CN107821446A - A kind of rice breeding bactericide specially containing Lanthanide complex - Google Patents
A kind of rice breeding bactericide specially containing Lanthanide complex Download PDFInfo
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- CN107821446A CN107821446A CN201711197347.XA CN201711197347A CN107821446A CN 107821446 A CN107821446 A CN 107821446A CN 201711197347 A CN201711197347 A CN 201711197347A CN 107821446 A CN107821446 A CN 107821446A
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- lanthanide complex
- rice breeding
- containing lanthanide
- bactericide specially
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/16—Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N55/00—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
- A01N55/02—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur containing metal atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F5/00—Compounds containing elements of Groups 3 or 13 of the Periodic System
- C07F5/003—Compounds containing elements of Groups 3 or 13 of the Periodic System without C-Metal linkages
Abstract
The invention discloses a kind of rice breeding bactericide specially containing Lanthanide complex, its raw material includes by weight：15 30 parts of Lanthanide complex, 28 parts of plants essential oil, 13 parts of plant polyose, 25 parts of allicin, to section 13 parts of Chinese wax extract, 25 parts of oleander extract, 3 10 parts of extra large mango extract, 13 parts of eugenol, 25 parts of rotenone, 0.3 2 parts of chitosan, 0.9 3.5 parts of amino-oligosaccharide, 10 25 parts of auxiliary agent, 100 parts of water；Wherein, the Lanthanide complex is formed by the reaction of 2 menaphthyl benzimidazoles, α furylacrylic acids and lanthanum chloride.Rice breeding bactericide specially proposed by the present invention containing Lanthanide complex, its bactericidal property is excellent, lasting period length, can prevent and treat multiple diseases, serve the effect of volume increase.
Description
Technical field
The present invention relates to rice breeding technology field, more particularly to a kind of rice breeding special sterilizing containing Lanthanide complex
Agent.
Background technology
Rice is one of important cereal crops in China, is occupied an important position in national economy, its sown area, total
Production and per unit area yield occupy the first place of cereal crops, it is seen that the importance of rice.In the rice of China's plantation, hybrid rice growing surface
Product accounts for the 57% of total rice area, the hm of hybrid paddy rice production of hybrid seeds area 180,0002Left and right.The quality of hybrid rice seed protonatomic mass is to realize rice
High-quality, high yield and the basis efficiently produced, hybrid rice seed level of production height are directly connected to China's grain security.
Although rice breeding progress is quickly in recent years, during rice breeding, its hybrid seed yield is by skill
Whether experienced and weather conditions the quality of art personnel influences greatly, therefore during the production of hybrid seeds, seed production efficiency be present
The defects of not high, wherein, pest and disease damage is also an important factor for influenceing rice hybrid seed yield, the use of bactericide is preventing and treating rice disease
A kind of cost-effective method, but existing rice breeding bactericide fails to reach preferable bactericidal yield-increase effect, limit
Its application is made.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes that a kind of rice breeding containing Lanthanide complex is special to kill
Microbial inoculum, its bactericidal property is excellent, lasting period length, can prevent and treat multiple diseases, serve the effect of volume increase.
A kind of rice breeding bactericide specially containing Lanthanide complex proposed by the present invention, its raw material include by weight：Lanthanum
Complex 15-30 parts, plants essential oil 2-8 parts, plant polyose 1-3 parts, allicin 2-5 parts, to section Chinese wax extract 1-3 parts, folder
Bamboo peach extract 2-5 parts, extra large mango extract 3-10 parts, eugenol 1-3 parts, rotenone 2-5 parts, chitosan 0.3-2 parts,
Amino-oligosaccharide 0.9-3.5 parts, auxiliary agent 10-25 parts, 100 parts of water；Wherein, the Lanthanide complex by 2- menaphthyls benzimidazole,
α-furyl acrylic acid and lanthanum chloride reaction form.
Preferably, the Lanthanide complex is prepared according to following technique：By 2- menaphthyls benzimidazole and α-furyl third
Olefin(e) acid is added in the mixed liquor of ethanol and water, and 30-50min is stirred after being heated to reflux, then adds lanthanum chloride, at 70-80 DEG C
Stirring reaction 10-18h, reaction are cooled to room temperature after terminating, through standing, filtering, washing, being dried to obtain the Lanthanide complex.
Preferably, in the mixed liquor of ethanol and water, the volume ratio of ethanol and water is 1：1-5.
Preferably, 2- menaphthyls benzimidazole, α-furyl acrylic acid, the weight ratio of lanthanum chloride are 2-3：1-2：1.5-2.
Preferably, the plants essential oil is one or two kinds of mixture in grass-leaved sweetflag essential oil, tea tree ethereal oil.
Preferably, the plant polyose is one or two kinds of mixture in lentinan, astragalus polyose.
Preferably, the auxiliary agent includes emulsifying agent, antifreezing agent, thickener and acetone, and emulsifying agent, antifreezing agent, thickener,
The weight ratio of acetone is 1-3：2-5：1-4：3-6.
Preferably, the emulsifying agent is one or two kinds of mixture in sodium alkyl benzene sulfonate, polyacrylamide.
Preferably, the antifreezing agent is one or more kinds of mixtures in magnesium chloride, glycerine, propane diols.
Preferably, the thickener is one or more kinds of mixtures in pectin, starch, sodium alginate.
It is heretofore described to section Chinese wax extract, oleander extract, extra large mango extract respectively by section Chinese wax
Branches and leaves, the branches and leaves of oleander, the branches and leaves of extra large mango are obtained using organic solvent cold soaking extraction method.
Rice breeding bactericide specially of the present invention containing Lanthanide complex, Lanthanide complex is added in its raw material, excellent
In the preparation process for selecting mode Lanthanide complex, using 2- menaphthyls benzimidazole and α-furyl acrylic acid to coordinate, using lanthanum chloride as
Metal salt is reacted, and by controlling the condition of reaction, 2- menaphthyls benzimidazole, α-furyl acrylic acid and lanthanum chloride occurs
Complexation reaction, so as to three are combined into one, Lanthanide complex is obtained, by obtained Lanthanide complex addition system, its
With plants essential oil, plant polyose, allicin, to section Chinese wax extract, oleander extract, extra large mango extract, eugenol,
After rotenone, chitosan, amino-oligosaccharide coordinate, it can complement each other, collaboration promotes, and the resistance of rice is enhanced, to water
The multiple diseases of rice have prevention effect, and the lasting period is grown, and bactericidal property is excellent, and the damage to rice is small, improves breeding
Yield and quality, serve the effect of volume increase antibacterial.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of rice breeding bactericide specially containing Lanthanide complex proposed by the present invention, its raw material include by weight：Lanthanum
30 parts of complex, 2 parts of plants essential oil, 3 parts of plant polyose, 2 parts of allicin, to section 3 parts of Chinese wax extract, oleander extract 2
Part, 10 parts of extra large mango extract, 1 part of eugenol, 5 parts of rotenone, 0.3 part of chitosan, 3.5 parts of amino-oligosaccharide, auxiliary agent
10 parts, 100 parts of water；Wherein, the Lanthanide complex by 2- menaphthyls benzimidazole, α-furyl acrylic acid and lanthanum chloride react and
Into.
Embodiment 2
A kind of rice breeding bactericide specially containing Lanthanide complex proposed by the present invention, its raw material include by weight：Lanthanum
15 parts of complex, 8 parts of plants essential oil, 1 part of plant polyose, 5 parts of allicin, to section 1 part of Chinese wax extract, oleander extract 5
Part, 3 parts of extra large mango extract, 3 parts of eugenol, 2 parts of rotenone, 2 parts of chitosan, 0.9 part of amino-oligosaccharide, auxiliary agent 25
Part, 100 parts of water；Wherein, the Lanthanide complex is formed by the reaction of 2- menaphthyls benzimidazole, α-furyl acrylic acid and lanthanum chloride.
Embodiment 3
A kind of rice breeding bactericide specially containing Lanthanide complex proposed by the present invention, its raw material include by weight：Lanthanum
26 parts of complex, 3 parts of grass-leaved sweetflag essential oil, 2.6 parts of lentinan, 3 parts of allicin, section 2.5 parts of Chinese wax extract, oleander are carried
Take 3 parts of thing, 8 parts of extra large mango extract, 1.6 parts of eugenol, 4.3 parts of rotenone, 0.6 part of chitosan, amino-oligosaccharide 3
Part, 16 parts of auxiliary agent, 100 parts of water；Wherein, the Lanthanide complex is by 2- menaphthyls benzimidazole, α-furyl acrylic acid and lanthanum chloride
Reaction forms；
Wherein, the Lanthanide complex is prepared according to following technique：By 2- menaphthyls benzimidazole and α-furyl propylene
Acid is added in the mixed liquor of ethanol and water, wherein, in the mixed liquor of ethanol and water, the volume ratio of ethanol and water is 1：1, heating
50min is stirred after backflow, then adds lanthanum chloride, wherein, 2- menaphthyls benzimidazole, α-furyl acrylic acid, the weight of lanthanum chloride
Amount is than being 2：2：1.5, the stirring reaction 10h at 80 DEG C, reaction are cooled to room temperature after terminating, and through standing, filtering, washing, dry
Obtain the Lanthanide complex；
The auxiliary agent includes emulsifying agent, antifreezing agent, thickener and acetone, and emulsifying agent, antifreezing agent, thickener, acetone
Weight ratio is 1：5：1：6；
The emulsifying agent is sodium alkyl benzene sulfonate；
The antifreezing agent is magnesium chloride；
The thickener is pectin.
Embodiment 4
A kind of rice breeding bactericide specially containing Lanthanide complex proposed by the present invention, its raw material include by weight：Lanthanum
17 parts of complex, 7 parts of tea tree ethereal oil, 1.3 parts of astragalus polyose, 4.3 parts of allicin, section 1.6 parts of Chinese wax extract, oleander are carried
Take 4.2 parts of thing, 4 parts of extra large mango extract, 2.5 parts of eugenol, 3 parts of rotenone, 1.7 parts of chitosan, amino-oligosaccharide 1.2
Part, 21 parts of auxiliary agent, 100 parts of water；Wherein, the Lanthanide complex is by 2- menaphthyls benzimidazole, α-furyl acrylic acid and lanthanum chloride
Reaction forms；
Wherein, the Lanthanide complex is prepared according to following technique：By 2- menaphthyls benzimidazole and α-furyl propylene
Acid is added in the mixed liquor of ethanol and water, wherein, in the mixed liquor of ethanol and water, the volume ratio of ethanol and water is 1：5, heating
30min is stirred after backflow, then adds lanthanum chloride, wherein, 2- menaphthyls benzimidazole, α-furyl acrylic acid, the weight of lanthanum chloride
Amount is than being 3：1：2, the stirring reaction 18h at 70 DEG C, reaction are cooled to room temperature after terminating, through standing, filtering, washing, dry
To the Lanthanide complex；
The auxiliary agent includes emulsifying agent, antifreezing agent, thickener and acetone, and emulsifying agent, antifreezing agent, thickener, acetone
Weight ratio is 3：2：4：3；
The emulsifying agent is polyacrylamide；
The antifreezing agent is that magnesium chloride, the mixture of propane diols, and the weight ratio of magnesium chloride, propane diols are 3：2；
The thickener is that starch, the mixture of sodium alginate, and the weight ratio of starch, sodium alginate are 4：5.
Embodiment 5
A kind of rice breeding bactericide specially containing Lanthanide complex proposed by the present invention, its raw material include by weight：Lanthanum
21 parts of complex, 5 parts of plants essential oil, 2 parts of plant polyose, 3 parts of allicin, to section 2 parts of Chinese wax extract, oleander extract
3.5 parts, 7 parts of extra large mango extract, 2 parts of eugenol, 3.8 parts of rotenone, 1.4 parts of chitosan, 2 parts of amino-oligosaccharide, help
16 parts of agent, 100 parts of water；Wherein, the Lanthanide complex by 2- menaphthyls benzimidazole, α-furyl acrylic acid and lanthanum chloride react and
Into；
Wherein, the Lanthanide complex is prepared according to following technique：By 2- menaphthyls benzimidazole and α-furyl propylene
Acid is added in the mixed liquor of ethanol and water, wherein, in the mixed liquor of ethanol and water, the volume ratio of ethanol and water is 1：4, heating
40min is stirred after backflow, then adds lanthanum chloride, wherein, 2- menaphthyls benzimidazole, α-furyl acrylic acid, the weight of lanthanum chloride
Amount is than being 2.3：1.6：1.7, the stirring reaction 15h at 75 DEG C, reaction are cooled to room temperature after terminating, through standing, filtering, washing,
It is dried to obtain the Lanthanide complex；
The plants essential oil is grass-leaved sweetflag essential oil, the mixture of tea tree ethereal oil, and the weight of grass-leaved sweetflag essential oil, tea tree ethereal oil
Than for 3：7；
The plant polyose is lentinan, the mixture of astragalus polyose, and the weight ratio of lentinan, astragalus polyose is
6：5；
The auxiliary agent includes emulsifying agent, antifreezing agent, thickener and acetone, and emulsifying agent, antifreezing agent, thickener, acetone
Weight ratio is 2：3：3：5；
The emulsifying agent is sodium alkyl benzene sulfonate, the mixture of polyacrylamide, and sodium alkyl benzene sulfonate, polyacrylamide
Weight ratio be 4：9；
The antifreezing agent is magnesium chloride, glycerine, the mixture of propane diols, and the weight of magnesium chloride, glycerine, propane diols
Than for 3：7：2；
The thickener is pectin, starch, the mixture of sodium alginate, and the weight ratio of pectin, starch, sodium alginate is
6：8：9.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (10)
1. a kind of rice breeding bactericide specially containing Lanthanide complex, it is characterised in that its raw material includes by weight：Lanthanum coordinates
Thing 15-30 parts, plants essential oil 2-8 parts, plant polyose 1-3 parts, allicin 2-5 parts, to section Chinese wax extract 1-3 parts, oleander
Extract 2-5 parts, extra large mango extract 3-10 parts, eugenol 1-3 parts, rotenone 2-5 parts, chitosan 0.3-2 parts, amino
Oligosaccharide 0.9-3.5 parts, auxiliary agent 10-25 parts, 100 parts of water；Wherein, the Lanthanide complex is by 2- menaphthyls benzimidazole, α-furan
Mutter acrylic acid and lanthanum chloride reaction form.
2. the rice breeding bactericide specially containing Lanthanide complex according to claim 1, it is characterised in that the Lanthanide complex
Prepared according to following technique：2- menaphthyls benzimidazole and α-furyl acrylic acid are added in the mixed liquor of ethanol and water,
30-50min is stirred after being heated to reflux, then adds lanthanum chloride, the stirring reaction 10-18h at 70-80 DEG C, reaction terminates rear cold
But to room temperature, through standing, filtering, washing, being dried to obtain the Lanthanide complex.
3. the rice breeding bactericide specially containing Lanthanide complex according to claim 2, it is characterised in that ethanol and water it is mixed
Close in liquid, the volume ratio of ethanol and water is 1：1-5.
4. the rice breeding bactericide specially containing Lanthanide complex according to any one of claim 1-3, it is characterised in that 2-
Menaphthyl benzimidazole, α-furyl acrylic acid, the weight ratio of lanthanum chloride are 2-3：1-2：1.5-2.
5. the rice breeding bactericide specially containing Lanthanide complex according to any one of claim 1-4, it is characterised in that institute
Plants essential oil is stated as one or two kinds of mixture in grass-leaved sweetflag essential oil, tea tree ethereal oil.
6. the rice breeding bactericide specially containing Lanthanide complex according to any one of claim 1-5, it is characterised in that institute
Plant polyose is stated as one or two kinds of mixture in lentinan, astragalus polyose.
7. the rice breeding bactericide specially containing Lanthanide complex according to any one of claim 1-6, it is characterised in that institute
Stating auxiliary agent includes emulsifying agent, antifreezing agent, thickener and acetone, and the weight ratio of emulsifying agent, antifreezing agent, thickener, acetone is 1-
3：2-5：1-4：3-6.
8. the rice breeding bactericide specially containing Lanthanide complex according to claim 7, it is characterised in that the emulsifying agent is
One or two kinds of mixture in sodium alkyl benzene sulfonate, polyacrylamide.
9. the rice breeding bactericide specially containing Lanthanide complex according to claim 7 or 8, it is characterised in that described antifreeze
Agent is one or more kinds of mixtures in magnesium chloride, glycerine, propane diols.
10. the rice breeding bactericide specially containing Lanthanide complex according to any one of claim 7-9, it is characterised in that
The thickener is one or more kinds of mixtures in pectin, starch, sodium alginate.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711197347.XA CN107821446A (en) | 2017-11-25 | 2017-11-25 | A kind of rice breeding bactericide specially containing Lanthanide complex |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711197347.XA CN107821446A (en) | 2017-11-25 | 2017-11-25 | A kind of rice breeding bactericide specially containing Lanthanide complex |
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Citations (5)
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|---|---|---|---|---|
| CN100998335A (en) * | 2006-12-29 | 2007-07-18 | 上海师范大学 | Kernel-shell structured rare-earth nanometer antibiotic agent, prepn. method and application thereof |
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| CN101156589A (en) * | 2007-11-27 | 2008-04-09 | 北京有色金属研究总院 | Caspase inhibitors and the use thereof |
| CN101180974A (en) * | 2007-12-21 | 2008-05-21 | 吕学良 | Yellow humic acid rare earths seed-dressing agent for resisting take-all of wheat |
| CN105248460A (en) * | 2015-10-09 | 2016-01-20 | 广州潮徽化工科技有限公司 | Compound antimicrobial composition containing microcapsules and preparation method and application of compound antimicrobial composition |
-
2017
- 2017-11-25 CN CN201711197347.XA patent/CN107821446A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100998335A (en) * | 2006-12-29 | 2007-07-18 | 上海师范大学 | Kernel-shell structured rare-earth nanometer antibiotic agent, prepn. method and application thereof |
| CN101124916A (en) * | 2007-08-06 | 2008-02-20 | 大连奥德植保药业有限公司 | Biological pesticide mixed with plant insecticide sterilization component and amino-oligosaccharin and preparation method thereof |
| CN101156589A (en) * | 2007-11-27 | 2008-04-09 | 北京有色金属研究总院 | Caspase inhibitors and the use thereof |
| CN101180974A (en) * | 2007-12-21 | 2008-05-21 | 吕学良 | Yellow humic acid rare earths seed-dressing agent for resisting take-all of wheat |
| CN105248460A (en) * | 2015-10-09 | 2016-01-20 | 广州潮徽化工科技有限公司 | Compound antimicrobial composition containing microcapsules and preparation method and application of compound antimicrobial composition |
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Application publication date: 20180323 |