CH118603A - Process for the production of a new intermediate product in the tar color industry. - Google Patents

Process for the production of a new intermediate product in the tar color industry.

Info

Publication number
CH118603A
CH118603A CH118603DA CH118603A CH 118603 A CH118603 A CH 118603A CH 118603D A CH118603D A CH 118603DA CH 118603 A CH118603 A CH 118603A
Authority
CH
Switzerland
Prior art keywords
production
mol
new intermediate
intermediate product
color industry
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH118603A publication Critical patent/CH118603A/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D251/00Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40Nitrogen atoms
    • C07D251/42One nitrogen atom
    • C07D251/44One nitrogen atom with halogen atoms attached to the two other ring carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)

Description

  

  Verfahren zur Herstellung eines neuen Zwischenproduktes der Teerfarbenindustrie.    Es wurde gefunden,     :dass    man ein neues  Zwischenprodukt, das     Kondensationsprodukt     aus     Cyanurtrikarbonsäurechlorid,    und 1,8  Aminonaphthol-3,6--disulfosäure, erhält, wenn  man 1     Mol.        CyanurtrikaTbonsäurechlorid     auf 1     Mol.        1,8-Aminonaphtho#l-3,6-;disulfo-          säure    einwirken     lässt..     



  Das     Kondensationsprodukt    aus 1     Mol.          Cyanurtrikarbonsäurechlorid        und    1     Mol.        1,8-          Aminonaphthol-3,6-disulfosäure    bildet ein  gelbliches Pulver, welches. ein     wertvolles     Ausgangsmaterial zur Herstellung von Farb  stoffen darstellt.

           Beispiel:       In eine eiskalte Lösung von 36,3 Teilen       1,8-aminonaphthol-3,6-sulfos.surem    Natrium  in 1000 Teilen Wasser werden unter Rühren  26,8 Teile     Cya.nurtrikarbansäurechlorid,    die  mit Äther verdünnt, worden sind, zugegeben;

    es wird zirka. eine halbe Stunde bei niedri  ger Temperatur weiter gerührt,     Das        $on=            densationsprodukt    aus     1,8-Aminonaphthol-          3,6-sulfosäure    und     Cyanurtrikarbonsäurechlo-          rid    fällt     nach    dieser Zeit     aus,    es wird     fil-          triert,    gewaschen und getrocknet.



  Process for the production of a new intermediate product in the tar color industry. It has been found that: a new intermediate, the condensation product of cyanurtricarboxylic acid chloride and 1,8 aminonaphthol-3,6-disulphonic acid, is obtained if 1 mol. Of cyanuricarboxylic acid chloride is added to 1 mol. Of 1,8-aminonaphtho # l-3 , 6-; disulfonic acid leaves it to act.



  The condensation product of 1 mol. Cyanurtricarboxylic acid chloride and 1 mol. 1,8-aminonaphthol-3,6-disulfonic acid forms a yellowish powder which. represents a valuable starting material for the production of dyes.

           Example: 26.8 parts of Cya.nurtrikarbansäurechlorid, which have been diluted with ether, are added to an ice-cold solution of 36.3 parts of 1,8-aminonaphthol-3,6-sulfos.surem sodium in 1000 parts of water;

    it will be about. Stirring is continued for half an hour at a low temperature. The on = densation product of 1,8-aminonaphthol-3,6-sulfonic acid and cyanuricarboxylic acid chloride precipitates after this time, it is filtered, washed and dried.

 

Claims (1)

<B>PATENTANSPRUCH:</B> Verfahren zur Herstellung eines neuen Zwischenproduktes der Teerfarbenindustrie, des Kondensationsproduktes aus Cyanurtri- k.arbonsäurechlorid und 1,8-Aminonaphthol- 3,6-disulfosäure, dadurch gekennzeichnet, dass man 1 Mol. Cyanurtrikarbonsäurechlorid auf 1 Mol. 1,8-Aminonaphthol-3,6-disulfosäure einwirken lässt. <B> PATENT CLAIM: </B> Process for the production of a new intermediate product of the tar color industry, the condensation product of cyanuric carboxylic acid chloride and 1,8-aminonaphthol-3,6-disulphonic acid, characterized in that 1 mol. Of cyanuricarboxylic acid chloride is added to 1 Mol. 1,8-Aminonaphthol-3,6-disulfonic acid can act. Das Kondensationsprodukt aus 1 Mol. Cyanurtrikarbonsäurechlorid und 1 Mol. 1,8- Amino@naphthol-3,6-disulfosäure bildet ein gelbliches Pulver, welches ein wertvolles Ausgangsmaterial zur Herstellung von Farb stoffen darstellt. The condensation product of 1 mol. Cyanurtricarboxylic acid chloride and 1 mol. 1,8-Amino @ naphthol-3,6-disulfonic acid forms a yellowish powder, which is a valuable starting material for the production of dyes.
CH118603D 1922-09-07 1924-10-07 Process for the production of a new intermediate product in the tar color industry. CH118603A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH103430T 1922-09-07
CH118603T 1924-10-07

Publications (1)

Publication Number Publication Date
CH118603A true CH118603A (en) 1927-01-03

Family

ID=25706440

Family Applications (1)

Application Number Title Priority Date Filing Date
CH118603D CH118603A (en) 1922-09-07 1924-10-07 Process for the production of a new intermediate product in the tar color industry.

Country Status (1)

Country Link
CH (1) CH118603A (en)

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