CH214808A - Process for the production of a new stain dye. - Google Patents

Process for the production of a new stain dye.

Info

Publication number
CH214808A
CH214808A CH214808DA CH214808A CH 214808 A CH214808 A CH 214808A CH 214808D A CH214808D A CH 214808DA CH 214808 A CH214808 A CH 214808A
Authority
CH
Switzerland
Prior art keywords
dye
sulfonic acid
oxy
acid
mol
Prior art date
Application number
Other languages
German (de)
Inventor
A-G Durand Huguenin
Original Assignee
Durand & Huguenin Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Durand & Huguenin Ag filed Critical Durand & Huguenin Ag
Publication of CH214808A publication Critical patent/CH214808A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B31/00Disazo and polyazo dyes of the type A->B->C, A->B->C->D, or the like, prepared by diazotising and coupling
    • C09B31/02Disazo dyes
    • C09B31/08Disazo dyes from a coupling component "C" containing directive hydroxyl and amino groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Zusatzpatent zum Hauptpatent     Nr.    -212415.    Verfahren zur Herstellung eines neuen     Beizenfarbstoffes.       Es wurde gefunden,     dass    man zu einem  neuen     Beizenfarbstoff    gelangt, wenn man  <B>1</B>     Mol.        2-Amino-5-naplitol-7-sulfosäure    mit  <B>1</B>     Mol.        diazotierter        1-Oxy-2-aminobenzol-4-          sulfosäure    alkalisch kuppelt,

   den erhaltenen       Monoazofarbstoff    weiter     diazotiert    und mit  der alkalischen Lösung von     1-(4'-Oxybenzol-          l'-sulfoyla,miiio)   <B>- 8 -</B>     oxynaphtalin-6-sulfosäure-          3'-carbonsäure    kombiniert.  



  Der erhaltene     Disazofarbstoff    kann vorteil  haft mit einer     ehromabgebenden    Substanz  behandelt werden, um als     ehromhaltiger    Farb  stoff verwendet zu werden.    <I>Beispiel:</I>    <B>189</B> Teile     1-Oxy-2-a-rninobenzol-4-sulfo-          säure    werden wie üblich     diazotiert    und in  alkalischer Lösung mit<B>239</B> Teilen     2-Amino-          5-iiaphtol,-7-sulfosäure    vereinigt.

   Der gebildete       Monoazofarbstoff    wird weiter     diazotiert    und  mit einer alkalischen Lösung von 439 Teilen  <B>1 -</B>     (4'-        Oxybenzol-        l'-sulfoylamino)-   <B>8</B> -oxynaph-         talin-   <B>6</B>     -sulfosäure-        3'-carbonsäure    kombiniert.  Nach beendeter Kupplung wird der erhaltene       Disazofarbstoff    in üblicher Weise durch     Aus-          salzen    abgeschieden.  



  Der neue, so erhaltene Farbstoff bildet       ein    dunkles Pulver, das sich in Wasser mit       rotsticliigblauer    Farbe und in konzentrierter  Schwefelsäure mit     grünstichigblauer    Farbe  löst. Im     Chromdruck    auf Baumwolle liefert  er blaue Töne, die sich durch gute     Echtheiten     auszeichnen.



  Additional patent to main patent no. -212415. Process for the production of a new mordant dye. It has been found that a new mordant dye is obtained if 1 mole of 2-amino-5-naplitol-7-sulfonic acid is mixed with 1 mole of diazotized 1-oxy -2-aminobenzene-4-sulfonic acid alkaline coupling,

   the monoazo dye obtained is further diazotized and combined with the alkaline solution of 1- (4'-oxybenzene-l'-sulfoyla, miiio) - 8 - oxynaphthalene-6-sulfonic acid-3'-carboxylic acid.



  The disazo dye obtained can advantageously be treated with an Ehrom-donating substance to be used as an Ehrom-containing dye. <I> Example: </I> <B> 189 </B> parts of 1-oxy-2-α-rninobenzene-4-sulfonic acid are diazotized as usual and in an alkaline solution with <B> 239 </B> Parts of 2-amino-5-iiaphtol, -7-sulfonic acid combined.

   The monoazo dye formed is further diazotized and treated with an alkaline solution of 439 parts 1 - (4'-oxybenzene-1'-sulfoylamino) - 8 -oxynaphthalene- <B > 6 </B> -sulfonic acid- 3'-carboxylic acid combined. After the coupling has ended, the disazo dye obtained is deposited in the customary manner by salting out.



  The new dye obtained in this way forms a dark powder which dissolves in water with a reddish blue color and in concentrated sulfuric acid with a greenish blue color. In chrome print on cotton, it delivers blue tones that are characterized by good fastness properties.

 

Claims (1)

PATENTANSPR-9011: Verfahren zur Herstellung eines neuen Beizenfarbstoffes, dadurch gekennzeichnet, dass man<B>1</B> Mol. 2-Amino-5-naphtol-7-sulfosäure mit<B>1</B> Mol. diazotierter 1-Oxy-2-aminobenzol- 4-sulfosäure alkalisch kuppelt, den erhalte nen Monoazofarbstoff weiter diazotiert und mit der alkalischen Lösung von 1-(4'-Oxy-- benzol <B>- l-</B> sulfoylamino) PATENTANSPR-9011: Process for the preparation of a new mordant dye, characterized in that <B> 1 </B> mol. 2-amino-5-naphthol-7-sulfonic acid is mixed with <B> 1 </B> mol. 1 -Oxy-2-aminobenzene- 4-sulphonic acid coupling, the monoazo dye obtained is further diazotized and with the alkaline solution of 1- (4'-oxy-- benzene <B> - l- </B> sulfoylamino) <B>- 8 -</B> oxynaphtahn <B>- 6</B> - sulfosäure-3'-carbonsäure kombiniert. Der erhaltene Farbstoff bildet ein dunkles Pulver, das sieh in Wasser mit rotgtielii--- c blauer Farbe und in konzentrierter Schwefel säure mit grünstichigblauer Farbe lbst. Er liefert im Chromdruck auf Baumwolle blaue Töne, die sieh durch gute Echtheiten aus zeichnen. <B> - 8 - </B> oxynaphtahn <B> - 6 </B> - sulfonic acid-3'-carboxylic acid combined. The dye obtained forms a dark powder, which looks red in water with a reddish blue color and in concentrated sulfuric acid with a greenish blue color. In chrome printing on cotton, it delivers blue tones, which are characterized by good fastness properties. Er kann mit einer ehromabgeben- den Substanz behandelt werden, um als ehron-ihaltiger Farbstoff verwendet zu werden. It can be treated with an ehroma-releasing substance in order to be used as an ehron-containing dye.
CH214808D 1938-04-04 1939-04-03 Process for the production of a new stain dye. CH214808A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE214808X 1938-04-04
CH212415T 1939-04-03

Publications (1)

Publication Number Publication Date
CH214808A true CH214808A (en) 1941-05-15

Family

ID=25725224

Family Applications (1)

Application Number Title Priority Date Filing Date
CH214808D CH214808A (en) 1938-04-04 1939-04-03 Process for the production of a new stain dye.

Country Status (1)

Country Link
CH (1) CH214808A (en)

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