CA3110398C - Method for preparing a high-purity hydrated nickel sulphate - Google Patents

Method for preparing a high-purity hydrated nickel sulphate Download PDF

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Publication number
CA3110398C
CA3110398C CA3110398A CA3110398A CA3110398C CA 3110398 C CA3110398 C CA 3110398C CA 3110398 A CA3110398 A CA 3110398A CA 3110398 A CA3110398 A CA 3110398A CA 3110398 C CA3110398 C CA 3110398C
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CA
Canada
Prior art keywords
nickel
organic phase
cobalt
rich
sulphate
Prior art date
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Active
Application number
CA3110398A
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English (en)
French (fr)
Other versions
CA3110398A1 (en
Inventor
Karel John Osten
Rossano Antonio Grassi
Arturo Gutierrez Clausdorff
Ryan Colin Harrison
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IGO Ltd
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IGO Ltd
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Filing date
Publication date
Priority claimed from AU2018903643A external-priority patent/AU2018903643A0/en
Application filed by IGO Ltd filed Critical IGO Ltd
Publication of CA3110398A1 publication Critical patent/CA3110398A1/en
Application granted granted Critical
Publication of CA3110398C publication Critical patent/CA3110398C/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/10—Sulfates
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/01—Preparation or separation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0476—Separation of nickel from cobalt
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/16—Extraction of metal compounds from ores or concentrates by wet processes by leaching in organic solutions
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C22B3/326—Ramified chain carboxylic acids or derivatives thereof, e.g. "versatic" acids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CA3110398A 2018-09-27 2019-09-26 Method for preparing a high-purity hydrated nickel sulphate Active CA3110398C (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
AU2018903643A AU2018903643A0 (en) 2018-09-27 Method for preparing a high-purity hydrated nickel sulphate
AU2018903643 2018-09-27
AU2019901760 2019-05-23
AU2019901760A AU2019901760A0 (en) 2019-05-23 Method for preparing a high-purity hydrated nickel sulphate
PCT/AU2019/051044 WO2020061639A1 (en) 2018-09-27 2019-09-26 Method for preparing a high-purity hydrated nickel sulphate

Publications (2)

Publication Number Publication Date
CA3110398A1 CA3110398A1 (en) 2020-04-02
CA3110398C true CA3110398C (en) 2024-01-16

Family

ID=69949184

Family Applications (1)

Application Number Title Priority Date Filing Date
CA3110398A Active CA3110398C (en) 2018-09-27 2019-09-26 Method for preparing a high-purity hydrated nickel sulphate

Country Status (8)

Country Link
US (1) US11993520B2 (https=)
EP (1) EP3856941A4 (https=)
JP (1) JP7459060B2 (https=)
KR (1) KR102820068B1 (https=)
CN (1) CN112840049B (https=)
AU (1) AU2019348192B2 (https=)
CA (1) CA3110398C (https=)
WO (1) WO2020061639A1 (https=)

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JP7360091B2 (ja) * 2019-12-27 2023-10-12 住友金属鉱山株式会社 溶媒抽出方法およびコバルト水溶液の製造方法
JP7348130B2 (ja) * 2020-04-24 2023-09-20 Ｊｘ金属株式会社 金属含有溶液中のマグネシウムイオン除去方法及び、金属回収方法
US10995014B1 (en) 2020-07-10 2021-05-04 Northvolt Ab Process for producing crystallized metal sulfates
CN114134341B (zh) * 2020-09-04 2023-01-13 苏州博萃循环科技有限公司 一种含镍钴锰的料液中镍钴锰的回收方法
CN116745236A (zh) 2020-11-03 2023-09-12 哈茨有限公司 用于结晶金属硫酸盐的处理工艺
PH12023551304A1 (en) 2020-11-12 2023-11-20 Hatch Ltd Processes and methods for production of crystallized metal sulfates
CN112553478A (zh) * 2020-12-02 2021-03-26 金川集团镍盐有限公司 一种氢氧化镍钴硫酸体系快速浸出的方法
KR20230145474A (ko) 2021-02-18 2023-10-17 해치 리미티드 리튬 및 배터리 화학물질 생성 시 황산나트륨 부산물 가공
JP7832303B2 (ja) * 2021-07-29 2026-03-17 ユミコア 金属を分離するための結晶化方法
KR102601662B1 (ko) * 2022-01-20 2023-11-10 포항공과대학교 산학협력단 2 서킷 공정에 의한 양극재용 고순도 니켈/코발트 혼합용액 제조방법
CN115058597B (zh) * 2022-06-30 2024-06-04 盛隆资源再生（无锡）有限公司 一种含钙、铁、钴、镍的电镀污泥的回收处理方法
WO2024073810A1 (en) * 2022-10-07 2024-04-11 Igo Limited Method for preparing high-purity mixed nickel and cobalt sulphate
WO2024213973A1 (en) * 2023-04-11 2024-10-17 Bactech Environmental Corporation A process for treating a material containing iron and sulphur
US12286360B2 (en) * 2023-07-26 2025-04-29 Pt Qmb New Energy Materials Cobalt-manganese sulfate solution from low nickel matte
WO2025020125A1 (zh) * 2023-07-26 2025-01-30 青美邦新能源材料有限公司 一种低冰镍制备电池级硫酸镍钴锰晶体的方法
JP2025530957A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料からニッケル酸化物を回収するためのオールインワンニッケル製錬方法
AU2024213150B2 (en) 2023-08-25 2025-06-26 Kemco All-in-one nickel recovering method for nickel metal recovery from raw materials containing nickel
JP2025530955A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料からニッケル水酸化物を回収するためのオールインワンニッケル製錬方法
JP2025530958A (ja) 2023-08-25 2025-09-19 コリア・ジンク・カンパニー・リミテッド ニッケルを含有する原料から硫酸ニッケル水溶液を製造する方法

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US3869257A (en) * 1972-08-17 1975-03-04 Int Nickel Co Production of nickel sulfate
NL169958C (nl) * 1977-03-09 1982-09-16 Stamicarbon Werkwijze voor het selectief extraheren van metaalionen uit waterige oplossingen daarvan.
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TWI667056B (zh) * 2018-04-30 2019-08-01 Chaoyang University Of Technology 錯合反應協同溶劑萃取回收金屬之方法
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Also Published As

Publication number Publication date
CN112840049B (zh) 2024-09-13
KR102820068B1 (ko) 2025-06-12
EP3856941A1 (en) 2021-08-04
US11993520B2 (en) 2024-05-28
JP7459060B2 (ja) 2024-04-01
JP2022502564A (ja) 2022-01-11
CA3110398A1 (en) 2020-04-02
AU2019348192A1 (en) 2021-03-18
US20210354997A1 (en) 2021-11-18
WO2020061639A1 (en) 2020-04-02
EP3856941A4 (en) 2022-06-15
AU2019348192B2 (en) 2024-07-11
CN112840049A (zh) 2021-05-25
KR20210065144A (ko) 2021-06-03

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