CN101044129A - 氧化烯烃和过氧化物的制备方法、反应器和其用途 - Google Patents

氧化烯烃和过氧化物的制备方法、反应器和其用途 Download PDF

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Publication number
CN101044129A
CN101044129A CNA2005800349897A CN200580034989A CN101044129A CN 101044129 A CN101044129 A CN 101044129A CN A2005800349897 A CNA2005800349897 A CN A2005800349897A CN 200580034989 A CN200580034989 A CN 200580034989A CN 101044129 A CN101044129 A CN 101044129A
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CN
China
Prior art keywords
reaction
reaction space
space
catalyst
reactor
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Pending
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CNA2005800349897A
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English (en)
Chinese (zh)
Inventor
S·席尔迈斯特
B·朗甘克
K·比克尔
F·贝克尔
J·阿尔布雷希特
G·马尔科夫兹
R·许特
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ThyssenKrupp Industrial Solutions AG
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Krupp Uhde GmbH
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Publication of CN101044129A publication Critical patent/CN101044129A/zh
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/249—Plate-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0246—Coatings comprising a zeolite
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00891—Feeding or evacuation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2451—Geometry of the reactor
    • B01J2219/2453—Plates arranged in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2469—Feeding means
    • B01J2219/247—Feeding means for the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2476—Construction materials
    • B01J2219/2477—Construction materials of the catalysts
    • B01J2219/2479—Catalysts coated on the surface of plates or inserts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNA2005800349897A 2004-10-15 2005-09-16 氧化烯烃和过氧化物的制备方法、反应器和其用途 Pending CN101044129A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102004050506A DE102004050506A1 (de) 2004-10-15 2004-10-15 Verfahren zur Herstellung von Olefinoxiden und Peroxiden, Reaktor und dessen Verwendung
DE102004050506.3 2004-10-15

Publications (1)

Publication Number Publication Date
CN101044129A true CN101044129A (zh) 2007-09-26

Family

ID=35432495

Family Applications (1)

Application Number Title Priority Date Filing Date
CNA2005800349897A Pending CN101044129A (zh) 2004-10-15 2005-09-16 氧化烯烃和过氧化物的制备方法、反应器和其用途

Country Status (17)

Country Link
US (1) US20080306288A1 (enExample)
EP (1) EP1802596A1 (enExample)
JP (1) JP2008516900A (enExample)
KR (1) KR20070063004A (enExample)
CN (1) CN101044129A (enExample)
AU (1) AU2005297530A1 (enExample)
BR (1) BRPI0516517A (enExample)
CA (1) CA2584049A1 (enExample)
DE (1) DE102004050506A1 (enExample)
EA (1) EA013086B1 (enExample)
EG (1) EG24502A (enExample)
HR (1) HRP20070150A2 (enExample)
MX (1) MX2007004501A (enExample)
NO (1) NO20072459L (enExample)
NZ (1) NZ554394A (enExample)
WO (1) WO2006042598A1 (enExample)
ZA (1) ZA200702469B (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109999821A (zh) * 2019-03-12 2019-07-12 内蒙古工业大学 一种表面处理的铝合金催化剂的制备及其应用
CN112159369A (zh) * 2015-11-26 2021-01-01 赢创运营有限公司 用于烯烃环氧化的反应器
CN112979587A (zh) * 2019-12-12 2021-06-18 中国科学院大连化学物理研究所 一种微通道反应器合成环氧丙烷的方法
CN113333029A (zh) * 2021-06-29 2021-09-03 南京先进生物材料与过程装备研究院有限公司 金属改性bea与卟啉配位的复合催化剂及其在环己烯选择性环氧化反应中的应用

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ZA200610755B (en) * 2005-12-22 2008-05-28 Shell Int Research A process for the preparation of an olefin oxide or a chemical derivable from an olefin oxide
US7750170B2 (en) 2005-12-22 2010-07-06 Shell Oil Company Process for mixing an oxidant having explosive potential with a hydrocarbon
US7459589B2 (en) 2005-12-22 2008-12-02 Shell Oil Company Process for the preparation of an alkylene glycol
JP5163921B2 (ja) * 2006-03-01 2013-03-13 荒川化学工業株式会社 エポキシ化合物の製造方法
DE102006015268A1 (de) * 2006-04-01 2007-10-25 Cognis Ip Management Gmbh Verfahren zur Herstellung von Alkylenoxiden
CN101279957B (zh) * 2007-04-04 2012-07-04 中国石油化工股份有限公司 丙烯环氧化制备环氧丙烷的方法
DE102009003466A1 (de) * 2009-02-11 2010-08-19 Karlsruher Institut für Technologie Hexaalkylguanidiniumsalze
JP5757126B2 (ja) * 2011-03-28 2015-07-29 日産化学工業株式会社 フローリアクターを用いたシャープレス不斉エポキシ化反応
US9481741B2 (en) 2012-11-26 2016-11-01 Lummus Novolen Technology Gmbh High performance Ziegler-Natta catalyst systems, process for producing such supported catalysts and use thereof
EP3954743A1 (de) 2020-08-12 2022-02-16 Evonik Operations GmbH Verwendung von siliziumdioxid zur verbesserung der leitfähigkeit von beschichtungen

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NL8502144A (nl) * 1985-07-27 1987-02-16 Stamicarbon Katalysator en werkwijze voor de katalytische heterogene gasfaseoxidatie van alkenen en cycloalkenen volgens de wacker-route.
DE4241942A1 (de) * 1992-12-11 1994-06-16 Basf Ag Verfahren zur Herstellung von 3,4-Epoxy-1-buten
DE69426907T2 (de) * 1993-08-11 2001-09-27 Mitsubishi Gas Chemical Co., Inc. Titanosilikate Katalysatorteilchen
DE19731627A1 (de) * 1997-07-23 1999-01-28 Degussa Granulate, enthaltend Titansilikalit-l
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DE10002514A1 (de) * 2000-01-21 2001-07-26 Degussa Verfahren zur Herstellung von Olefinoxiden in der Gasphase
DE10042746A1 (de) * 2000-08-31 2002-03-28 Degussa Verfahren und Vorrichtung zum Durchführen von Reaktionen in einem Reaktor mit spaltförmigen Reaktionsräumen
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Publication number Priority date Publication date Assignee Title
CN112159369A (zh) * 2015-11-26 2021-01-01 赢创运营有限公司 用于烯烃环氧化的反应器
CN109999821A (zh) * 2019-03-12 2019-07-12 内蒙古工业大学 一种表面处理的铝合金催化剂的制备及其应用
CN109999821B (zh) * 2019-03-12 2021-11-16 内蒙古工业大学 一种表面处理的铝合金催化剂的制备及其应用
CN112979587A (zh) * 2019-12-12 2021-06-18 中国科学院大连化学物理研究所 一种微通道反应器合成环氧丙烷的方法
CN112979587B (zh) * 2019-12-12 2022-12-02 中国科学院大连化学物理研究所 一种微通道反应器合成环氧丙烷的方法
CN113333029A (zh) * 2021-06-29 2021-09-03 南京先进生物材料与过程装备研究院有限公司 金属改性bea与卟啉配位的复合催化剂及其在环己烯选择性环氧化反应中的应用
CN113333029B (zh) * 2021-06-29 2023-08-25 南京先进生物材料与过程装备研究院有限公司 金属改性bea与卟啉配位的复合催化剂及其在环己烯选择性环氧化反应中的应用

Also Published As

Publication number Publication date
NZ554394A (en) 2009-10-30
US20080306288A1 (en) 2008-12-11
ZA200702469B (en) 2008-12-31
KR20070063004A (ko) 2007-06-18
AU2005297530A1 (en) 2006-04-27
BRPI0516517A (pt) 2008-09-16
EP1802596A1 (de) 2007-07-04
DE102004050506A1 (de) 2006-04-20
NO20072459L (no) 2007-06-29
EA013086B1 (ru) 2010-02-26
MX2007004501A (es) 2007-05-09
CA2584049A1 (en) 2006-04-27
WO2006042598A1 (de) 2006-04-27
JP2008516900A (ja) 2008-05-22
HRP20070150A2 (hr) 2007-08-31
EG24502A (en) 2009-08-18
EA200700873A1 (ru) 2007-08-31

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