CL2018003357A1 - Proceso para preparar material adsorbente y proceso para extracción de litio utilizando dicho material. - Google Patents

Proceso para preparar material adsorbente y proceso para extracción de litio utilizando dicho material.

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Publication number
CL2018003357A1
CL2018003357A1 CL2018003357A CL2018003357A CL2018003357A1 CL 2018003357 A1 CL2018003357 A1 CL 2018003357A1 CL 2018003357 A CL2018003357 A CL 2018003357A CL 2018003357 A CL2018003357 A CL 2018003357A CL 2018003357 A1 CL2018003357 A1 CL 2018003357A1
Authority
CL
Chile
Prior art keywords
stage
materials
lithium
adsortion
licl
Prior art date
Application number
CL2018003357A
Other languages
English (en)
Inventor
Malika Boualleg
Fabien Burdet
Yohan Florent Oudart
Original Assignee
Eramet
Ifp Energies Now
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eramet, Ifp Energies Now filed Critical Eramet
Publication of CL2018003357A1 publication Critical patent/CL2018003357A1/es

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/04—Halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/20—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the sorbent material
    • B01D15/206—Packing or coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/046—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing halogens, e.g. halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/2803—Sorbents comprising a binder, e.g. for forming aggregated, agglomerated or granulated products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28052—Several layers of identical or different sorbents stacked in a housing, e.g. in a column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28057—Surface area, e.g. B.E.T specific surface area
    • B01J20/28059—Surface area, e.g. B.E.T specific surface area being less than 100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282—Porous sorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3007—Moulding, shaping or extruding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3071—Washing or leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3085—Chemical treatments not covered by groups B01J20/3007 - B01J20/3078
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/78—Compounds containing aluminium and two or more other elements, with the exception of oxygen and hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/52—Sorbents specially adapted for preparative chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/60—Use in several different columns
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/60—Compounds characterised by their crystallite size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

LA PRESENTE INVENCIÓN TIENE RELACIÓN CON EL CAMPO DE MATERIALES SÓLIDOS PARA LA ABSORCIÓN DE LITIO. EN PARTICULAR, LA PRESENTE INVENCIÓN TIENE RELACIÓN CON UN PROCESO NUEVO PARA PREPARAR UN MATERIAL CRISTALINO SÓLIDO QUE SE FORMA PREFERENTEMENTE EN FORMA DE EXTRUIDOS DE LA FÓRMULA (LICL)X.2AL(OH)3,NH2O CON N ESTANDO ENTRE 0.01 Y10, X ESTANDO ENTRE 0.4 Y 1, COMPRENDIENDO UNA ETAPA A) PARA PRECIPITAR BOEHMITA BAJO CONDICIONES ESPECÍFICAS DE TEMPERATURA Y PH, UNA ETAPA PARA COLOCAR EL PRECIPITADO OBTENIDO EN CONTACTO CON UNA CANTIDAD ESPECÍFICA DE LICL, AL MENOS UNA ETAPA DE FORMACIÓN PREFERENTEMENTE MEDIANTE EXTRUSIÓN, DICHO PROCESO TAMBIÉN COMPRENDIENDO UNA ETAPA DE TRATAMIENTO HIDROTÉRMICO FINAL, TODOS PERMITIENDO UN AUMENTO EN LA CAPACIDAD DE ADSORCIÓN DE LITIO Y EN LAS CINÉTICAS DE ADSORCIÓN DE LOS MATERIALES OBTENIDOS EN COMPARACIÓN CON LOS MATERIALES DE LA TÉCNICA ANTERIOR, CUANDO SON USADOS EN UN PROCESO PARA EXTRAER LITIO DE SOLUCIONES SALINAS.
CL2018003357A 2016-05-25 2018-11-23 Proceso para preparar material adsorbente y proceso para extracción de litio utilizando dicho material. CL2018003357A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1654703A FR3051787B1 (fr) 2016-05-25 2016-05-25 Procede de preparation d'un materiau adsorbant et procede d'extraction de lithium utilisant ledit materiau

Publications (1)

Publication Number Publication Date
CL2018003357A1 true CL2018003357A1 (es) 2019-02-22

Family

ID=57136976

Family Applications (1)

Application Number Title Priority Date Filing Date
CL2018003357A CL2018003357A1 (es) 2016-05-25 2018-11-23 Proceso para preparar material adsorbente y proceso para extracción de litio utilizando dicho material.

Country Status (7)

Country Link
US (1) US11554358B2 (es)
EP (1) EP3464181B1 (es)
CN (1) CN109415219B (es)
AR (1) AR108577A1 (es)
CL (1) CL2018003357A1 (es)
FR (1) FR3051787B1 (es)
WO (1) WO2017202825A1 (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11365128B2 (en) 2017-06-15 2022-06-21 Energysource Minerals Llc Process for selective adsorption and recovery of lithium from natural and synthetic brines
JP2023524467A (ja) 2020-04-28 2023-06-12 １エス１ エナジー インコーポレイテッド リチウム塩の選択抽出のための含酸素金属化合物及びその使用方法
CA3227977A1 (en) * 2021-07-30 2023-02-02 Schlumberger Canada Limited Capillary electrophoresis analysis of lithium in brine
US11904297B1 (en) 2023-01-11 2024-02-20 Iliad Ip Company, Llc Process for manufacturing lithium selective adsorption/separation media

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US4348297A (en) 1979-11-19 1982-09-07 The Dow Chemical Company Crystalline lithium aluminates
EP0103034A1 (en) * 1982-09-09 1984-03-21 The Dow Chemical Company Crystalline lithium aluminates and a process for the preparation thereof
US5599516A (en) 1993-05-24 1997-02-04 Fmc Corporation Recovery of lithium values from brines
CN1243112A (zh) 1999-08-23 2000-02-02 李凤杰 多元增效氮肥添加剂及其制备方法
DE10197095D2 (de) * 2001-10-25 2004-09-16 Eurosina Technology Consulting Verfahren zur Herstellung von granuliertem Sorbensmittel und Anlage zur Durchführung des Verfahrens
RU2234367C1 (ru) 2002-12-15 2004-08-20 Закрытое акционерное общество "Экостар-Наутех" Способ получения сорбента для извлечения лития из рассолов
CN1243112C (zh) * 2002-12-27 2006-02-22 中国科学院青海盐湖研究所 吸附法从盐湖卤水中提取锂的方法
WO2009039133A1 (en) * 2007-09-17 2009-03-26 Areva Federal Services Llc A process for removal of aluminum oxides from aqueous media
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CN102872792A (zh) * 2012-08-28 2013-01-16 常州大学 一种去除天然水体中锂离子的复合吸附材料及其制备方法
FR3015458A1 (fr) * 2013-12-23 2015-06-26 Eramet Procede de preparation d'un materiau adsorbant mis en forme comprenant une etape de mise en forme en presence d'un liant mineral et procede d'extraction de lithium a partir de solutions salines utilisant ledit materiau
FR3015456B1 (fr) 2013-12-23 2017-05-19 Eramet Procede de preparation d'un materiau adsorbant mis en forme en l'absence de liant et procede d'extraction de lithium a partir de solutions salines utilisant ledit materiau
FR3020284A1 (fr) 2014-04-25 2015-10-30 Eramet Procede de preparation d'un materiau absorbant en l'absence de liant comprenant une etape de traitement hydrothermal et pocede d'extraction de lithium a partir de solutions salines utilisant ledit materiau
FR3036978B1 (fr) * 2015-06-05 2020-02-21 Eramet Procede de preparation d'un materiau adsorbant comprenant une etape de precipitation de boehmite operant dans des conditions specifiques et procede d'extraction de lithium a partir de solutions salines utilisant ledit materiau
CN105199434B (zh) * 2015-07-30 2017-08-25 四川大学 一种造纸专用型钛白粉的表面处理方法

Also Published As

Publication number Publication date
EP3464181B1 (fr) 2021-03-24
US11554358B2 (en) 2023-01-17
CN109415219B (zh) 2021-10-08
EP3464181A1 (fr) 2019-04-10
AR108577A1 (es) 2018-09-05
WO2017202825A1 (fr) 2017-11-30
FR3051787B1 (fr) 2022-07-08
FR3051787A1 (fr) 2017-12-01
CN109415219A (zh) 2019-03-01
US20200316557A1 (en) 2020-10-08

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