CN100399023C - 一种改进的气相色谱系统 - Google Patents
一种改进的气相色谱系统 Download PDFInfo
- Publication number
- CN100399023C CN100399023C CNB2004100809883A CN200410080988A CN100399023C CN 100399023 C CN100399023 C CN 100399023C CN B2004100809883 A CNB2004100809883 A CN B2004100809883A CN 200410080988 A CN200410080988 A CN 200410080988A CN 100399023 C CN100399023 C CN 100399023C
- Authority
- CN
- China
- Prior art keywords
- pressure
- sample
- closed loop
- coupled
- outlet pathway
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000002347 injection Methods 0.000 claims abstract description 35
- 239000007924 injection Substances 0.000 claims abstract description 35
- 238000004817 gas chromatography Methods 0.000 claims abstract description 24
- 238000005070 sampling Methods 0.000 claims description 8
- 230000008859 change Effects 0.000 claims description 6
- 230000037361 pathway Effects 0.000 claims 14
- 230000007613 environmental effect Effects 0.000 claims 3
- 230000005540 biological transmission Effects 0.000 claims 1
- 230000008878 coupling Effects 0.000 claims 1
- 238000010168 coupling process Methods 0.000 claims 1
- 238000005859 coupling reaction Methods 0.000 claims 1
- 239000000523 sample Substances 0.000 description 84
- 239000007789 gas Substances 0.000 description 19
- 238000000034 method Methods 0.000 description 17
- 238000010586 diagram Methods 0.000 description 12
- 230000008569 process Effects 0.000 description 10
- 238000004458 analytical method Methods 0.000 description 7
- 238000004587 chromatography analysis Methods 0.000 description 7
- 239000012159 carrier gas Substances 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 230000006870 function Effects 0.000 description 5
- 230000003287 optical effect Effects 0.000 description 5
- 238000004891 communication Methods 0.000 description 4
- 230000001276 controlling effect Effects 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- 230000007423 decrease Effects 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000012491 analyte Substances 0.000 description 2
- 238000003491 array Methods 0.000 description 2
- RBFQJDQYXXHULB-UHFFFAOYSA-N arsane Chemical compound [AsH3] RBFQJDQYXXHULB-UHFFFAOYSA-N 0.000 description 2
- 230000033228 biological regulation Effects 0.000 description 2
- 238000004590 computer program Methods 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 239000003345 natural gas Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000538 analytical sample Substances 0.000 description 1
- 229910000070 arsenic hydride Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000012864 cross contamination Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
-
- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D16/00—Control of fluid pressure
- G05D16/20—Control of fluid pressure characterised by the use of electric means
- G05D16/2006—Control of fluid pressure characterised by the use of electric means with direct action of electric energy on controlling means
- G05D16/2013—Control of fluid pressure characterised by the use of electric means with direct action of electric energy on controlling means using throttling means as controlling means
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/32—Control of physical parameters of the fluid carrier of pressure or speed
-
- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D16/00—Control of fluid pressure
- G05D16/20—Control of fluid pressure characterised by the use of electric means
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/0318—Processes
- Y10T137/0396—Involving pressure control
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/7722—Line condition change responsive valves
- Y10T137/7758—Pilot or servo controlled
- Y10T137/7761—Electrically actuated valve
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/8593—Systems
- Y10T137/87917—Flow path with serial valves and/or closures
Landscapes
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- General Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Automation & Control Theory (AREA)
- Analytical Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Sampling And Sample Adjustment (AREA)
- Control Of Fluid Pressure (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/871,930 | 2004-06-18 | ||
| US10/871,930 US7258132B2 (en) | 2004-06-18 | 2004-06-18 | Electronically controlled back pressure regulator |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1710422A CN1710422A (zh) | 2005-12-21 |
| CN100399023C true CN100399023C (zh) | 2008-07-02 |
Family
ID=34839076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100809883A Expired - Lifetime CN100399023C (zh) | 2004-06-18 | 2004-10-26 | 一种改进的气相色谱系统 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US7258132B2 (enExample) |
| JP (1) | JP4719516B2 (enExample) |
| CN (1) | CN100399023C (enExample) |
| DE (1) | DE102004052584A1 (enExample) |
| GB (1) | GB2415267B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104583770A (zh) * | 2012-09-05 | 2015-04-29 | 株式会社岛津制作所 | 顶空试料导入装置与具备该顶空试料导入装置的气相色谱仪 |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8725434B2 (en) * | 2006-12-29 | 2014-05-13 | Saudi Arabian Oil Company | Wellhead hips with automatic testing and self-diagnostics |
| DE102008006266B4 (de) | 2008-01-25 | 2011-06-09 | Dionex Softron Gmbh | Probengeber für die Flüssigkeitschromatographie, insbesondere für die Hochleistungsflüssigkeitschromatographie |
| US8141411B2 (en) * | 2008-09-30 | 2012-03-27 | Thermo Finnigan Llc | Method for determining a low cylinder pressure condition for a gas chromatograph |
| CN101769901B (zh) * | 2008-12-31 | 2012-07-04 | 北京联合大学生物化学工程学院 | 基于fpga的液相色谱数据处理系统 |
| GB2468845B (en) * | 2009-03-23 | 2015-02-11 | Joseph George Poole | Compressed-gas regulator apparatus |
| US9435773B2 (en) | 2009-06-03 | 2016-09-06 | Agilent Technologies, Inc. | Sample injector with metering device balancing pressure differences in an intermediate valve state |
| CN102103381B (zh) * | 2009-12-16 | 2014-06-25 | 上海神开石油化工装备股份有限公司 | 电子压力控制器 |
| US8887586B2 (en) * | 2010-10-29 | 2014-11-18 | Agilent Technologies, Inc. | Head space sampling device and method for detecting leaks in same |
| US9429499B2 (en) | 2010-10-29 | 2016-08-30 | Agilent Technologies, Inc. | Methods, devices, and systems for controlling the rate of gas depressurization within a vial containing a gas sample |
| CA2823258C (en) * | 2011-01-19 | 2016-03-22 | Saudi Arabian Oil Company | Wellhead hips with automatic testing and self-diagnostics |
| WO2012125574A1 (en) * | 2011-03-11 | 2012-09-20 | Brigham Young University | Simple equilibrium distribution sampling device for gc-ms calibration |
| CN102879482A (zh) * | 2011-07-13 | 2013-01-16 | 江苏汉邦科技有限公司 | 超临界流体色谱仪(sfc)以及用于其中的自动背压装置 |
| US9151731B2 (en) * | 2012-01-19 | 2015-10-06 | Idexx Laboratories Inc. | Fluid pressure control device for an analyzer |
| US9804609B2 (en) | 2012-02-22 | 2017-10-31 | Agilent Technologies, Inc. | Mass flow controllers and methods for auto-zeroing flow sensor without shutting off a mass flow controller |
| WO2015171821A1 (en) * | 2014-05-06 | 2015-11-12 | The Regents Of The University Of California | Tracer gas airflow measurement system with high turndown ratio |
| DE202016100451U1 (de) | 2015-06-25 | 2016-02-16 | Dionex Softron Gmbh | Probengeber für die Flüssigkeitschromatographie, insbesondere für die Hochleistungsflüssigkeitschromatographie |
| US11275062B2 (en) | 2016-05-30 | 2022-03-15 | Agilent Technologies, Inc | Sample injection with fluidic connection between fluid drive unit and sample accommodation volume |
| EP3252464B1 (en) | 2016-05-30 | 2024-03-27 | Agilent Technologies, Inc. (A Delaware Corporation) | Injector and method for sample injection with fludic connection between fluid drive unit and sample accomodation volume |
| JP6658906B2 (ja) * | 2016-10-11 | 2020-03-04 | 株式会社島津製作所 | ガスクロマトグラフ |
| IT201700034608A1 (it) * | 2017-03-29 | 2018-09-29 | Thermo Fisher Scient Spa | Metodo di campionamento per l’analisi gascromatografica dello spazio di testa |
| US10508750B2 (en) | 2017-10-04 | 2019-12-17 | DDS Investments, LLC | Hammer union back pressure regulator |
| EP3882737B1 (en) * | 2020-03-20 | 2022-04-27 | Siemens Aktiengesellschaft | Fluid pressure control apparatus |
| US20220146464A1 (en) * | 2020-10-14 | 2022-05-12 | Wyatt Technology Corporation | Performing a separation on a field flow fractonator |
| US20250052731A1 (en) * | 2023-08-11 | 2025-02-13 | Agilent Technologies, Inc. | Methods and systems for estimating gas supply pressure |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08327618A (ja) * | 1995-05-31 | 1996-12-13 | Shimadzu Corp | ガスクロマトグラフの試料導入装置 |
| EP0770869A2 (en) * | 1995-10-23 | 1997-05-02 | The Perkin-Elmer Corporation | Gas chromatographic system with controlled sample transfer |
| CN1376918A (zh) * | 2001-03-22 | 2002-10-30 | 海城市石油化工仪器厂 | 岩石热解气相色谱仪 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3240052A (en) * | 1962-12-31 | 1966-03-15 | Phillips Petroleum Co | Pressure and flow rate regulation in a fluid circulation system |
| US4196612A (en) | 1978-09-13 | 1980-04-08 | Phillips Petroleum Company | Pressure regulator for a chromatograph |
| US4359891A (en) * | 1981-01-05 | 1982-11-23 | The Dow Chemical Company | Repetitive chromatographic apparatus |
| DE3851763T2 (de) * | 1987-01-17 | 1995-03-02 | Jasco Corp | Extraktionsvorrichtung. |
| US5163979A (en) * | 1991-06-27 | 1992-11-17 | The Dow Chemical Company | Pressure programmable gas chromatograph regulator |
| US5476000A (en) * | 1994-03-31 | 1995-12-19 | Hewlett-Packard Company | Retention time stability in a gas chromatographic apparatus |
| US5431712A (en) * | 1994-05-31 | 1995-07-11 | Hewlett-Packard Company | Reconfigurable pneumatic control for split/splitless injection |
| US5567227A (en) | 1995-01-23 | 1996-10-22 | Hewlett-Packard Company | Method for improving the range of stable control of the pneumatic system of a gas chromatograph |
| JPH0996630A (ja) * | 1995-09-29 | 1997-04-08 | Shimadzu Corp | 試料導入装置 |
| NL1010815C2 (nl) * | 1998-12-15 | 2000-06-19 | Chrompack Int Bv | Inrichting en werkwijze voor het regelen van de druk van een gasstroom. |
| JP4020016B2 (ja) | 2003-05-28 | 2007-12-12 | 株式会社島津製作所 | ガスクロマトグラフ |
-
2004
- 2004-06-18 US US10/871,930 patent/US7258132B2/en not_active Expired - Lifetime
- 2004-10-26 CN CNB2004100809883A patent/CN100399023C/zh not_active Expired - Lifetime
- 2004-10-29 DE DE200410052584 patent/DE102004052584A1/de not_active Withdrawn
-
2005
- 2005-05-20 GB GB0510380A patent/GB2415267B/en not_active Expired - Fee Related
- 2005-06-16 JP JP2005175861A patent/JP4719516B2/ja not_active Expired - Lifetime
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08327618A (ja) * | 1995-05-31 | 1996-12-13 | Shimadzu Corp | ガスクロマトグラフの試料導入装置 |
| EP0770869A2 (en) * | 1995-10-23 | 1997-05-02 | The Perkin-Elmer Corporation | Gas chromatographic system with controlled sample transfer |
| CN1376918A (zh) * | 2001-03-22 | 2002-10-30 | 海城市石油化工仪器厂 | 岩石热解气相色谱仪 |
Non-Patent Citations (2)
| Title |
|---|
| 气相色谱六通阀气体进样技巧. 庞增义.分析仪器,第4期. 2003 |
| 气相色谱六通阀气体进样技巧. 庞增义.分析仪器,第4期. 2003 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104583770A (zh) * | 2012-09-05 | 2015-04-29 | 株式会社岛津制作所 | 顶空试料导入装置与具备该顶空试料导入装置的气相色谱仪 |
| CN104583770B (zh) * | 2012-09-05 | 2017-06-23 | 株式会社岛津制作所 | 顶空试料导入装置与具备该顶空试料导入装置的气相色谱仪 |
Also Published As
| Publication number | Publication date |
|---|---|
| GB2415267A (en) | 2005-12-21 |
| US7258132B2 (en) | 2007-08-21 |
| JP2006003360A (ja) | 2006-01-05 |
| GB2415267B (en) | 2008-04-09 |
| GB0510380D0 (en) | 2005-06-29 |
| JP4719516B2 (ja) | 2011-07-06 |
| DE102004052584A1 (de) | 2006-01-12 |
| US20050279408A1 (en) | 2005-12-22 |
| CN1710422A (zh) | 2005-12-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100399023C (zh) | 一种改进的气相色谱系统 | |
| EP0730151B1 (en) | Flow regulation in gas chromatograph | |
| JP3526102B2 (ja) | 流体のクロマトグラフ分析方法 | |
| US5542286A (en) | Method and apparatus for correcting flow and pressure sensor drift in a gas chromatograph | |
| US5339673A (en) | Gas chromatograph and method of using same | |
| US8343258B2 (en) | Apparatus and method for controlling constant mass flow to gas chromatography column | |
| JPH1144682A (ja) | ターゲットクロマトグラフィックシステムの標準化の方法、ターゲットクロマトグラフィックシステムのカラム温度を較正する方法、ターゲットクロマトグラフィックシステムを確認する方法及びクロマトグラフィックシステムの1つ又は複数の特定のパラメータの値を測定する方法 | |
| CN102859459B (zh) | 用于校准气流稀释器的方法和系统 | |
| US5952556A (en) | Gas chromatograph with carrier gas control system | |
| EP0840116B1 (en) | Calibration method for a chromatography column | |
| US8549894B2 (en) | Gas chromatography with ambient pressure stability control | |
| EP1403363B1 (en) | CO2 incubator | |
| JP4345967B2 (ja) | 分析循環路用の流体レギュレータ装置及びクロマトグラフィにおいての前記分析循環路用の流体レギュレータ装置の利用 | |
| AU729790B2 (en) | Flow regulation in gas chromatograph | |
| RU2468363C1 (ru) | Потоковый хроматограф | |
| JP2008164413A (ja) | 排出ガスサンプリング分析システム | |
| EP2315021B1 (en) | Gas chromatography with ambient pressure stability control | |
| JP3075178B2 (ja) | ガスクロマトグラフ装置 | |
| JP7750935B2 (ja) | ガスクロマトグラフィのキャリアガス識別のための方法及びシステム | |
| KR20010090641A (ko) | 샘플주입방식을 이용한 비분산적외선 탄산가스 측정시스템 | |
| Taylor | Electronic flow and pressure control in gas chromatography: opening the lid of the black box! | |
| WO2024243199A1 (en) | Digital gas assist with flow control and gauge | |
| JPH08101176A (ja) | ガスクロマトグラフ | |
| BAKER | Automated stream analysis for process control, Vol. 2 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20080702 |
|
| CX01 | Expiry of patent term |