CN100469813C - 连续制备高分子量聚酯的方法和实施该方法的装置 - Google Patents

连续制备高分子量聚酯的方法和实施该方法的装置 Download PDF

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Publication number
CN100469813C
CN100469813C CNB028270207A CN02827020A CN100469813C CN 100469813 C CN100469813 C CN 100469813C CN B028270207 A CNB028270207 A CN B028270207A CN 02827020 A CN02827020 A CN 02827020A CN 100469813 C CN100469813 C CN 100469813C
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reaction
temperature
zone
pressure
product
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CN1612907A (zh
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E·舒尔茨范恩德尔特
R·哈根
T·希勒
C·阿特拉斯
U·蒂勒
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Uhde Inventa Fischer GmbH
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Inventa Fischer GmbH and Co KG
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/785—Preparation processes characterised by the apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1887—Stationary reactors having moving elements inside forming a thin film
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/82—Preparation processes characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • C08J3/22—Compounding polymers with additives, e.g. colouring using masterbatch techniques
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
    • B01J2219/0011—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant liquids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
CNB028270207A 2001-11-12 2002-11-11 连续制备高分子量聚酯的方法和实施该方法的装置 Expired - Fee Related CN100469813C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10155419A DE10155419B4 (de) 2001-11-12 2001-11-12 Verfahren zur kontinuierlichen Herstellung von hochmolekularem Polyester sowie Vorrichtung zur Durchführung des Verfahrens
DE10155419.2 2001-11-12

Publications (2)

Publication Number Publication Date
CN1612907A CN1612907A (zh) 2005-05-04
CN100469813C true CN100469813C (zh) 2009-03-18

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US (2) US7115701B2 (enExample)
EP (1) EP1448658B1 (enExample)
JP (1) JP2005519141A (enExample)
KR (1) KR100776859B1 (enExample)
CN (1) CN100469813C (enExample)
AT (1) ATE388184T1 (enExample)
DE (2) DE10155419B4 (enExample)
ES (1) ES2300491T3 (enExample)
MX (1) MXPA04004426A (enExample)
TW (1) TW593408B (enExample)
WO (1) WO2003042278A1 (enExample)

Cited By (1)

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CN109400856A (zh) * 2018-09-26 2019-03-01 浙江恒澜科技有限公司 一种采用金属复合催化剂催化合成高特性粘度且良好色相的聚对苯二甲酸丙二醇酯的方法

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DE102005013764B3 (de) * 2005-03-22 2006-10-12 Epc Industrial Engineering Gmbh Modulare Vorrichtung zur kontinuierlichen Entgasung und Herstellung polymerer Vorkondensate, mit reaktionstechnisch hohem Verhältnis Produktoberfläche zu Volumen, bei schonender Behandlung der Reaktionsproduktmasse
US7718137B2 (en) * 2005-10-28 2010-05-18 Eastman Chemical Company Reactor with optimized internal tray design
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CN102492127B (zh) * 2011-11-22 2013-06-12 浙江尤夫高新纤维股份有限公司 列管式缩聚反应釜
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CN110433513B (zh) * 2019-09-12 2023-05-23 张健 降膜管
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JP2023506396A (ja) * 2019-12-19 2023-02-16 ディーエスエム アイピー アセッツ ビー．ブイ． 連続固相重合方法及びそこで使用するための反応器カラム
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CN117659362A (zh) * 2022-08-31 2024-03-08 科泽新材料股份有限公司 一种制备pent共聚酯的方法
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Publication number Priority date Publication date Assignee Title
CN109400856A (zh) * 2018-09-26 2019-03-01 浙江恒澜科技有限公司 一种采用金属复合催化剂催化合成高特性粘度且良好色相的聚对苯二甲酸丙二醇酯的方法

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TW593408B (en) 2004-06-21
EP1448658A1 (de) 2004-08-25
ATE388184T1 (de) 2008-03-15
US20050163679A1 (en) 2005-07-28
JP2005519141A (ja) 2005-06-30
WO2003042278A1 (de) 2003-05-22
KR20050002807A (ko) 2005-01-10
ES2300491T3 (es) 2008-06-16
CN1612907A (zh) 2005-05-04
DE10155419B4 (de) 2005-06-16
MXPA04004426A (es) 2005-05-16
US7259227B2 (en) 2007-08-21
KR100776859B1 (ko) 2007-12-12
DE10155419A1 (de) 2003-05-28
US20070066790A1 (en) 2007-03-22
US7115701B2 (en) 2006-10-03
DE50211853D1 (de) 2008-04-17
EP1448658B1 (de) 2008-03-05

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