CN101177543B - 含紫外吸收基的活性染料 - Google Patents
含紫外吸收基的活性染料 Download PDFInfo
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- CN101177543B CN101177543B CN2006101181989A CN200610118198A CN101177543B CN 101177543 B CN101177543 B CN 101177543B CN 2006101181989 A CN2006101181989 A CN 2006101181989A CN 200610118198 A CN200610118198 A CN 200610118198A CN 101177543 B CN101177543 B CN 101177543B
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- Prior art keywords
- formula
- compound
- liquid
- diazonium salt
- carry out
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 150000001875 compounds Chemical class 0.000 claims abstract description 58
- 238000002360 preparation method Methods 0.000 claims abstract description 31
- 239000000975 dye Substances 0.000 claims description 99
- 239000000203 mixture Substances 0.000 claims description 54
- 239000007788 liquid Substances 0.000 claims description 46
- 238000005859 coupling reaction Methods 0.000 claims description 35
- 230000008878 coupling Effects 0.000 claims description 33
- 238000010168 coupling process Methods 0.000 claims description 33
- 150000001989 diazonium salts Chemical class 0.000 claims description 31
- 229910052799 carbon Inorganic materials 0.000 claims description 28
- 239000012954 diazonium Substances 0.000 claims description 28
- 238000009833 condensation Methods 0.000 claims description 24
- 230000005494 condensation Effects 0.000 claims description 24
- 239000002994 raw material Substances 0.000 claims description 22
- 229910052739 hydrogen Inorganic materials 0.000 claims description 19
- 229910052783 alkali metal Inorganic materials 0.000 claims description 17
- 150000001340 alkali metals Chemical group 0.000 claims description 16
- 238000005829 trimerization reaction Methods 0.000 claims description 15
- MAOBFOXLCJIFLV-UHFFFAOYSA-N (2-aminophenyl)-phenylmethanone Chemical compound NC1=CC=CC=C1C(=O)C1=CC=CC=C1 MAOBFOXLCJIFLV-UHFFFAOYSA-N 0.000 claims description 13
- 238000001035 drying Methods 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 125000003545 alkoxy group Chemical group 0.000 claims description 8
- 150000003839 salts Chemical class 0.000 claims description 8
- -1 amino compound Chemical class 0.000 claims description 7
- 239000002131 composite material Substances 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 5
- 238000006193 diazotization reaction Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 239000000725 suspension Substances 0.000 claims description 5
- JVMSQRAXNZPDHF-UHFFFAOYSA-N 2,4-diaminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C(N)=C1 JVMSQRAXNZPDHF-UHFFFAOYSA-N 0.000 claims description 3
- 239000011260 aqueous acid Substances 0.000 claims description 2
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 13
- 229920003043 Cellulose fiber Polymers 0.000 abstract description 2
- 239000004744 fabric Substances 0.000 description 46
- 239000000243 solution Substances 0.000 description 39
- 238000006243 chemical reaction Methods 0.000 description 36
- 239000000835 fiber Substances 0.000 description 24
- 238000004043 dyeing Methods 0.000 description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 21
- 229920000742 Cotton Polymers 0.000 description 20
- 241000219146 Gossypium Species 0.000 description 20
- 238000000034 method Methods 0.000 description 20
- 238000003756 stirring Methods 0.000 description 19
- 239000006096 absorbing agent Substances 0.000 description 17
- 230000035484 reaction time Effects 0.000 description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 11
- 230000008569 process Effects 0.000 description 11
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 10
- 239000007787 solid Substances 0.000 description 10
- 0 *c1cc([U]=C)c(C(c(cc2)ccc2N)[U])cc1 Chemical compound *c1cc([U]=C)c(C(c(cc2)ccc2N)[U])cc1 0.000 description 7
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 description 7
- 235000011167 hydrochloric acid Nutrition 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 6
- 239000010813 municipal solid waste Substances 0.000 description 6
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 6
- 238000010792 warming Methods 0.000 description 6
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 5
- 239000012965 benzophenone Substances 0.000 description 5
- 238000006482 condensation reaction Methods 0.000 description 5
- 239000000706 filtrate Substances 0.000 description 5
- 238000002390 rotary evaporation Methods 0.000 description 5
- 235000017550 sodium carbonate Nutrition 0.000 description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 description 5
- 235000010288 sodium nitrite Nutrition 0.000 description 5
- QPILZZVXGUNELN-UHFFFAOYSA-M sodium;4-amino-5-hydroxynaphthalene-2,7-disulfonate;hydron Chemical compound [Na+].OS(=O)(=O)C1=CC(O)=C2C(N)=CC(S([O-])(=O)=O)=CC2=C1 QPILZZVXGUNELN-UHFFFAOYSA-M 0.000 description 5
- NXTNASSYJUXJDV-UHFFFAOYSA-N 3-nitrobenzoyl chloride Chemical compound [O-][N+](=O)C1=CC=CC(C(Cl)=O)=C1 NXTNASSYJUXJDV-UHFFFAOYSA-N 0.000 description 4
- IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical compound ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 4
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 4
- 150000004699 copper complex Chemical class 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 239000003643 water by type Substances 0.000 description 4
- QZZSAWGVHXXMID-UHFFFAOYSA-N 1-amino-4-bromo-9,10-dioxoanthracene-2-sulfonic acid Chemical compound C1=CC=C2C(=O)C3=C(Br)C=C(S(O)(=O)=O)C(N)=C3C(=O)C2=C1 QZZSAWGVHXXMID-UHFFFAOYSA-N 0.000 description 3
- AFPHTEQTJZKQAQ-UHFFFAOYSA-N 3-nitrobenzoic acid Chemical compound OC(=O)C1=CC=CC([N+]([O-])=O)=C1 AFPHTEQTJZKQAQ-UHFFFAOYSA-N 0.000 description 3
- 230000006750 UV protection Effects 0.000 description 3
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 3
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 3
- 230000002194 synthesizing effect Effects 0.000 description 3
- 238000009941 weaving Methods 0.000 description 3
- ONYCIZMTGCXDEZ-UHFFFAOYSA-N (2,4-dihydroxyphenyl)-(3-nitrophenyl)methanone Chemical compound OC1=CC(O)=CC=C1C(=O)C1=CC=CC([N+]([O-])=O)=C1 ONYCIZMTGCXDEZ-UHFFFAOYSA-N 0.000 description 2
- VINASSTWBVKERF-UHFFFAOYSA-N (3-aminophenyl)-(2,4-dihydroxyphenyl)methanone Chemical compound NC1=CC=CC(C(=O)C=2C(=CC(O)=CC=2)O)=C1 VINASSTWBVKERF-UHFFFAOYSA-N 0.000 description 2
- MFYLRNKOXORIPK-UHFFFAOYSA-N (3-nitrophenyl)-phenylmethanone Chemical compound [O-][N+](=O)C1=CC=CC(C(=O)C=2C=CC=CC=2)=C1 MFYLRNKOXORIPK-UHFFFAOYSA-N 0.000 description 2
- HTSVYUUXJSMGQC-UHFFFAOYSA-N 2-chloro-1,3,5-triazine Chemical compound ClC1=NC=NC=N1 HTSVYUUXJSMGQC-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 229910021591 Copper(I) chloride Inorganic materials 0.000 description 2
- 239000004218 Orcein Substances 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 238000010009 beating Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical compound [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 description 2
- 229940045803 cuprous chloride Drugs 0.000 description 2
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 2
- 239000003792 electrolyte Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000007730 finishing process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 235000019248 orcein Nutrition 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 229960001755 resorcinol Drugs 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 2
- 239000001043 yellow dye Substances 0.000 description 2
- SGDKXQGGKPQZGD-UHFFFAOYSA-N (2,4-dihydroxyphenyl)-(4-nitrophenyl)methanone Chemical compound OC1=CC(O)=CC=C1C(=O)C1=CC=C([N+]([O-])=O)C=C1 SGDKXQGGKPQZGD-UHFFFAOYSA-N 0.000 description 1
- OTLNPYWUJOZPPA-UHFFFAOYSA-N 4-nitrobenzoic acid Chemical compound OC(=O)C1=CC=C([N+]([O-])=O)C=C1 OTLNPYWUJOZPPA-UHFFFAOYSA-N 0.000 description 1
- SKDHHIUENRGTHK-UHFFFAOYSA-N 4-nitrobenzoyl chloride Chemical compound [O-][N+](=O)C1=CC=C(C(Cl)=O)C=C1 SKDHHIUENRGTHK-UHFFFAOYSA-N 0.000 description 1
- RXQNKKRGJJRMKD-UHFFFAOYSA-N 5-bromo-2-methylaniline Chemical compound CC1=CC=C(Br)C=C1N RXQNKKRGJJRMKD-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 1
- CUMIEPWCUMLJLH-UHFFFAOYSA-N C=Nc(cc1)ccc1C(c(ccc(O)c1)c1O)=O Chemical compound C=Nc(cc1)ccc1C(c(ccc(O)c1)c1O)=O CUMIEPWCUMLJLH-UHFFFAOYSA-N 0.000 description 1
- QUIXYMMJBVXVOB-UHFFFAOYSA-N C=[S](c1cc2cc(S(O)(=O)=O)cc(O)c2c(N)c1)(O)(=O)=O Chemical compound C=[S](c1cc2cc(S(O)(=O)=O)cc(O)c2c(N)c1)(O)(=O)=O QUIXYMMJBVXVOB-UHFFFAOYSA-N 0.000 description 1
- MUKIJJJGEXVDJV-UHFFFAOYSA-N Cc(c(N=Nc1cccc(S(=O)=O)c1)c1O)n[n]1-c(cc1)ccc1Nc1nc(Nc2cccc(C(c(ccc(O)c3)c3O)=O)c2)nc(Cl)n1 Chemical compound Cc(c(N=Nc1cccc(S(=O)=O)c1)c1O)n[n]1-c(cc1)ccc1Nc1nc(Nc2cccc(C(c(ccc(O)c3)c3O)=O)c2)nc(Cl)n1 MUKIJJJGEXVDJV-UHFFFAOYSA-N 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- AAKNCXNXBGFSND-UHFFFAOYSA-N Clc1nc([Cl]=[IH])nc(Cl)n1 Chemical compound Clc1nc([Cl]=[IH])nc(Cl)n1 AAKNCXNXBGFSND-UHFFFAOYSA-N 0.000 description 1
- 101100489867 Mus musculus Got2 gene Proteins 0.000 description 1
- MLYBQGISNQKZDH-UHFFFAOYSA-N Nc(cc1)cc(N)c1[S](CC=N)(O)(=O)=O Chemical compound Nc(cc1)cc(N)c1[S](CC=N)(O)(=O)=O MLYBQGISNQKZDH-UHFFFAOYSA-N 0.000 description 1
- UFLISPRESNVPAI-UHFFFAOYSA-N Nc(cc1)ccc1C(c(ccc(O)c1)c1O)=O Chemical compound Nc(cc1)ccc1C(c(ccc(O)c1)c1O)=O UFLISPRESNVPAI-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000029936 alkylation Effects 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- FNXLCIKXHOPCKH-UHFFFAOYSA-N bromamine Chemical class BrN FNXLCIKXHOPCKH-UHFFFAOYSA-N 0.000 description 1
- 239000012928 buffer substance Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910000365 copper sulfate Inorganic materials 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-M dihydrogenphosphate Chemical compound OP(O)([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-M 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N methyl monoether Natural products COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 201000000849 skin cancer Diseases 0.000 description 1
- 201000008261 skin carcinoma Diseases 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate group Chemical group S(=O)(=O)([O-])[O-] QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 239000000979 synthetic dye Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Landscapes
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Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN2006101181989A CN101177543B (zh) | 2006-11-10 | 2006-11-10 | 含紫外吸收基的活性染料 |
Applications Claiming Priority (1)
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CN2006101181989A CN101177543B (zh) | 2006-11-10 | 2006-11-10 | 含紫外吸收基的活性染料 |
Publications (2)
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CN101177543A CN101177543A (zh) | 2008-05-14 |
CN101177543B true CN101177543B (zh) | 2011-04-06 |
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CN2006101181989A Expired - Fee Related CN101177543B (zh) | 2006-11-10 | 2006-11-10 | 含紫外吸收基的活性染料 |
Country Status (1)
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Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101880470A (zh) * | 2010-03-02 | 2010-11-10 | 浙江吉华集团有限公司 | 苯并三唑抗紫外线辐射活性染料及其制备方法 |
DK2563843T3 (en) | 2010-04-28 | 2018-03-12 | Univ Georgia | PHOTOCHEMICAL CROSS-POLYMERS, PROCEDURES FOR MARKING PHOTOCHEMIC CROSS-POLYMERS, PROCEDURES FOR USING PHOTOCHEMIC CROSS-POLYMERS, AND ... |
US9315628B2 (en) | 2011-07-15 | 2016-04-19 | University Of Georgia Research Foundation, Inc. | Permanent attachment of agents to surfaces containing C-H functionality |
WO2013056007A2 (en) | 2011-10-14 | 2013-04-18 | University Of Georgia Research Foundation, Inc. | Photochemical cross-linkable polymers, methods of making photochemical cross-linkable plolymers, methods of using photochemical cross-linkable poloymers, and methods of making articles containing photochemical cross-linkable polymers |
CN104326947B (zh) * | 2013-10-14 | 2016-08-24 | 大连理工大学 | 活性艳蓝k-gr中间体的制备方法 |
CN110761091B (zh) * | 2019-10-29 | 2022-10-11 | 浙江理工大学上虞工业技术研究院有限公司 | 具有紫外线吸收功能的水溶性交联固色剂及其制备方法 |
CN116218254B (zh) * | 2022-12-05 | 2024-05-17 | 湖北丽源科技股份有限公司 | 一种艳红色活性染料及其制备方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5700394A (en) * | 1994-12-13 | 1997-12-23 | Ciba Specialty Chemicals Corporation | Method for the treatment of textile fibers |
EP0717140B1 (en) * | 1994-12-13 | 2006-08-09 | Ciba SC Holding AG | Method for the treatment of textile fibres |
-
2006
- 2006-11-10 CN CN2006101181989A patent/CN101177543B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5700394A (en) * | 1994-12-13 | 1997-12-23 | Ciba Specialty Chemicals Corporation | Method for the treatment of textile fibers |
EP0717140B1 (en) * | 1994-12-13 | 2006-08-09 | Ciba SC Holding AG | Method for the treatment of textile fibres |
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Publication number | Publication date |
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CN101177543A (zh) | 2008-05-14 |
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