CN100418993C - 活性起始混合物及相关方法 - Google Patents

活性起始混合物及相关方法 Download PDF

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Publication number
CN100418993C
CN100418993C CNB031550290A CN03155029A CN100418993C CN 100418993 C CN100418993 C CN 100418993C CN B031550290 A CNB031550290 A CN B031550290A CN 03155029 A CN03155029 A CN 03155029A CN 100418993 C CN100418993 C CN 100418993C
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CN
China
Prior art keywords
initial compounds
equivalent
glycol
mixture
semi
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB031550290A
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English (en)
Chinese (zh)
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CN1487000A (zh
Inventor
J·E·哈耶斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Koth A Ltd By Share Ltd
Original Assignee
Bayer Antwerpen NV
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Publication of CN1487000A publication Critical patent/CN1487000A/zh
Application granted granted Critical
Publication of CN100418993C publication Critical patent/CN100418993C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4866—Polyethers having a low unsaturation value
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CNB031550290A 2002-07-19 2003-07-18 活性起始混合物及相关方法 Expired - Fee Related CN100418993C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/199,916 US6835801B2 (en) 2002-07-19 2002-07-19 Activated starter mixtures and the processes related thereto
US10/199916 2002-07-19

Publications (2)

Publication Number Publication Date
CN1487000A CN1487000A (zh) 2004-04-07
CN100418993C true CN100418993C (zh) 2008-09-17

Family

ID=29780237

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB031550290A Expired - Fee Related CN100418993C (zh) 2002-07-19 2003-07-18 活性起始混合物及相关方法

Country Status (15)

Country Link
US (1) US6835801B2 (ja)
EP (1) EP1382629B1 (ja)
JP (1) JP4574964B2 (ja)
KR (1) KR100961362B1 (ja)
CN (1) CN100418993C (ja)
AT (1) ATE415437T1 (ja)
BR (1) BR0302450A (ja)
CA (1) CA2434864C (ja)
DE (1) DE60324864D1 (ja)
ES (1) ES2316672T3 (ja)
HK (1) HK1064395A1 (ja)
MX (1) MXPA03006392A (ja)
PL (1) PL214395B1 (ja)
PT (1) PT1382629E (ja)
RU (1) RU2346959C2 (ja)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080108719A1 (en) * 1999-10-25 2008-05-08 Geiger Eric J Phthalic Anhydride Based Polyester-Ether Polyols and Double Metal Cyanide Catalyst System for Preparing Same
US6696383B1 (en) * 2002-09-20 2004-02-24 Bayer Polymers Llc Double-metal cyanide catalysts which can be used to prepare polyols and the processes related thereto
US20060223979A1 (en) * 2005-04-04 2006-10-05 Thomas Ostrowski Process for preparing polyether polyols
DE102007057147A1 (de) 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Alkoxylierung mit DMC-Katalysatoren im Schlaufenreaktor mit Strahlsauger
EP2241584B1 (en) 2008-01-25 2012-03-21 Kaneka Corporation Process for producing polyalkylene oxide
US20100324340A1 (en) * 2009-06-23 2010-12-23 Bayer Materialscience Llc Short chain polyether polyols prepared from ultra-low water-content starters via dmc catalysis
GB2482176A (en) * 2010-07-23 2012-01-25 Christopher Wickham Noakes Production of polyols for use in low ball rebound polyurethane foams
KR20180023906A (ko) * 2015-07-02 2018-03-07 코베스트로 엘엘씨 Ｄｍｃ 촉매 및 출발물의 연속적 첨가를 사용한 폴리에테르 폴리올의 제조 방법
US9879114B2 (en) * 2015-12-22 2018-01-30 Covestro Llc Process for the production of low molecular weight polyoxyalkylene polyols
CN107200837B (zh) 2016-03-18 2019-10-18 淮安巴德聚氨酯科技有限公司 一种利用dmc催化剂循环制备聚醚多元醇的方法
US10873316B2 (en) * 2017-03-02 2020-12-22 Samsung Electro-Mechanics Co., Ltd. Acoustic resonator and method of manufacturing the same
CN109679085B (zh) * 2019-01-18 2022-02-08 上海东大化学有限公司 一种窄分布无规聚醚及其制备方法
CN113348191B (zh) 2019-01-31 2023-06-30 陶氏环球技术有限责任公司 无雾聚氨酯制剂
EP4279534A1 (en) 2022-05-20 2023-11-22 PCC ROKITA Spolka Akcyjna A method for producing low unsaturation level oxyalkylates, an oxyalkylate, a use thereof and a polyurethane foam

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0459825A (ja) * 1990-06-29 1992-02-26 Asahi Glass Co Ltd ポリエーテル類の製造方法
CN1210549A (zh) * 1996-02-07 1999-03-10 阿克奥化学技术公司 通过连续加入起始物进行双金属氰化物催化多醇的制备

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3278459A (en) 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
US3278457A (en) 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
US3427256A (en) 1963-02-14 1969-02-11 Gen Tire & Rubber Co Double metal cyanide complex compounds
US3829505A (en) 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3941849A (en) 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
AU551979B2 (en) 1982-03-31 1986-05-15 Shell Internationale Research Maatschappij B.V. Epoxy polymerisation catalysts
AU552988B2 (en) 1982-03-31 1986-06-26 Shell Internationale Research Maatschappij B.V. Polymerizing epoxides and catalyst suspensions for this
JP3025312B2 (ja) * 1990-12-18 2000-03-27 旭硝子株式会社 ポリエーテル類の製造法
JPH0517569A (ja) 1991-07-08 1993-01-26 Asahi Glass Co Ltd ポリエーテル類の製造方法
JP3085740B2 (ja) 1991-07-17 2000-09-11 旭硝子株式会社 ポリエーテル類の製造方法
US5158922A (en) 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
JP3114481B2 (ja) * 1993-05-25 2000-12-04 トヨタ自動車株式会社 作業負担評価指数の算出方法とそのための装置とそれを利用した作業工程計画方法
US5470813A (en) 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5563221A (en) 1995-06-21 1996-10-08 Arco Chemical Technology, L.P. Process for making ethylene oxide-capped polyols from double metal cyanide-catalyzed polyols
US5545601A (en) 1995-08-22 1996-08-13 Arco Chemical Technology, L.P. Polyether-containing double metal cyanide catalysts
US5767323A (en) * 1995-12-22 1998-06-16 Arco Chemical Technology, L.P. Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation
US5639705A (en) 1996-01-19 1997-06-17 Arco Chemical Technology, L.P. Double metal cyanide catalysts and methods for making them
US5689012A (en) 1996-07-18 1997-11-18 Arco Chemical Technology, L.P. Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter
US5844070A (en) 1997-05-16 1998-12-01 Arco Chemical Technology, L.P. Process for rapid activation of double metal cyanide catalysts
US6077978A (en) * 1997-09-17 2000-06-20 Arco Chemical Technology L.P. Direct polyoxyalkylation of glycerine with double metal cyanide catalysis
BR0013193A (pt) 1999-07-09 2002-07-02 Dow Chemical Co Polimerização de óxido de etileno usando catalisadores de cianeto metálico
US6359101B1 (en) 1999-12-15 2002-03-19 Synuthane International, Inc. Preparing polyether polyols with DMC catalysts
US6491846B1 (en) 2001-06-21 2002-12-10 Bayer Antwerpen, N.V. Process for the in-situ production of polyol blends, the in-situ produced polyol blends, and their use in the production of viscoelastic foam

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0459825A (ja) * 1990-06-29 1992-02-26 Asahi Glass Co Ltd ポリエーテル類の製造方法
CN1210549A (zh) * 1996-02-07 1999-03-10 阿克奥化学技术公司 通过连续加入起始物进行双金属氰化物催化多醇的制备

Also Published As

Publication number Publication date
HK1064395A1 (ja) 2005-01-28
CA2434864C (en) 2010-09-14
KR100961362B1 (ko) 2010-06-04
CA2434864A1 (en) 2004-01-19
JP4574964B2 (ja) 2010-11-04
US20040014908A1 (en) 2004-01-22
ATE415437T1 (de) 2008-12-15
ES2316672T3 (es) 2009-04-16
PL361330A1 (en) 2004-01-26
DE60324864D1 (de) 2009-01-08
CN1487000A (zh) 2004-04-07
BR0302450A (pt) 2004-08-24
KR20040010239A (ko) 2004-01-31
PT1382629E (pt) 2009-02-03
MXPA03006392A (es) 2005-08-16
EP1382629B1 (en) 2008-11-26
EP1382629A1 (en) 2004-01-21
JP2004051996A (ja) 2004-02-19
US6835801B2 (en) 2004-12-28
RU2003122077A (ru) 2005-02-10
RU2346959C2 (ru) 2009-02-20
PL214395B1 (pl) 2013-07-31

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Granted publication date: 20080917