CN101104586B - 丙烯酸酯的制备方法 - Google Patents

丙烯酸酯的制备方法 Download PDF

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Publication number
CN101104586B
CN101104586B CN2007101124800A CN200710112480A CN101104586B CN 101104586 B CN101104586 B CN 101104586B CN 2007101124800 A CN2007101124800 A CN 2007101124800A CN 200710112480 A CN200710112480 A CN 200710112480A CN 101104586 B CN101104586 B CN 101104586B
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China
Prior art keywords
acrylate
tower
acid
knockout tower
boils
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Chinese (zh)
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CN101104586A (zh
Inventor
原槇英文
松井学
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Nippon Shokubai Co Ltd
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Nippon Shokubai Co Ltd
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Publication of CN101104586A publication Critical patent/CN101104586A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN2007101124800A 2006-07-11 2007-06-28 丙烯酸酯的制备方法 Active CN101104586B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2006-190889 2006-07-11
JP2006190889A JP4160087B2 (ja) 2006-07-11 2006-07-11 アクリル酸エステルの製造方法
JP2006190889 2006-07-11

Publications (2)

Publication Number Publication Date
CN101104586A CN101104586A (zh) 2008-01-16
CN101104586B true CN101104586B (zh) 2011-06-08

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ID=38950102

Family Applications (1)

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CN2007101124800A Active CN101104586B (zh) 2006-07-11 2007-06-28 丙烯酸酯的制备方法

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US (1) US7491841B2 (enExample)
JP (1) JP4160087B2 (enExample)
CN (1) CN101104586B (enExample)
SA (1) SA07280369B1 (enExample)
TW (1) TW200808716A (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102008060218A1 (de) * 2008-12-04 2010-06-10 Evonik Stockhausen Gmbh Aufarbeitungsverfahren bei der Herstellung von (Meth)Acrylsäurealkylestern
TWI415836B (zh) * 2011-10-19 2013-11-21 Shiny Chemical Ind Co Ltd A process for preparing an alkyl diol alkyl ether (meth) acrylate
FR2982258B1 (fr) * 2011-11-04 2013-11-15 Arkema France Procede de production d'acrylate de 2-octyle par esterification directe
CN102675098A (zh) * 2012-05-29 2012-09-19 江门谦信化工发展有限公司 一种丙烯酸丁酯连续生产新工艺
CN104761450B (zh) * 2012-12-20 2016-08-24 常州市松盛香料有限公司 丙酸乙酯的制备方法
FR3024143B1 (fr) * 2014-07-28 2016-07-15 Arkema France Procede perfectionne de fabrication de (meth)acrylates d'alkyle
CN107011165B (zh) * 2017-04-24 2020-07-03 朱大春 Uv光固化单体连续化生产方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3882167A (en) * 1972-06-02 1975-05-06 Hoechst Ag Process for the manufacture of acrylic acid esters
US4956493A (en) * 1987-04-16 1990-09-11 Nippon Shokubai Kagaku Kogyo Co., Ltd. Process for producing methacrylic ester
CN1164528A (zh) * 1996-02-06 1997-11-12 巴斯福股份公司 (甲基)丙烯酸烷基酯的连续制备方法
CN1326431A (zh) * 1998-11-11 2001-12-12 巴斯福股份公司 (甲基)丙烯酸烷基酯的连续制备

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2548561C2 (de) 1975-10-30 1983-09-29 Hoechst Ag, 6230 Frankfurt Verfahren zur kontinuierlichen Herstellung dioctylätherfreien 2-Äthyl- hexylacrylats
JPS58159442A (ja) 1982-03-17 1983-09-21 Nippon Kayaku Co Ltd アクリル酸エステル又はメタクリル酸エステルの製造方法
JPS63275544A (ja) 1987-05-06 1988-11-14 Osaka Yuki Kagaku Kogyo Kk エステルの安定化方法
JPH0686406B2 (ja) 1989-04-21 1994-11-02 株式会社日本触媒 アクリル酸エステルの製造方法
JPH0764791B2 (ja) 1989-06-30 1995-07-12 出光石油化学株式会社 アクリル酸エステル又はメタクリル酸エステルの製造方法
JPH0686407B2 (ja) 1989-07-21 1994-11-02 株式会社日本触媒 メタクリル酸エステルの製造方法
JPH0699365B2 (ja) 1989-07-21 1994-12-07 株式会社日本触媒 アクリル酸エステルの製造法
DE3935470A1 (de) 1989-10-25 1991-05-02 Hoechst Ag Verfahren zur kontinuierlichen herstellung von estern niederer aliphatischer carbonsaeuren mit niederen alkoholen
US6649787B1 (en) * 1999-10-12 2003-11-18 Nippon Shokubai Co., Ltd. Method for preparing (meth) acrylic acid ester
JP3981550B2 (ja) 2001-12-03 2007-09-26 三菱化学株式会社 アクリル酸エステルの製造方法
JP2003226669A (ja) 2001-11-28 2003-08-12 Mitsubishi Chemicals Corp （メタ）アクリル酸エステルの製造方法
DE10200171A1 (de) * 2002-01-04 2003-07-10 Roehm Gmbh Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3882167A (en) * 1972-06-02 1975-05-06 Hoechst Ag Process for the manufacture of acrylic acid esters
US4956493A (en) * 1987-04-16 1990-09-11 Nippon Shokubai Kagaku Kogyo Co., Ltd. Process for producing methacrylic ester
CN1164528A (zh) * 1996-02-06 1997-11-12 巴斯福股份公司 (甲基)丙烯酸烷基酯的连续制备方法
CN1326431A (zh) * 1998-11-11 2001-12-12 巴斯福股份公司 (甲基)丙烯酸烷基酯的连续制备

Also Published As

Publication number Publication date
CN101104586A (zh) 2008-01-16
JP2008019189A (ja) 2008-01-31
SA07280369B1 (ar) 2011-10-08
TWI353976B (enExample) 2011-12-11
JP4160087B2 (ja) 2008-10-01
US7491841B2 (en) 2009-02-17
TW200808716A (en) 2008-02-16
US20080015384A1 (en) 2008-01-17

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