KR20070063004A - 올레핀 옥사이드 및 과산화물의 제조방법, 반응기 및 이의용도 - Google Patents

올레핀 옥사이드 및 과산화물의 제조방법, 반응기 및 이의용도 Download PDF

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Publication number
KR20070063004A
KR20070063004A KR1020077008549A KR20077008549A KR20070063004A KR 20070063004 A KR20070063004 A KR 20070063004A KR 1020077008549 A KR1020077008549 A KR 1020077008549A KR 20077008549 A KR20077008549 A KR 20077008549A KR 20070063004 A KR20070063004 A KR 20070063004A
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South Korea
Prior art keywords
reaction space
reaction
catalyst
oxide
reactor
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KR1020077008549A
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English (en)
Korean (ko)
Inventor
슈테펜 쉬르마이스터
베른트 란간케
카르스텐 뷔커
프랑크 벡커
요한네스 알브레흐트
게오르크 마르코브츠
뤼디거 쉿테
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우데 게엠베하
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/249—Plate-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0246—Coatings comprising a zeolite
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00891—Feeding or evacuation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2451—Geometry of the reactor
    • B01J2219/2453—Plates arranged in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2469—Feeding means
    • B01J2219/247—Feeding means for the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2476—Construction materials
    • B01J2219/2477—Construction materials of the catalysts
    • B01J2219/2479—Catalysts coated on the surface of plates or inserts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020077008549A 2004-10-15 2005-09-16 올레핀 옥사이드 및 과산화물의 제조방법, 반응기 및 이의용도 Withdrawn KR20070063004A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102004050506.3 2004-10-15
DE102004050506A DE102004050506A1 (de) 2004-10-15 2004-10-15 Verfahren zur Herstellung von Olefinoxiden und Peroxiden, Reaktor und dessen Verwendung

Publications (1)

Publication Number Publication Date
KR20070063004A true KR20070063004A (ko) 2007-06-18

Family

ID=35432495

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020077008549A Withdrawn KR20070063004A (ko) 2004-10-15 2005-09-16 올레핀 옥사이드 및 과산화물의 제조방법, 반응기 및 이의용도

Country Status (17)

Country Link
US (1) US20080306288A1 (enExample)
EP (1) EP1802596A1 (enExample)
JP (1) JP2008516900A (enExample)
KR (1) KR20070063004A (enExample)
CN (1) CN101044129A (enExample)
AU (1) AU2005297530A1 (enExample)
BR (1) BRPI0516517A (enExample)
CA (1) CA2584049A1 (enExample)
DE (1) DE102004050506A1 (enExample)
EA (1) EA013086B1 (enExample)
EG (1) EG24502A (enExample)
HR (1) HRP20070150A2 (enExample)
MX (1) MX2007004501A (enExample)
NO (1) NO20072459L (enExample)
NZ (1) NZ554394A (enExample)
WO (1) WO2006042598A1 (enExample)
ZA (1) ZA200702469B (enExample)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7750170B2 (en) 2005-12-22 2010-07-06 Shell Oil Company Process for mixing an oxidant having explosive potential with a hydrocarbon
BE1017793A3 (fr) * 2005-12-22 2009-07-07 Shell Int Research Procede de preparation d'un oxyde d'olefine ou d'un produit chimique pouvant provenir d'un oxyde d'olefine.
US7459589B2 (en) 2005-12-22 2008-12-02 Shell Oil Company Process for the preparation of an alkylene glycol
JP5163921B2 (ja) * 2006-03-01 2013-03-13 荒川化学工業株式会社 エポキシ化合物の製造方法
DE202006020415U1 (de) 2006-04-01 2008-07-03 Cognis Ip Management Gmbh Verwendung von Mikroreaktionssystemen
CN101279957B (zh) * 2007-04-04 2012-07-04 中国石油化工股份有限公司 丙烯环氧化制备环氧丙烷的方法
DE102009003466A1 (de) * 2009-02-11 2010-08-19 Karlsruher Institut für Technologie Hexaalkylguanidiniumsalze
JP5757126B2 (ja) * 2011-03-28 2015-07-29 日産化学工業株式会社 フローリアクターを用いたシャープレス不斉エポキシ化反応
US9481741B2 (en) 2012-11-26 2016-11-01 Lummus Novolen Technology Gmbh High performance Ziegler-Natta catalyst systems, process for producing such supported catalysts and use thereof
MY184843A (en) * 2015-11-26 2021-04-26 Evonik Operations Gmbh Process for the epoxidation of an olefin
CN109999821B (zh) * 2019-03-12 2021-11-16 内蒙古工业大学 一种表面处理的铝合金催化剂的制备及其应用
CN112979587B (zh) * 2019-12-12 2022-12-02 中国科学院大连化学物理研究所 一种微通道反应器合成环氧丙烷的方法
EP3954743A1 (de) 2020-08-12 2022-02-16 Evonik Operations GmbH Verwendung von siliziumdioxid zur verbesserung der leitfähigkeit von beschichtungen
CN113333029B (zh) * 2021-06-29 2023-08-25 南京先进生物材料与过程装备研究院有限公司 金属改性bea与卟啉配位的复合催化剂及其在环己烯选择性环氧化反应中的应用

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4374260A (en) * 1976-08-30 1983-02-15 Texaco Inc. Ethylene oxide production
NL8502144A (nl) * 1985-07-27 1987-02-16 Stamicarbon Katalysator en werkwijze voor de katalytische heterogene gasfaseoxidatie van alkenen en cycloalkenen volgens de wacker-route.
DE4241942A1 (de) * 1992-12-11 1994-06-16 Basf Ag Verfahren zur Herstellung von 3,4-Epoxy-1-buten
DE69426907T2 (de) * 1993-08-11 2001-09-27 Mitsubishi Gas Chemical Co., Inc. Titanosilikate Katalysatorteilchen
DE19731627A1 (de) * 1997-07-23 1999-01-28 Degussa Granulate, enthaltend Titansilikalit-l
DE19748481C2 (de) * 1997-11-03 2003-09-25 Inst Mikrotechnik Mainz Gmbh Statischer Mikrovermischer
DE19841993B4 (de) * 1998-09-04 2005-02-17 P21 - Power For The 21St Century Gmbh Mikrostruktur-Reaktor
US6488838B1 (en) * 1999-08-17 2002-12-03 Battelle Memorial Institute Chemical reactor and method for gas phase reactant catalytic reactions
CA2381154C (en) * 1999-08-17 2009-02-03 Battelle Memorial Institute Chemical reactor and method for catalytic gas phase reactions
DE10002514A1 (de) * 2000-01-21 2001-07-26 Degussa Verfahren zur Herstellung von Olefinoxiden in der Gasphase
DE10042746A1 (de) * 2000-08-31 2002-03-28 Degussa Verfahren und Vorrichtung zum Durchführen von Reaktionen in einem Reaktor mit spaltförmigen Reaktionsräumen
DE10111747A1 (de) * 2000-09-12 2002-09-19 Penth Bernd Mikrorektor mit Katalyse
US6969505B2 (en) * 2002-08-15 2005-11-29 Velocys, Inc. Process for conducting an equilibrium limited chemical reaction in a single stage process channel
DE10248599A1 (de) * 2002-10-17 2004-04-29 Degussa Ag Verfahren zur Gewinnung einer gasförmigen Phase aus einem flüssigen Medium und Vorrichtung zu seiner Durchführung
EP1415706B1 (en) * 2002-10-29 2017-07-12 Corning Incorporated Coated microstructure and method of manufacture
DE10317451A1 (de) * 2003-04-16 2004-11-18 Degussa Ag Reaktor für heterogen katalysierte Reaktionen
US7294734B2 (en) * 2003-05-02 2007-11-13 Velocys, Inc. Process for converting a hydrocarbon to an oxygenate or a nitrile
US7220390B2 (en) * 2003-05-16 2007-05-22 Velocys, Inc. Microchannel with internal fin support for catalyst or sorption medium
US7029647B2 (en) * 2004-01-27 2006-04-18 Velocys, Inc. Process for producing hydrogen peroxide using microchannel technology
US7442360B2 (en) * 2004-04-27 2008-10-28 Velocys, Inc. Hydrogen peroxide production in microchannel reactors

Also Published As

Publication number Publication date
MX2007004501A (es) 2007-05-09
EG24502A (en) 2009-08-18
DE102004050506A1 (de) 2006-04-20
NZ554394A (en) 2009-10-30
AU2005297530A1 (en) 2006-04-27
WO2006042598A1 (de) 2006-04-27
CN101044129A (zh) 2007-09-26
US20080306288A1 (en) 2008-12-11
ZA200702469B (en) 2008-12-31
HRP20070150A2 (hr) 2007-08-31
EP1802596A1 (de) 2007-07-04
EA013086B1 (ru) 2010-02-26
CA2584049A1 (en) 2006-04-27
EA200700873A1 (ru) 2007-08-31
BRPI0516517A (pt) 2008-09-16
NO20072459L (no) 2007-06-29
JP2008516900A (ja) 2008-05-22

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Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20070413

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
PC1203 Withdrawal of no request for examination
WITN Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid