CN101124916A - Biological pesticide mixed with plant insecticide sterilization component and amino-oligosaccharin and preparation method thereof - Google Patents
Biological pesticide mixed with plant insecticide sterilization component and amino-oligosaccharin and preparation method thereof Download PDFInfo
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- CN101124916A CN101124916A CNA2007100124165A CN200710012416A CN101124916A CN 101124916 A CN101124916 A CN 101124916A CN A2007100124165 A CNA2007100124165 A CN A2007100124165A CN 200710012416 A CN200710012416 A CN 200710012416A CN 101124916 A CN101124916 A CN 101124916A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
The invention relates to an ecological agricultural drug and a preparing method compounded by a content of Chinese traditional herb plant insecticide and amino group oligosaccharide. The ecological agricultural drug is refined by blending and processing the plant gradients containing one or a plurality of insecticide and disinfecting components and the Chitosante raw materials and solutions which are extracted with the amino group oligosaccharide. The weight percentages of all components are respectively: five to thirty percent of plant materials, seventy to ninety five percent of Chitosante material, and the solvents are alcohol and water. When in blending and configuring process, additives are added; wherein, the additives are one or a plurality of the agents, such as an antiseptic agent, a dispersing agent, a surface active agent, a penetrant or an emulsifying agent. The plant materials are materials such as Sophora flavescens, tobacco, Indian chinaberry fruit, pyrethrum, climbing groundsel or Aztec marigold, etc., the invention has the beneficial effects of multifunction of insecticide and disinfection, anti disease, disease prevention; easy degradation of the product, no residues and extensive raw material source. The working process of the invention simplifies the processes of extraction, condensation and filter with low producing cost.
Description
Technical field
The invention belongs to biomedicine field, relate to the ecological agricultural chemical that a kind of plant insecticide sterilization component becomes with amino-oligosaccharide and the new method of preparing process thereof.
Background technology
Stripe disease is a kind of with rice grub---rice fulgorid is host and by its common disease that extensively infects and propagate, and all often there is generation each paddy rice main producing region, Southeast Asia.The state of an illness is propagated rapidly, and destructive power is strong, usually causes the large tracts of land of crop to infect, and causes the underproduction even total crop failure.At present, domestic chemistry and the biological pesticide product of China all can alleviate and alleviate such disease to a certain extent.But owing to stripe virus disease virus is propagated by rice fulgorid, and rice fulgorid is a kind of extremely strong to the agricultural chemicals pesticide resistance, the pernicious insect pest that fertility is high, and plyability infects concurrent propagation simultaneously like this, brings great difficulty for the prevention and the radical cure of such disease.In addition, in the existing Pesticidal products, insecticide is desinsection by all means, and bacteriostatic agent only can be antibacterial, eradicate this disease by the legal system method of routine, and medicine is implemented the spraying control separately to insect pest, disease respectively at least, and repeats several times by spraying cycle.Several cycles just can be subjected to effect repeatedly, and in the process of doing like this, certainly will cause a large amount of wastes to multiple resources such as agricultural chemicals, labour, the water source energy.For a long time, be to be difficult to the problem that overcomes in the agricultural production always.
Summary of the invention
The purpose of this invention is to provide a kind of plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide and preparation method thereof, this biopesticide pesticide-germicide effect is remarkable, processing steps such as its preparation method has been simplified extraction greatly, concentrated, filtration, energy savings; Simultaneously, also increased the drug effect of biopesticide significantly.
Technical scheme of the present invention is, a kind of plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide, it is by one or more chitin raw material and solvent that has the plant material of insecticide sterilization component and can extract amino-oligosaccharide, processing and refining forms, the percentage by weight of each component is: plant material is 5%~30%, chitin raw material is 70%~95%, and solvent is alcohol or water.
Two of technical scheme of the present invention is, a kind of plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide, the percentage by weight of each component is: plant material is 3.5%~21%, chitin raw material is 49%~66.5%, additive and solvent are 30%, solvent is alcohol or water, and additive is one or more in preservative, dispersant, surfactant, bleeding agent or the emulsifier.
Three of technical scheme of the present invention is, the percentage by weight of each component is: the total weight percent of plant material and chitin raw material is 70%~100%, the percentage by weight of additive and solvent is 0~30%, wherein, the percentage by weight of plant material accounts for 5%~30% of described total weight percent, and the percentage by weight of chitin raw material accounts for 70~95% of described total weight percent.Solvent is alcohol or water, and additive is one or more in preservative, dispersant, surfactant, bleeding agent or the emulsifier.
Aforesaid plant material is meant kuh-seng, tobacco, seed of Azadirachta indica, Dalmatian chrysanthemum, climbing groundsel, Aztec marigold, the tuber of stemona, Sophora alopecuroide, Celastrus angulatus, garlic, chinaberry, the root of large-flowered skullcap, winter daphne, the root of langdu, OX-heart is mended son, betel nut, Chinese honey locust, stone-like omphalia, datura, overgrown with weeds flower bar, sweet-scented oleander, Rhododendron molle, elegant jessamine, Li Lu, frutus cnidii, hemlock, Fructus Bruceae, the bristles wormwood artemisia, radix bupleuri, Ageratum conyzoides, the bighead atractylodes rhizome, the rhizome of Chinese monkshood, ginkgo, cape jasmine, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, pumpkin seeds, French marigold, in Ageratum conyzoides or the castor-oil plant one or more.
Described preservative is a Sodium Benzoate, and dispersant is an organosilicon, and surfactant is AEO, O, OS, NP, JFC, PEG, and bleeding agent is azone or Chinese honey locust extract, and emulsifier is polysorbate60 or Tween 80.
Prepare the method for a kind of plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide, its step is as follows:
1) required one or more plant materials that can extract insecticide sterilization component are cleaned, dry the back and pulverize, pulverizing the order number is 40 orders~1200 orders;
2) chitin is carried out fermentation process, generate required amino-oligosaccharide;
3) with the plant material after pulverizing in the step 1) with step 2) in fermentation and handle the amino-oligosaccharide of back generation and solvent and stir in proportion and be mixed through killing viable bacteria, mixed ratio is: plant material: amino-oligosaccharide: solvent and additive=and 3: 4: 3, whole mixing process is carried out at normal temperatures and pressures.
In above-mentioned steps 3) in, when being mixed, stirring adds additive, and additives ratio is: it is 12% that preservative sodium benzoate accounts for total weight percent, and it is 18% that the bleeding agent azone accounts for total weight percent.
Extract from China tradition pesticide plant and to have insecticidal function effective active composition, the food refusal by making that harmful insect smells, food and neural paralysis, destroy all a plurality of aspects kill virus host rice ash aleyrodids such as chitinous copy function, reduce and reduce the route of transmission of direct losses and indirect blocking-up rice blast.The more important thing is, this active component can reduce and even thoroughly destroy its genital system function, cause the insect comprehensive fertility ability such as maturing rate, spawning rate, survival rate of pupating to descend greatly, the accumulation through certain hour reaches the effect of eliminating insect population quantity significantly.
The active component that extracts from marine organisms---amino-oligosacchride have the copy function of the RNA that suppresses spore development and virus and the complex functionality of protein, by the gene expression and the growth metabolism of break virus, has stoped the propagation and the development of disease effectively.
The invention has the beneficial effects as follows:
1. plant material need not carry out extraction process, but after it is crushed to certain fineness, directly joins in the fermentation tank of oligosaccharide to be mixed in proportion, has simplified extraction greatly, concentrates, processing step such as filtration, energy savings.
2. be crushed to certain fineness by plant material, increased the surface area of drug particles, simultaneously with the plant cell wall structural deterioration, active ingredient is flowed out, make drug ingedient more easily with solvent diffusion and dissolving, not only saved solvent, improved recovery rate, shorten process cycle, also increased drug effect significantly.Have desinsection and antibacterial double effects, take stopgap measures and effect a permanent cure, the degree of harmful insect infringement plant is obviously descended.
3. the multiple kind of effect that has pesticide-germicide, defending and fighting against diseases, its product high-efficiency low-toxicity, easily degraded, noresidue, to insect be difficult for developing immunity to drugs and raw material sources extensively, low production cost.
Embodiment
300 kilograms of kuh-sengs are cleaned, be crushed to 120 orders after drying, on 1 cubic metre fermentation tank, 400 kilograms of chitins are carried out fermentation process, through killing the amino-oligosaccharide that generates after viable bacteria is handled, kuh-seng raw material after pulverizing is joined in the fermentation tank that amino-oligosaccharide is housed, simultaneously, add 300 kg water and make solvent, stir and make their even mixing.Three's material ratio is---kuh-seng raw material: amino-oligosaccharide: and solvent and additive=3: 4: 3, whole mixing process can be carried out at normal temperatures and pressures, the final organic agricultural chemicals that must meet the organic farming production standard.Look the various criterion requirement of required insecticidal bactericide, also proper amount of surfactant such as tween 1 can be added in above-mentioned prescription, additives such as dispersant, bleeding agent, preservative, the biopesticide of formation green standard, to play the prolongation storage life, strengthen effects such as drug effect.
Claims (7)
1. plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide, it is characterized in that, it is by one or more chitin raw material and solvent that has the plant material of insecticide sterilization component and can extract amino-oligosaccharide, processing and refining forms, the percentage by weight of each component is: plant material is 5%~30%, chitin raw material is 70%~95%, and solvent is alcohol or water.
2. a kind of plant insecticide sterilization component according to claim 1 and the composite biopesticide of amino-oligosaccharide, it is characterized in that, the percentage by weight of each component is: plant material is 3.5%~21%, chitin raw material is 49%~66.5%, additive and solvent are 30%, solvent is alcohol or water, and additive is one or more in preservative, dispersant, surfactant, bleeding agent or the emulsifier.
3. a kind of plant insecticide sterilization component according to claim 1 and the composite biopesticide of amino-oligosaccharide, it is characterized in that, the percentage by weight of each component is: the total weight percent of plant material and chitin raw material is 70%~100%, the percentage by weight of additive and solvent is 0~30%, wherein: the percentage by weight of plant material accounts for 5%~30% of described total weight percent, and the percentage by weight of chitin raw material accounts for 70~95% of described total weight percent.Solvent is alcohol or water, and additive is one or more in preservative, dispersant, surfactant, bleeding agent or the emulsifier.
4. as any described a kind of plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide in the claim 1 to 3, it is characterized in that described plant material is meant kuh-seng, tobacco, seed of Azadirachta indica, Dalmatian chrysanthemum, climbing groundsel, Aztec marigold, the tuber of stemona, Sophora alopecuroide, Celastrus angulatus, garlic, chinaberry, the root of large-flowered skullcap, winter daphne, the root of langdu, OX-heart is mended son, betel nut, Chinese honey locust, stone-like omphalia, datura, overgrown with weeds flower bar, sweet-scented oleander, Rhododendron molle, elegant jessamine, Li Lu, frutus cnidii, hemlock, Fructus Bruceae, the bristles wormwood artemisia, radix bupleuri, Ageratum conyzoides, the bighead atractylodes rhizome, the rhizome of Chinese monkshood, ginkgo, cape jasmine, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, pumpkin seeds, French marigold, in Ageratum conyzoides or the castor-oil plant one or more.
5. as claim 2 or 3 described a kind of plant insecticide sterilization component and the composite biopesticides of amino-oligosaccharide, it is characterized in that, described preservative is a Sodium Benzoate, dispersant is an organosilicon, surfactant is AEO, O, OS, NP, JFC, PEG, bleeding agent is azone or Chinese honey locust extract, and emulsifier is polysorbate60 or Tween 80.
6. prepare the method for a kind of plant insecticide sterilization component and the composite biopesticide of amino-oligosaccharide, it is characterized in that, its step is as follows:
1) required one or more plant materials that can extract insecticide sterilization component are cleaned, dry the back and pulverize, pulverizing the order number is 40 orders~1200 orders;
2) chitin is carried out fermentation process, generate required amino-oligosaccharide;
3) with the plant material after pulverizing in the step 1) with step 2) in fermentation and handle the amino-oligosaccharide of back generation and solvent and stir in proportion and be mixed through killing viable bacteria, mixed ratio is: plant material: amino-oligosaccharide: solvent and additive=and 3: 4: 3, whole mixing process is carried out at normal temperatures and pressures.
7. a kind of preparation as claimed in claim 8 has the plant of insecticide sterilization component and the method for the composite biopesticide of amino-oligosaccharide, it is characterized in that, in above-mentioned steps 3) in, when being mixed, stirring adds additive, additives ratio is: it is 12% that preservative sodium benzoate accounts for total weight percent, and it is 18% that the bleeding agent azone accounts for total weight percent.
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