.3 | 22.4 | 91.6 |
| Gradient 5 | 45 | 5.0 | 30.3 | 5.3 | 10.2 | 18.3 | 22.3 | 91.4 |
| Gradient 6 | 50 | 5.0 | 30.3 | 5.3 | 10.2 | 18.2 | 22.3 | 91.3 |
Having 17 judging panels' participation smokes panel test.Statistics smoking result (seeing Table 3), showing preferable sphere of action is that 15mg～35mg/ props up, selecting addition is that 25mg/ props up optimum 9 judging panels that have.
Claims (7)
1. composite filter tip adsorption material is characterized in that: with piece root, stem tuber, bulb or the bulb of plant through clean, dry, steam wet, steam drying, pulverizing after, made the fine particle of 40 orders～60 mesh sieves.
2. prepare the method for the described composite filter tip adsorption material of claim 1, form by following steps:
(1) piece root, stem tuber, bulb or the bulb of plant are cleaned, removed impurity such as silt, the section back is standby;
(2) raw material does not have obvious moisture vestige through natural drying or with oven drying to surface;
(3) dry good raw material steams 5～15 minutes with 100 ℃～150 ℃ steam, with removal bad smell wherein, place 2～5 hours at normal temperatures after, add wet process with steam;
(4) with 300 ℃～400 ℃ superheat steam drying raw material, controlling its final moisture content is 10%～15%;
(5) with after the raw material pulverizing, cross 40 orders～60 mesh sieves, promptly obtain required composite filter tip adsorption material.
3. the application of the described composite filter tip adsorption material of claim 1 in the preparation cigarette filter.
4. composite filter tip adsorption material according to claim 3 is used, and it is characterized in that: before the filter tow moulding, described composite filter tip adsorption material is sprinkling upon on the filter core equably, makes the composite particles filter stick; Composite particles filter stick and conventional filter element filtering rod are carried out compound, make the binary composite filter tip.
5. application process according to claim 4 is characterized in that: the addition of described sorbing material is that 5～50mg/ props up.
6. application process according to claim 4 is characterized in that: the addition of described sorbing material is that 15～35mg/ props up.
7. application process according to claim 4 is characterized in that: the addition of described sorbing material is that 25mg/ props up.
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| CNA200810058011XA CN101214090A (en) | 2008-01-07 | 2008-01-07 | Composite filter tip adsorption material and preparation and application thereof |
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| CNA200810058011XA CN101214090A (en) | 2008-01-07 | 2008-01-07 | Composite filter tip adsorption material and preparation and application thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101390658B (en) * | 2008-11-07 | 2011-12-28 | 云南烟草科学研究院 | Cigarette composite tip containing plant saponin extract |
| CN102742936A (en) * | 2012-07-27 | 2012-10-24 | 红云红河烟草(集团)有限责任公司 | Application of cane shoots in cigarettes |
| CN103315387A (en) * | 2013-07-18 | 2013-09-25 | 中国烟草总公司郑州烟草研究院 | Application of Chinese yam extractives in cigarettes |
| CN103355743A (en) * | 2013-08-14 | 2013-10-23 | 中国烟草总公司郑州烟草研究院 | Preparation and application of crop waste cigarette filter additive carrier materials |
| CN104801276A (en) * | 2015-02-13 | 2015-07-29 | 云南中烟工业有限责任公司 | Gastrodia elata porous particle and applications thereof |
| CN106263024A (en) * | 2016-08-12 | 2017-01-04 | 福建中烟工业有限责任公司 | A kind of reduce the method for phenol content in cigarette smoke |
| CN115606834A (en) * | 2021-07-16 | 2023-01-17 | 江苏浩丰生物科技有限公司 | Taro extract applied to tobacco industry and preparation method and application thereof |
-
2008
- 2008-01-07 CN CNA200810058011XA patent/CN101214090A/en active Pending
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101390658B (en) * | 2008-11-07 | 2011-12-28 | 云南烟草科学研究院 | Cigarette composite tip containing plant saponin extract |
| CN102742936A (en) * | 2012-07-27 | 2012-10-24 | 红云红河烟草(集团)有限责任公司 | Application of cane shoots in cigarettes |
| CN103315387A (en) * | 2013-07-18 | 2013-09-25 | 中国烟草总公司郑州烟草研究院 | Application of Chinese yam extractives in cigarettes |
| CN103355743A (en) * | 2013-08-14 | 2013-10-23 | 中国烟草总公司郑州烟草研究院 | Preparation and application of crop waste cigarette filter additive carrier materials |
| CN104801276A (en) * | 2015-02-13 | 2015-07-29 | 云南中烟工业有限责任公司 | Gastrodia elata porous particle and applications thereof |
| CN106263024A (en) * | 2016-08-12 | 2017-01-04 | 福建中烟工业有限责任公司 | A kind of reduce the method for phenol content in cigarette smoke |
| CN115606834A (en) * | 2021-07-16 | 2023-01-17 | 江苏浩丰生物科技有限公司 | Taro extract applied to tobacco industry and preparation method and application thereof |
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Owner name: HONGYUN HONGHE TOBACCO(GROUP )CO.LTD. Free format text: FORMER OWNER: HONGYUN TOBACCO (GROUP) CO.,LTD. Effective date: 20090703 |
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Effective date of registration: 20090703 Address after: Yunnan province Kunming City area village post encoding: 650202 Applicant after: Hongyun Honghe tobacco (Group) Co., Ltd. Address before: Yunnan province Kunming City area village post encoding: 650202 Applicant before: Hongyun Tobacco (Group) Co., Ltd. |
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Open date: 20080709 |